SU1337399A1 - Method of producing extract from vegetable raw material - Google Patents
Method of producing extract from vegetable raw material Download PDFInfo
- Publication number
- SU1337399A1 SU1337399A1 SU853963223A SU3963223A SU1337399A1 SU 1337399 A1 SU1337399 A1 SU 1337399A1 SU 853963223 A SU853963223 A SU 853963223A SU 3963223 A SU3963223 A SU 3963223A SU 1337399 A1 SU1337399 A1 SU 1337399A1
- Authority
- SU
- USSR - Soviet Union
- Prior art keywords
- freon
- substances
- vitamin
- extract
- extraction
- Prior art date
Links
- 239000000284 extract Substances 0.000 title claims abstract description 12
- 239000002994 raw material Substances 0.000 title claims abstract description 9
- 238000000034 method Methods 0.000 title claims abstract description 7
- 235000013311 vegetables Nutrition 0.000 title abstract description 5
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 239000000126 substance Substances 0.000 claims abstract description 11
- AJDIZQLSFPQPEY-UHFFFAOYSA-N 1,1,2-Trichlorotrifluoroethane Chemical compound FC(F)(Cl)C(F)(Cl)Cl AJDIZQLSFPQPEY-UHFFFAOYSA-N 0.000 claims abstract description 6
- CYRMSUTZVYGINF-UHFFFAOYSA-N trichlorofluoromethane Chemical compound FC(Cl)(Cl)Cl CYRMSUTZVYGINF-UHFFFAOYSA-N 0.000 claims abstract description 6
- 244000205574 Acorus calamus Species 0.000 claims description 7
- 235000011996 Calamus deerratus Nutrition 0.000 claims description 7
- 241000196324 Embryophyta Species 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 240000000950 Hippophae rhamnoides Species 0.000 claims description 2
- 235000003145 Hippophae rhamnoides Nutrition 0.000 claims description 2
- 239000003507 refrigerant Substances 0.000 claims description 2
- 229930003231 vitamin Natural products 0.000 claims 3
- 239000011782 vitamin Substances 0.000 claims 3
- 229940088594 vitamin Drugs 0.000 claims 3
- 235000013343 vitamin Nutrition 0.000 claims 3
- 150000003722 vitamin derivatives Chemical class 0.000 claims 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 150000007513 acids Chemical class 0.000 claims 2
- YZXBAPSDXZZRGB-DOFZRALJSA-N arachidonic acid Chemical compound CCCCC\C=C/C\C=C/C\C=C/C\C=C/CCCC(O)=O YZXBAPSDXZZRGB-DOFZRALJSA-N 0.000 claims 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 claims 1
- 235000005979 Citrus limon Nutrition 0.000 claims 1
- 244000131522 Citrus pyriformis Species 0.000 claims 1
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims 1
- 229930003268 Vitamin C Natural products 0.000 claims 1
- 239000013543 active substance Substances 0.000 claims 1
- 229940114079 arachidonic acid Drugs 0.000 claims 1
- 235000021342 arachidonic acid Nutrition 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 229960001295 tocopherol Drugs 0.000 claims 1
- 239000011732 tocopherol Substances 0.000 claims 1
- 235000019154 vitamin C Nutrition 0.000 claims 1
- 239000011718 vitamin C Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000002904 solvent Substances 0.000 abstract description 2
- 239000000341 volatile oil Substances 0.000 abstract description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 1
- 244000025254 Cannabis sativa Species 0.000 description 4
- 244000144730 Amygdalus persica Species 0.000 description 2
- 235000006040 Prunus persica var persica Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 241000132536 Cirsium Species 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Изобретение относитс к эфирномасличному производству и направлено на повышение выхода экстрактивных веществ из растительного сырь . Способ получени экстракта предусматривает использование селективно действующих растворителей: хладона 11 и хладона 113 в соотношении от 99:1 до 90:10 при температурных режимах, обеспечивающих последовательное экстрагирование спирто-и жирорастворимых компонентов растительного сырь . 2 табл. СО СО -« Ьо Г) соThe invention relates to essential oil production and is aimed at increasing the yield of extractive substances from vegetable raw materials. The method of obtaining the extract involves the use of selectively acting solvents: freon 11 and freon 113 in a ratio from 99: 1 to 90:10 at temperature conditions that ensure the sequential extraction of alcohol and fat-soluble components of vegetable raw materials. 2 tab. CO CO - “bo d) with
Description
Изобретение относитс к эфиромас- личному производству и конкретно касаетс извлечени экстрактивных веществ из растительного сырь ,.The invention relates to the production of essential oils and specifically relates to the extraction of extractive substances from plant raw materials,.
Цель изобретени - более полное извлечение экстрактивных веществ,The purpose of the invention is a more complete extraction of extractives,
Способ осуществл етс следующим образом.The method is carried out as follows.
Растительное сьфье (корневища аира 5 трава тыс челистника и др.) измельчают до размера частиц 2-3 мм с последующим плющением до толщины лепестка 0,15-0,20 мм и экстрагируют смесью хладона 11 и хпадона 113 при их отнощении 99:1 - 90-10 в течение 90 мин при перемешивании при 15-2С с Далее температуру повышают до 50- 55 С .в течение 30-33 мин, после чего смесь охлаждают до 18-20°С и проно- д т отделение мисцеллы и выделение из нее экстракта известными способами .Vegetable sfye (rhizomes of calamus 5 grass, thousands of leaves, etc.) is crushed to a particle size of 2-3 mm, followed by flattening to a lobe thickness of 0.15-0.20 mm and extracted with a mixture of freon 11 and hpadone 113 at their ratio of 99: 1 - 90-10 for 90 minutes with stirring at 15-2 ° C After that, the temperature is raised to 50-55 ° C for 30-33 minutes, after which the mixture is cooled to 18-20 ° C and miscella is removed and the separation from her extract by known methods.
Наибольший выход экстрактивных веществ получен при этом при соот- ношени х хладон 1J: хладон 113 от 99:1 до 90:10 (см.табл.).The highest yield of extractive substances was obtained at the same time at a ratio of x freon 1J: freon 113 from 99: 1 to 90:10 (see tab.).
Использование смеси хладонов дл экстракции обеспечивает в сравнении с известными решени ми более полное извлечение экстрактивных веществ из растительного сырь (см,табл.2).The use of a mixture of refrigerants for extraction provides, in comparison with the known solutions, a more complete extraction of extractive substances from vegetable raw materials (see Table 2).
П .р и м е р 1. Экстрагируют корень аира, содержащий экстрактивные вещества 6,2 %, траву тыс челистника содержащую экстрактивные вещества 2,8 %. Растительное сырье измельчают до 2,,0 мм, лепесток до толщины 0,15-0,20 мм. Соотношение сырье грает воритель 1:4. Общее врем экстракции 90 мин, температура экстракции с 18P and me R 1. Extrarate the root of calamus, containing extractives 6.2%, and thousands of peach grass containing extractives 2.8%. Plant material is crushed to 2, ..., 0 mm, petal to a thickness of 0.15-0.20 mm. The ratio of raw materials graet voritel 1: 4. The total extraction time of 90 minutes, the extraction temperature with 18
до с последующим понижением температуры до .up with a subsequent decrease in temperature to.
Число оборотов мешалки 80 об/мин, хладон 11 - 90 %, хладон 113 - 10 %, выход экстракта аира 5,9 %, выход экстракта травы тыс челистника 2,5 %.The number of revolutions of the agitator is 80 rpm, freon 11 - 90%, freon 113 - 10%, the yield of extract of calamus 5.9%, the yield of extract of grass thousand populations 2.5%.
Пример 2. Экстрагируют корень аира, содержащий з кстрактивные вещества 6,2 %, траву тыс челистника, содержащую экстрактивных веществ 2,8%. Растительное сырье измельчают до 2,0-3,0 мм, лепесток до толщины 0,15-0,20 мм. Соотношение сырье: растворитель 1:4. Общее врем экстракций 90 мин, температура экстракции 18 - с последующим понижением температуры до 18 С. Число оборотов мешалки 80 об/мин, хладон II - 99 %, хладон 113 - I %, выход экстракта аира 5,6 %, выход экстракта тыс челистника 2,4 %.Example 2. Extract of calamus root containing extractable substances of 6.2%, grass thousand of peach extract containing 2.8% of extractive substances. Plant material is crushed to 2.0-3.0 mm, petal to a thickness of 0.15-0.20 mm. The ratio of raw materials: solvent 1: 4. The total extraction time is 90 minutes, the extraction temperature is 18 - followed by lowering the temperature to 18 C. The speed of the stirrer is 80 rpm, freon II - 99%, freon 113 - I%, extract of calamus extract 5.6%, extract yield thousand thistle 2.4%.
Данным способом можно экстрагировать различные виды растительного сырь : аира, тыс челистника, зверобо , облепихи и др.This method can be used to extract various types of plant raw materials: calamus, thousanist, zvetobo, sea buckthorn, etc.
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU853963223A SU1337399A1 (en) | 1985-10-08 | 1985-10-08 | Method of producing extract from vegetable raw material |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SU853963223A SU1337399A1 (en) | 1985-10-08 | 1985-10-08 | Method of producing extract from vegetable raw material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| SU1337399A1 true SU1337399A1 (en) | 1987-09-15 |
Family
ID=21200687
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SU853963223A SU1337399A1 (en) | 1985-10-08 | 1985-10-08 | Method of producing extract from vegetable raw material |
Country Status (1)
| Country | Link |
|---|---|
| SU (1) | SU1337399A1 (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2290043C1 (en) * | 2005-07-04 | 2006-12-27 | Олег Иванович Квасенков | Method for producing of smoking tobacco article having reduced resin and nicotine content |
| RU2290007C1 (en) * | 2005-07-08 | 2006-12-27 | Олег Иванович Квасенков | Method for producing of exploded tobacco |
-
1985
- 1985-10-08 SU SU853963223A patent/SU1337399A1/en active
Non-Patent Citations (1)
| Title |
|---|
| Патент US № 3150050, кл.16794, 1964. * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2290043C1 (en) * | 2005-07-04 | 2006-12-27 | Олег Иванович Квасенков | Method for producing of smoking tobacco article having reduced resin and nicotine content |
| RU2290007C1 (en) * | 2005-07-08 | 2006-12-27 | Олег Иванович Квасенков | Method for producing of exploded tobacco |
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