SU213005A1 - - Google Patents
Info
- Publication number
- SU213005A1 SU213005A1 SU1087548A SU1087548A SU213005A1 SU 213005 A1 SU213005 A1 SU 213005A1 SU 1087548 A SU1087548 A SU 1087548A SU 1087548 A SU1087548 A SU 1087548A SU 213005 A1 SU213005 A1 SU 213005A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- sulfuric acid
- kaolin
- alumina
- alunite
- dehydrated
- Prior art date
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 13
- 239000005995 Aluminium silicate Substances 0.000 description 6
- 235000012211 aluminium silicate Nutrition 0.000 description 6
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 6
- 238000000034 method Methods 0.000 description 6
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 5
- KPZTWMNLAFDTGF-UHFFFAOYSA-D trialuminum;potassium;hexahydroxide;disulfate Chemical class [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Al+3].[Al+3].[Al+3].[K+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O KPZTWMNLAFDTGF-UHFFFAOYSA-D 0.000 description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 3
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 229910021653 sulphate ion Inorganic materials 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052934 alunite Inorganic materials 0.000 description 1
- 239000010424 alunite Substances 0.000 description 1
- BIGPRXCJEDHCLP-UHFFFAOYSA-N ammonium bisulfate Chemical compound [NH4+].OS([O-])(=O)=O BIGPRXCJEDHCLP-UHFFFAOYSA-N 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000004576 sand Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Inorganic materials O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Landscapes
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Description
1 one
Изобретение касаетс переработки каолина сернокислотным способом с получением глинозема и других продуктов.The invention relates to the processing of kaolin by the sulfuric acid method to produce alumina and other products.
Известный способ переработки каолина на глинозем состоит в том, что .каолин обжигают при 560-580°С, обрабатывают концентрированной серной КИСЛОТОЙ, а затем полученный раствор обезжелезивают, обрабатыва , например бисульфатом аммони . Однако этот способ сложен, так как требует использовани серной КИСЛОТЫ высокой концентрации.A known method of processing kaolin on alumina is that calcium is calcined at 560-580 ° C, treated with concentrated sulfuric acid, and then the resulting solution is deironed by treating, for example, with ammonium bisulfate. However, this method is difficult because it requires the use of high concentration of sulfuric acid.
С целью интенсификации процесса предлагаетс серную кислоту использовать в концентрации 12-20% и обезжелезивание вести дегидратированным алунитом.In order to intensify the process, it is proposed to use sulfuric acid in a concentration of 12–20% and deironing to lead dehydrated alunite.
Пример. Каолин обжигают при 600- 800°С в течение 1 час, а затем обрабатывают оборотным раствором, содержащим 15-20% серной КИСЛОТЫ, при 103-105°С также 1 час. Иульпу сгущают при 90-98°С, после чего провод т трехкратную противоточную промывку кремнеземистого щлама, который используют в строительных цел х. Сернокислый раствор обезжелезивают добавлением дегидратированного алунита в количестве примерно 10% от каолина.Example. Kaolin is burned at 600–800 ° C for 1 hour, and then treated with a circulating solution containing 15–20% sulfuric acid, at 103–105 ° C, also for 1 hour. The pulp is concentrated at 90-98 ° C, after which a threefold counter-current washing of the silica sand, which is used for construction purposes, is carried out. The sulphate solution is deironed by adding dehydrated alunite in an amount of about 10% of kaolin.
Извлечение глинозема из каолина составл ет 90-92%, из алунита 90-95%, извлечение серного ангидрида и щелочей составл ет 89-96%.The extraction of alumina from kaolin is 90-92%, from alunite 90-95%, the extraction of sulfuric anhydride and alkali is 89-96%.
10ten
Предмет изобретени Subject invention
Способ переработки каолина на глинозем облсигом при повыщенных температурах иA method of processing kaolin to alumina by molding at elevated temperatures and
обработкой серной кислотой с последующим обезжелезиванием сернокислого раствора и выделением глинозема, отличающийс тем, что, с целью интенсификации процесса, серную кислоту используют в концентрацииtreatment with sulfuric acid followed by deferrization of the sulphate solution and release of alumina, characterized in that, in order to intensify the process, sulfuric acid is used in concentration
15-20% и обезжелезивание ведут дегидратированным алунитом.15-20% and deironing are dehydrated alunite.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1087548A SU213005A1 (en) | 1966-06-29 | 1966-06-29 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU1087548A SU213005A1 (en) | 1966-06-29 | 1966-06-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU213005A1 true SU213005A1 (en) | 1974-07-25 |
Family
ID=20439475
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU1087548A SU213005A1 (en) | 1966-06-29 | 1966-06-29 |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU213005A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6153157A (en) * | 1996-09-30 | 2000-11-28 | Mclaughlin Geosurveys Pty. Limited | Value improvements of clays |
-
1966
- 1966-06-29 SU SU1087548A patent/SU213005A1/ru active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6153157A (en) * | 1996-09-30 | 2000-11-28 | Mclaughlin Geosurveys Pty. Limited | Value improvements of clays |
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