SE0403202L - Method for oxygen delignification of cellulose pulp with high-pressure mixing of chemicals - Google Patents
Method for oxygen delignification of cellulose pulp with high-pressure mixing of chemicalsInfo
- Publication number
- SE0403202L SE0403202L SE0403202A SE0403202A SE0403202L SE 0403202 L SE0403202 L SE 0403202L SE 0403202 A SE0403202 A SE 0403202A SE 0403202 A SE0403202 A SE 0403202A SE 0403202 L SE0403202 L SE 0403202L
- Authority
- SE
- Sweden
- Prior art keywords
- pulp
- pressure
- run
- delignification
- dwell time
- Prior art date
Links
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title abstract 2
- 229920002678 cellulose Polymers 0.000 title abstract 2
- 239000001913 cellulose Substances 0.000 title abstract 2
- 239000001301 oxygen Substances 0.000 title abstract 2
- 229910052760 oxygen Inorganic materials 0.000 title abstract 2
- 239000000126 substance Substances 0.000 title abstract 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 3
- 229910001882 dioxygen Inorganic materials 0.000 abstract 3
- 239000003513 alkali Substances 0.000 abstract 1
- 238000010924 continuous production Methods 0.000 abstract 1
- 238000010411 cooking Methods 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C9/00—After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
- D21C9/10—Bleaching ; Apparatus therefor
- D21C9/147—Bleaching ; Apparatus therefor with oxygen or its allotropic modifications
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Paper (AREA)
Abstract
The pulp is passed through a high-pressure delignification reactor run (R1-R3) and then depressurized and heated with steam before being supplied to a reactor system (R4) in a low-pressure run where the dwell time is greater than that in the high-pressure run. - A continuous process for the alkaline oxygen gas delignification of cellulose pulp which has been cooked and optionally washed (W1) after cooking and which is stored in a substantially atmospheric storage tower (ST) or pulp tank, comprises the use of a reactor system with multiple oxygen gas reactors. The pulp being delignified has a consistency of 8-18 % and a kappa value of at least 15 (more than 20). During delignification, alkali (NaOHMAIN) is added to the pulp to provide a starting pH of more than 9 and 5-50 kg oxygen per tonne pulp is added at a point before the first oxygen gas reactor in the system. The total dwell time for the pulp in the system is more than 45 minutes. The pulp is pressurized to a starting pressure of more than 15 bar during the initial addition of chemicals and initial mixing in required for delignification, then the pulp is supplied to multiple mixing locations (M1-M3), the pressure in the final location being at least 13 bar. The dwell time in this first high-pressure run is at least 3-10 minutes. The pulp is then depressurized to less than 10-12 bar, heated with steam in order to increase its temperature by at least 5 deg. C and then supplied to a reactor system in a low-pressure run where the dwell time is greater than that in the high-pressure run.
Priority Applications (7)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE0403202A SE0403202L (en) | 2004-12-30 | 2004-12-30 | Method for oxygen delignification of cellulose pulp with high-pressure mixing of chemicals |
| BRPI0506424-4A BRPI0506424A (en) | 2004-12-30 | 2005-09-05 | method for oxygen delignification of cellulose pulp by mixing chemicals |
| CA002559362A CA2559362A1 (en) | 2004-12-30 | 2005-09-05 | Method for oxygen delignification of cellulose pulp by mixing of chemicals |
| EP05777705A EP1834034A4 (en) | 2004-12-30 | 2005-09-05 | Method for oxygen delignification of cellulose pulp by mixing of chemicals |
| PCT/SE2005/001274 WO2006071163A1 (en) | 2004-12-30 | 2005-09-05 | Method for oxygen delignification of cellulose pulp by mixing of chemicals |
| JP2007549311A JP2008527183A (en) | 2004-12-30 | 2005-09-05 | Process for delignification of cellulose pulp with oxygen by mixing chemicals |
| US10/595,839 US20080271861A1 (en) | 2004-12-30 | 2005-09-05 | Method for Oxygen Delignification of Cellulose Pulp by Mixing of Chemicals |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE0403202A SE0403202L (en) | 2004-12-30 | 2004-12-30 | Method for oxygen delignification of cellulose pulp with high-pressure mixing of chemicals |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| SE0403202D0 SE0403202D0 (en) | 2004-12-30 |
| SE526707C2 SE526707C2 (en) | 2005-10-25 |
| SE0403202L true SE0403202L (en) | 2005-10-25 |
Family
ID=34102144
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE0403202A SE0403202L (en) | 2004-12-30 | 2004-12-30 | Method for oxygen delignification of cellulose pulp with high-pressure mixing of chemicals |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20080271861A1 (en) |
| EP (1) | EP1834034A4 (en) |
| JP (1) | JP2008527183A (en) |
| BR (1) | BRPI0506424A (en) |
| CA (1) | CA2559362A1 (en) |
| SE (1) | SE0403202L (en) |
| WO (1) | WO2006071163A1 (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20100317053A1 (en) * | 2009-06-15 | 2010-12-16 | Andritz Inc. | Process machinery for feeding pre-treated lignocellulosic materials into bioreactors for bio-fuels and biochemicals |
| SE540043C2 (en) * | 2015-11-27 | 2018-03-06 | Valmet Oy | Method and system for oxygen delignification of cellulose pulp |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4363697A (en) * | 1979-12-03 | 1982-12-14 | The Black Clawson Company | Method for medium consistency oxygen delignification of pulp |
| US5217575A (en) * | 1988-10-18 | 1993-06-08 | Kamyr Ab | Process for oxygen bleaching using two vertical reactors |
| US5460696A (en) * | 1993-08-12 | 1995-10-24 | The Boc Group, Inc. | Oxygen delignification method incorporating wood pulp mixing apparatus |
| SE9401628L (en) * | 1994-05-10 | 1995-11-11 | Stora Kopparbergs Bergslags Ab | Oxygen delignification procedure |
| US6319357B1 (en) * | 1995-10-23 | 2001-11-20 | Valmet Fibertech Aktiebolag | Method for two-stage oxygen bleaching and delignification of chemical pulp |
| SE505141C2 (en) * | 1995-10-23 | 1997-06-30 | Sunds Defibrator Ind Ab | Oxygen delignification of pulp in two stages with high loading of alkali and oxygen and temperature below 90 C in the first step |
| ATE214113T1 (en) * | 1995-12-07 | 2002-03-15 | Beloit Technologies Inc | DELIGNIFICATION OF MEDIUM CONSISTENCY PULP USING OXYGEN |
| SE510740C2 (en) * | 1996-11-26 | 1999-06-21 | Sunds Defibrator Ind Ab | Oxygen delignification control |
| SE522593C2 (en) * | 1999-07-06 | 2004-02-24 | Kvaerner Pulping Tech | Oxygen gas delignification system and method of pulp of lignocellulosic material |
-
2004
- 2004-12-30 SE SE0403202A patent/SE0403202L/en not_active IP Right Cessation
-
2005
- 2005-09-05 BR BRPI0506424-4A patent/BRPI0506424A/en not_active Application Discontinuation
- 2005-09-05 EP EP05777705A patent/EP1834034A4/en not_active Withdrawn
- 2005-09-05 CA CA002559362A patent/CA2559362A1/en not_active Abandoned
- 2005-09-05 US US10/595,839 patent/US20080271861A1/en not_active Abandoned
- 2005-09-05 WO PCT/SE2005/001274 patent/WO2006071163A1/en not_active Ceased
- 2005-09-05 JP JP2007549311A patent/JP2008527183A/en active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| EP1834034A1 (en) | 2007-09-19 |
| SE0403202D0 (en) | 2004-12-30 |
| EP1834034A4 (en) | 2012-12-19 |
| WO2006071163A1 (en) | 2006-07-06 |
| BRPI0506424A (en) | 2006-12-26 |
| US20080271861A1 (en) | 2008-11-06 |
| JP2008527183A (en) | 2008-07-24 |
| SE526707C2 (en) | 2005-10-25 |
| CA2559362A1 (en) | 2006-07-06 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| NUG | Patent has lapsed |