SE0004155D0 - Process for manufacture of a dendritic polyether - Google Patents
Process for manufacture of a dendritic polyetherInfo
- Publication number
- SE0004155D0 SE0004155D0 SE0004155A SE0004155A SE0004155D0 SE 0004155 D0 SE0004155 D0 SE 0004155D0 SE 0004155 A SE0004155 A SE 0004155A SE 0004155 A SE0004155 A SE 0004155A SE 0004155 D0 SE0004155 D0 SE 0004155D0
- Authority
- SE
- Sweden
- Prior art keywords
- core
- hydroxyoxetane
- initiator
- compound
- amount
- Prior art date
Links
- 239000004721 Polyphenylene oxide Substances 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 229920000570 polyether Polymers 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 3
- 239000003999 initiator Substances 0.000 abstract 3
- DWYJHMSKXMHOAP-UHFFFAOYSA-N oxetan-2-ol Chemical compound OC1CCO1 DWYJHMSKXMHOAP-UHFFFAOYSA-N 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 2
- 230000015556 catabolic process Effects 0.000 abstract 1
- 125000002091 cationic group Chemical group 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- 238000006731 degradation reaction Methods 0.000 abstract 1
- AHHWIHXENZJRFG-UHFFFAOYSA-N oxetane Chemical compound C1COC1 AHHWIHXENZJRFG-UHFFFAOYSA-N 0.000 abstract 1
- 125000003566 oxetanyl group Chemical group 0.000 abstract 1
- 238000007151 ring opening polymerisation reaction Methods 0.000 abstract 1
- 238000007142 ring opening reaction Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G83/00—Macromolecular compounds not provided for in groups C08G2/00 - C08G81/00
- C08G83/002—Dendritic macromolecules
- C08G83/003—Dendrimers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/06—Cyclic ethers having no atoms other than carbon and hydrogen outside the ring
- C08G65/16—Cyclic ethers having four or more ring atoms
- C08G65/18—Oxetanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/04—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers only
- C08G65/22—Cyclic ethers having at least one atom other than carbon and hydrogen outside the ring
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyethers (AREA)
Abstract
A process for manufacture of a dendritic polyether comprising a core, derived from a compound having two or more hydroxyl groups, and at least one branching generation being built up from at least one hydroxyoxetane having one oxetane group and at least one hydroxyl group is disclosed. The process comprises ring opening addition to said core and ring opening polymerization of said hydroxyoxetane. A mixture of the core compound and at least one cationic initiator is prepared and said hydroxyoxetane is fed to said mixture at a rate resulting in and/or maintaining a reaction temperature below onset at thermal degradation and in an amount resulting in at least one branching generation. The initiator is present in an amount of 0.1-0.5% by weight calculated on said core and said oxetane, preferably in an amount giving a ratio hydroxyl groups to initiator of between 1:0.01 and 1:0.05. Yielded dendritic polyether is sebsequently neutralised by addition of at least one alkaline compound and optionally purified.
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE0004155A SE524174C2 (en) | 2000-11-14 | 2000-11-14 | Process for preparing a dendritic polyether |
| EP01983047.0A EP1355975B1 (en) | 2000-11-14 | 2001-11-12 | Process for manufacture of a dendritic polyether |
| US10/416,712 US7176264B2 (en) | 2000-11-14 | 2001-11-12 | Process for manufacture of a dendritic polyether |
| AU2002214502A AU2002214502A1 (en) | 2000-11-14 | 2001-11-12 | Process for manufacture of a dendritic polyether |
| PCT/SE2001/002519 WO2002040572A1 (en) | 2000-11-14 | 2001-11-12 | Process for manufacture of a dendritic polyether |
| JP2002543576A JP2004514037A (en) | 2000-11-14 | 2001-11-12 | Method for producing dendritic polyether |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE0004155A SE524174C2 (en) | 2000-11-14 | 2000-11-14 | Process for preparing a dendritic polyether |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| SE0004155D0 true SE0004155D0 (en) | 2000-11-14 |
| SE0004155L SE0004155L (en) | 2002-05-15 |
| SE524174C2 SE524174C2 (en) | 2004-07-06 |
Family
ID=20281805
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| SE0004155A SE524174C2 (en) | 2000-11-14 | 2000-11-14 | Process for preparing a dendritic polyether |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7176264B2 (en) |
| EP (1) | EP1355975B1 (en) |
| JP (1) | JP2004514037A (en) |
| AU (1) | AU2002214502A1 (en) |
| SE (1) | SE524174C2 (en) |
| WO (1) | WO2002040572A1 (en) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1440995B1 (en) * | 2003-01-23 | 2019-08-07 | Rapp Polymere GmbH | Hydroxyl-group containing polymers |
| JP4639332B2 (en) * | 2005-02-09 | 2011-02-23 | 学校法人神奈川大学 | Dendritic polymer, radiation curable dendritic polymer, cured product, and production method thereof |
| EP1971627A1 (en) * | 2005-12-22 | 2008-09-24 | The Dow Chemical Company | Branched polyglycols and branched polyether functional organopolysiloxanes and coatings containing same |
| DE102006031152A1 (en) * | 2006-07-04 | 2008-01-10 | Byk-Chemie Gmbh | Polyhydroxy-functional polysiloxanes as anti-adhesive and dirt-repellent additives in coatings, polymeric molding compounds and thermoplastics, process for their preparation and their use |
| JP5383196B2 (en) * | 2006-09-19 | 2014-01-08 | 新日鉄住金化学株式会社 | Thermally polymerizable resin composition |
| DE102007026724A1 (en) * | 2007-06-06 | 2008-12-11 | Basf Coatings Japan Ltd., Yokohama | High OH binder and clearcoat compositions containing it with good optical properties and good scratch and chemical resistance |
| DE102007026722A1 (en) * | 2007-06-06 | 2008-12-11 | Basf Coatings Japan Ltd., Yokohama | Clearcoat compositions comprising hyperbranched, dendritic hydroxy-functional polyesters |
| US20090314183A1 (en) * | 2008-06-24 | 2009-12-24 | S.D. Warren Company | Multi-component Starch Binder Compositions |
| DE102008032066A1 (en) | 2008-07-08 | 2010-01-14 | Byk-Chemie Gmbh | Polyhydroxy-functional polysiloxanes as anti-adhesive and dirt-repellent additives in coatings, polymeric molding compounds and thermoplastics, process for their preparation and their use |
| DE102008032064A1 (en) | 2008-07-08 | 2010-01-14 | Byk-Chemie Gmbh | Polyhydroxy-functional polysiloxanes for increasing the surface energy of thermoplastics, processes for their preparation and their use |
| DE102009021912A1 (en) * | 2009-05-19 | 2010-12-02 | Byk-Chemie Gmbh | From oxetane-based macromonomers available polymers, processes for their preparation and their use as additives in coating materials and plastics |
| DE102009021913A1 (en) | 2009-05-19 | 2010-12-02 | Byk-Chemie Gmbh | Terminal unsaturated, oxetane-based macromonomers and process for their preparation |
| DE102011076019A1 (en) | 2011-05-18 | 2012-11-22 | Evonik Goldschmidt Gmbh | Alkoxylation products and processes for their preparation by means of DMC catalysts |
| DE102011109545A1 (en) | 2011-08-03 | 2013-02-07 | Evonik Goldschmidt Gmbh | Process for the preparation of polyethersiloxanes containing polyethercarbonate base structures |
| DE102011109541A1 (en) | 2011-08-03 | 2013-02-07 | Evonik Goldschmidt Gmbh | Use of polysiloxanes containing branched polyether radicals for the production of polyurethane foams |
| DE102011109614A1 (en) | 2011-08-03 | 2013-02-07 | Evonik Goldschmidt Gmbh | Process for the preparation of branched polyethercarbonates and their use |
| WO2018091448A1 (en) | 2016-11-15 | 2018-05-24 | Byk-Chemie Gmbh | Polyethers based on oxetanes for use as wetting agents and as dispersants and production thereof |
| CN109937222B (en) | 2016-11-15 | 2021-08-17 | 毕克化学有限公司 | Oxetane-based polyethers for use as wetting and dispersing agents and their production |
| CN110527109B (en) * | 2019-09-03 | 2021-06-11 | 北京大学口腔医学院 | Polyhydroxy hyperbranched polymer, preparation method and application thereof in dental composite resin |
| CN110760071A (en) * | 2019-10-12 | 2020-02-07 | 青岛大学 | Preparation method of a novel dendritic high-viscosity oil viscosity reducer |
| TWI781508B (en) * | 2020-10-30 | 2022-10-21 | 財團法人工業技術研究院 | Resin and ink |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2947722A (en) * | 1954-08-17 | 1960-08-02 | Hercules Powder Co Ltd | Stabilized polymeric oxetane molding compositions |
| FR2218351B1 (en) * | 1973-02-16 | 1976-05-14 | Protex Manuf Prod Chimiq | |
| US4393199A (en) * | 1981-05-12 | 1983-07-12 | S R I International | Cationic polymerization |
| US4988797B1 (en) * | 1989-03-14 | 1993-12-28 | Cationic polymerization of cyclic ethers | |
| US5099042A (en) | 1989-03-14 | 1992-03-24 | Thiokol Corporation | Synthesis of tetrafunctional polyethers and compositions formed therefrom |
| US4952644A (en) * | 1989-06-07 | 1990-08-28 | Thiokol Corporation | Synthesis of ABA triblock polymers and An B star polymers from cyclic ethers |
| US5516854A (en) * | 1990-07-27 | 1996-05-14 | Thiokol Corporation | Method of producing thermoplastic elastomers having alternate crystalline structure such as polyoxetane ABA or star block copolymers by a block linking process |
| SE514207C2 (en) * | 1999-03-23 | 2001-01-22 | Perstorp Ab | Hyperbranched dendritic polyether and process for its preparation |
| SE520971C2 (en) | 1999-08-20 | 2003-09-16 | Perstorp Ab | Process for producing an etheric alcohol |
-
2000
- 2000-11-14 SE SE0004155A patent/SE524174C2/en unknown
-
2001
- 2001-11-12 JP JP2002543576A patent/JP2004514037A/en active Pending
- 2001-11-12 WO PCT/SE2001/002519 patent/WO2002040572A1/en not_active Ceased
- 2001-11-12 US US10/416,712 patent/US7176264B2/en not_active Expired - Lifetime
- 2001-11-12 EP EP01983047.0A patent/EP1355975B1/en not_active Expired - Lifetime
- 2001-11-12 AU AU2002214502A patent/AU2002214502A1/en not_active Abandoned
Also Published As
| Publication number | Publication date |
|---|---|
| WO2002040572A1 (en) | 2002-05-23 |
| EP1355975A1 (en) | 2003-10-29 |
| SE0004155L (en) | 2002-05-15 |
| US20040059086A1 (en) | 2004-03-25 |
| SE524174C2 (en) | 2004-07-06 |
| JP2004514037A (en) | 2004-05-13 |
| EP1355975B1 (en) | 2016-08-31 |
| AU2002214502A1 (en) | 2002-05-27 |
| US7176264B2 (en) | 2007-02-13 |
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