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SG11201609677WA - Method for reducing the chlorine content of organomonophosphites using dimethylaminobutane, triethylamine or triethanolamine - Google Patents

Method for reducing the chlorine content of organomonophosphites using dimethylaminobutane, triethylamine or triethanolamine

Info

Publication number
SG11201609677WA
SG11201609677WA SG11201609677WA SG11201609677WA SG11201609677WA SG 11201609677W A SG11201609677W A SG 11201609677WA SG 11201609677W A SG11201609677W A SG 11201609677WA SG 11201609677W A SG11201609677W A SG 11201609677WA SG 11201609677W A SG11201609677W A SG 11201609677WA
Authority
SG
Singapore
Prior art keywords
organomonophosphites
dimethylaminobutane
triethanolamine
triethylamine
reducing
Prior art date
Application number
SG11201609677WA
Inventor
Katrin Marie Dyballa
Robert Franke
Original Assignee
Evonik Degussa Gmbh
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE102014209536.0A external-priority patent/DE102014209536A1/en
Priority claimed from DE102014209534.4A external-priority patent/DE102014209534A1/en
Priority claimed from DE102014209532.8A external-priority patent/DE102014209532A1/en
Priority claimed from DE102014209533.6A external-priority patent/DE102014209533A1/en
Priority claimed from DE102015202722.8A external-priority patent/DE102015202722A1/en
Application filed by Evonik Degussa Gmbh filed Critical Evonik Degussa Gmbh
Publication of SG11201609677WA publication Critical patent/SG11201609677WA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/06Phosphorus compounds without P—C bonds
    • C07F9/062Organo-phosphoranes without P-C bonds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/18Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms
    • B01J31/1845Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes containing nitrogen, phosphorus, arsenic or antimony as complexing atoms, e.g. in pyridine ligands, or in resonance therewith, e.g. in isocyanide ligands C=N-R or as complexed central atoms the ligands containing phosphorus
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/025Purification; Separation; Stabilisation; Desodorisation of organo-phosphorus compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/06Phosphorus compounds without P—C bonds
    • C07F9/08Esters of oxyacids of phosphorus
    • C07F9/141Esters of phosphorous acids
    • C07F9/145Esters of phosphorous acids with hydroxyaryl compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/6574Esters of oxyacids of phosphorus
    • C07F9/65742Esters of oxyacids of phosphorus non-condensed with carbocyclic rings or heterocyclic rings or ring systems
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/6574Esters of oxyacids of phosphorus
    • C07F9/65744Esters of oxyacids of phosphorus condensed with carbocyclic or heterocyclic rings or ring systems
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07FACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02Phosphorus compounds
    • C07F9/547Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/6574Esters of oxyacids of phosphorus
    • C07F9/65748Esters of oxyacids of phosphorus the cyclic phosphorus atom belonging to more than one ring system

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
SG11201609677WA 2014-05-20 2015-04-29 Method for reducing the chlorine content of organomonophosphites using dimethylaminobutane, triethylamine or triethanolamine SG11201609677WA (en)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
DE102014209536.0A DE102014209536A1 (en) 2014-05-20 2014-05-20 Production of high-quality oxo alcohols from unstable raw material sources
DE102014209535 2014-05-20
DE102014209534.4A DE102014209534A1 (en) 2014-05-20 2014-05-20 New monophosphite ligands with a carbonate group
DE102014209532.8A DE102014209532A1 (en) 2014-05-20 2014-05-20 New monophosphite ligands with a tert-butyloxycarbonyl group
DE102014209533.6A DE102014209533A1 (en) 2014-05-20 2014-05-20 Mixtures of monophosphite ligand and their use to catalyze a hydroformylation reaction
DE102015202722.8A DE102015202722A1 (en) 2014-05-20 2015-02-16 Process for the catalytic production of aldehydes from olefins using monophosphite mixtures
PCT/EP2015/059290 WO2015176929A1 (en) 2014-05-20 2015-04-29 Method for reducing the chlorine content of organomonophosphites using dimethylaminobutane, triethylamine or triethanolamine

Publications (1)

Publication Number Publication Date
SG11201609677WA true SG11201609677WA (en) 2016-12-29

Family

ID=53039422

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201609677WA SG11201609677WA (en) 2014-05-20 2015-04-29 Method for reducing the chlorine content of organomonophosphites using dimethylaminobutane, triethylamine or triethanolamine

Country Status (10)

Country Link
US (2) US9840524B2 (en)
EP (3) EP3145941B1 (en)
JP (1) JP6490717B2 (en)
KR (1) KR101898369B1 (en)
CN (1) CN106414467A (en)
ES (3) ES2772074T3 (en)
PL (1) PL3145940T3 (en)
SG (1) SG11201609677WA (en)
TW (3) TW201607953A (en)
WO (3) WO2015176929A1 (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102014201756A1 (en) 2014-01-31 2015-08-06 Evonik Degussa Gmbh Purification of chlorine-contaminated organophosphorus compounds
DE102014202500A1 (en) 2014-02-12 2015-08-13 Evonik Degussa Gmbh Process for reducing the chlorine content of organobisphosphites
EP3029013B1 (en) * 2014-12-04 2018-06-13 Evonik Degussa GmbH Monophosphites with structural unit 4,4,5,5-Tetraphenyl-1,3,2-dioxaphospholan as ligands for hydroformylation catalysts
DE102015207860A1 (en) 2015-04-29 2016-11-03 Evonik Degussa Gmbh New monophosphite compounds with a methyl group
DE102015207864A1 (en) 2015-04-29 2016-11-03 Evonik Degussa Gmbh New monophosphite compounds with an ether group
EP3147291A1 (en) 2015-09-28 2017-03-29 Evonik Degussa GmbH Method for reducing the chlorine content of organo tetraphosphites
EP3176174A1 (en) * 2015-12-03 2017-06-07 Evonik Degussa GmbH Method for reducing the chlorine content of organo tetraphosphites
TWI874467B (en) 2019-11-05 2025-03-01 美商陶氏科技投資有限公司 Process for the recovery of rhodium from a catalyst purge stream from a c6 or higher olefin hydroformylation process
EP4393926B1 (en) * 2022-12-27 2025-07-02 Evonik Oxeno GmbH & Co. KG Process for the preparation of monophosphites
ES3041442T3 (en) * 2022-12-27 2025-11-12 Evonik Oxeno Gmbh & Co Kg Process for the preparation of a phosphoramidite and its further conversion to monophosphite

Family Cites Families (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2259104B1 (en) * 1974-01-25 1976-11-26 Rhone Poulenc Ind
US4835299A (en) * 1987-03-31 1989-05-30 Union Carbide Corporation Process for purifying tertiary organophosphites
ATE203044T1 (en) * 1992-10-05 2001-07-15 Ciba Sc Holding Ag METHOD FOR STABILIZING TRIVALUENT PHOSPHORUS COMPOUNDS WITH AMINES
US5449807A (en) 1994-11-18 1995-09-12 E. I. Du Pont De Nemours And Company Catalyzed vapor phase hydrocyanation of diolefinic compounds
US5440067A (en) 1994-11-18 1995-08-08 E. I. Dupont De Nemours And Company Catalyzed gas phase isomerization of nonconjugated 2-alkyl-3-monoalkenenitriles
US5962744A (en) 1998-03-27 1999-10-05 The Research Foundation Of State University Of New York Process for hydrocarbonylations in supercritical carbon dioxide
DE19853748A1 (en) * 1998-11-21 2000-05-25 Studiengesellschaft Kohle Mbh Production of chiral aldehyde by enantioselective hydroformylation, useful e.g. as intermediate for pharmaceuticals, uses transition metal catalyst complex containing phosphine-phosphite ligand
US6380421B1 (en) * 1999-09-20 2002-04-30 E. I. Du Pont De Nemours And Company Multidentate phosphite ligands, catalytic compositions containing such ligands and catalytic processes utilizing such catalytic compositions
DE19953058A1 (en) 1999-11-03 2001-05-10 Basf Ag Phosphites
DE102004049339A1 (en) 2004-10-08 2006-04-13 Basf Ag Process for the purification of phosphorus-containing chelate ligands
GB0519651D0 (en) 2005-09-27 2005-11-02 Univ Nottingham Ferrocenyl phosphite ligands for asymmetric catalysis and a method for their production
DE102006058682A1 (en) 2006-12-13 2008-06-19 Evonik Oxeno Gmbh Bisphosphite ligands for transition metal-catalyzed hydroformylation
DE102008043584A1 (en) 2008-11-07 2010-05-12 Evonik Oxeno Gmbh Process for the preparation of 6-chlorodibenzo (d, f) (1,3,2) -dioxaphosphepin
DE102011002640B4 (en) 2011-01-13 2021-10-07 Evonik Operations Gmbh Process for the purification of Biphephos
DE102011085883A1 (en) * 2011-11-08 2013-05-08 Evonik Oxeno Gmbh New organophosphorus compounds based on anthracentriol
US9108988B2 (en) * 2011-12-30 2015-08-18 Basf Se Method of purifying organic diphosphite compounds
CN104053663B (en) 2011-12-30 2017-07-04 巴斯夫欧洲公司 Method for purifying organic diphosphite compounds

Also Published As

Publication number Publication date
EP3145938B1 (en) 2018-12-26
ES2715677T3 (en) 2019-06-05
KR20170007428A (en) 2017-01-18
US9840524B2 (en) 2017-12-12
TW201602126A (en) 2016-01-16
EP3145940A1 (en) 2017-03-29
WO2015176927A1 (en) 2015-11-26
EP3145938A1 (en) 2017-03-29
KR101898369B1 (en) 2018-09-12
WO2015176928A1 (en) 2015-11-26
PL3145940T4 (en) 2019-05-31
PL3145940T3 (en) 2019-05-31
US20170088570A1 (en) 2017-03-30
EP3145941B1 (en) 2019-12-18
EP3145940B1 (en) 2018-12-12
JP6490717B2 (en) 2019-03-27
ES2772074T3 (en) 2020-07-07
US20170121355A1 (en) 2017-05-04
EP3145941A1 (en) 2017-03-29
US9751904B2 (en) 2017-09-05
JP2017515874A (en) 2017-06-15
WO2015176929A1 (en) 2015-11-26
ES2724352T3 (en) 2019-09-10
TW201607953A (en) 2016-03-01
TW201609778A (en) 2016-03-16
CN106414467A (en) 2017-02-15

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