SE9703928D0 - Methods of Preparing Prills of Ammonium Dinitramide (ADN) and Bimodal Blend of ADN Prills - Google Patents
Methods of Preparing Prills of Ammonium Dinitramide (ADN) and Bimodal Blend of ADN PrillsInfo
- Publication number
- SE9703928D0 SE9703928D0 SE9703928A SE9703928A SE9703928D0 SE 9703928 D0 SE9703928 D0 SE 9703928D0 SE 9703928 A SE9703928 A SE 9703928A SE 9703928 A SE9703928 A SE 9703928A SE 9703928 D0 SE9703928 D0 SE 9703928D0
- Authority
- SE
- Sweden
- Prior art keywords
- prills
- adn
- medium
- preparing
- methods
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 4
- 239000000203 mixture Substances 0.000 title abstract 2
- BRUFJXUJQKYQHA-UHFFFAOYSA-O ammonium dinitramide Chemical compound [NH4+].[O-][N+](=O)[N-][N+]([O-])=O BRUFJXUJQKYQHA-UHFFFAOYSA-O 0.000 title 3
- 230000002902 bimodal effect Effects 0.000 title 1
- 239000006185 dispersion Substances 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 1
- 238000002844 melting Methods 0.000 abstract 1
- 230000008018 melting Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
- 230000008023 solidification Effects 0.000 abstract 1
- 238000007711 solidification Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/087—Compounds containing nitrogen and non-metals and optionally metals containing one or more hydrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
- C06B21/005—By a process involving melting at least part of the ingredients
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B21/00—Apparatus or methods for working-up explosives, e.g. forming, cutting, drying
- C06B21/0033—Shaping the mixture
- C06B21/0066—Shaping the mixture by granulation, e.g. flaking
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B31/00—Compositions containing an inorganic nitrogen-oxygen salt
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/32—Compounds containing nitrogen bound to oxygen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Peptides Or Proteins (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Apparatus Associated With Microorganisms And Enzymes (AREA)
Abstract
The invention relates to a method of producing prills of ADN. The method comprises melting and dispersion of ADN in a nonpolar medium to obtain droplets of ADN in the medium; cooling the medium for solidification of the droplets into prills and separation of said prills from the medium. The invention is characterised in that ultrasonic energy is supplied to the medium during dispersion. The invention also concerns a polymodal mixture of ADN prills containing prills having a particle size of less than 40 mu m produced according to the method.
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9703928A SE512396C2 (en) | 1997-10-28 | 1997-10-28 | Methods of Preparing Prills of Ammonium Dinitramide (ADN) |
| AU97715/98A AU9771598A (en) | 1997-10-28 | 1998-10-27 | Method of producing prills of ammonium dinitramide (adn) |
| AU97716/98A AU9771698A (en) | 1997-10-28 | 1998-10-27 | Method of producing adn prills suitable for use in a polymer system |
| PCT/SE1998/001938 WO1999021795A1 (en) | 1997-10-28 | 1998-10-27 | Method of producing adn prills |
| AU97717/98A AU9771798A (en) | 1997-10-28 | 1998-10-27 | Method of producing adn prills |
| PCT/SE1998/001936 WO1999021793A1 (en) | 1997-10-28 | 1998-10-27 | Method of producing prills of ammonium dinitramide (adn) |
| PCT/SE1998/001937 WO1999021794A1 (en) | 1997-10-28 | 1998-10-27 | Method of producing adn prills suitable for use in a polymer system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE9703928A SE512396C2 (en) | 1997-10-28 | 1997-10-28 | Methods of Preparing Prills of Ammonium Dinitramide (ADN) |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| SE9703928D0 true SE9703928D0 (en) | 1997-10-28 |
| SE9703928L SE9703928L (en) | 1999-04-29 |
| SE512396C2 SE512396C2 (en) | 2000-03-13 |
Family
ID=20408770
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE9703928A SE512396C2 (en) | 1997-10-28 | 1997-10-28 | Methods of Preparing Prills of Ammonium Dinitramide (ADN) |
Country Status (3)
| Country | Link |
|---|---|
| AU (3) | AU9771598A (en) |
| SE (1) | SE512396C2 (en) |
| WO (3) | WO1999021793A1 (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6610157B1 (en) | 2000-01-14 | 2003-08-26 | Alliant Techsystems Inc. | Prilled energetic particles, and process for making the same |
| FR2935969B1 (en) | 2008-09-18 | 2011-05-13 | Snpe Materiaux Energetiques | PROCESS FOR OBTAINING DNA CRYSTALS BY VISCOUS-BASED CRYSTALLIZATION; DNA CRYSTALS AND ENERGETIC MATERIALS CONTAINING |
| WO2013043099A2 (en) * | 2011-09-22 | 2013-03-28 | Ijorari Hb | Process for manufacturing particles and particles thereby manufactured |
| FR3081864B1 (en) | 2018-05-30 | 2022-03-18 | Arianegroup Sas | OBTAINING CRYSTALS OF AMMMONIUM DINITROAMIDIDE (DNA); DNA CRYSTALS AND THE ENERGETIC COMPOSITES CONTAINING THEM |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5415852A (en) * | 1992-01-29 | 1995-05-16 | Sri International | Process for forming a dinitramide salt or acid by reaction of a salt or free acid of an N(alkoxycarbonyl)N-nitroamide with a nitronium-containing compound followed by reaction of the intermediate product respectively with a base or alcohol |
| US5587553A (en) * | 1994-11-07 | 1996-12-24 | Thiokol Corporation | High performance pressable explosive compositions |
| JP3719614B2 (en) * | 1995-05-26 | 2005-11-24 | 株式会社アイ・エイチ・アイ・エアロスペース | Synthesis method of ADN |
| SE516719C2 (en) * | 1995-08-08 | 2002-02-19 | Totalfoersvarets Forskningsins | Methods for preparing dinitramic acid and salts thereof |
| US5801453A (en) * | 1996-06-11 | 1998-09-01 | United Technologies Corporation | Process for preparing spherical energetic compounds |
| US5759458A (en) * | 1996-07-26 | 1998-06-02 | Thiokol Corporation | Process for the manufacture of high performance gun propellants |
-
1997
- 1997-10-28 SE SE9703928A patent/SE512396C2/en not_active IP Right Cessation
-
1998
- 1998-10-27 WO PCT/SE1998/001936 patent/WO1999021793A1/en not_active Ceased
- 1998-10-27 WO PCT/SE1998/001937 patent/WO1999021794A1/en not_active Ceased
- 1998-10-27 AU AU97715/98A patent/AU9771598A/en not_active Abandoned
- 1998-10-27 WO PCT/SE1998/001938 patent/WO1999021795A1/en not_active Ceased
- 1998-10-27 AU AU97716/98A patent/AU9771698A/en not_active Abandoned
- 1998-10-27 AU AU97717/98A patent/AU9771798A/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| AU9771798A (en) | 1999-05-17 |
| AU9771698A (en) | 1999-05-17 |
| SE9703928L (en) | 1999-04-29 |
| SE512396C2 (en) | 2000-03-13 |
| WO1999021795A1 (en) | 1999-05-06 |
| WO1999021793A1 (en) | 1999-05-06 |
| WO1999021794A1 (en) | 1999-05-06 |
| AU9771598A (en) | 1999-05-17 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| NUG | Patent has lapsed |