RU2248160C2 - Method for manufacturing non-smoking products out of rustic tobacco - Google Patents
Method for manufacturing non-smoking products out of rustic tobacco Download PDFInfo
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- RU2248160C2 RU2248160C2 RU2003114904/12A RU2003114904A RU2248160C2 RU 2248160 C2 RU2248160 C2 RU 2248160C2 RU 2003114904/12 A RU2003114904/12 A RU 2003114904/12A RU 2003114904 A RU2003114904 A RU 2003114904A RU 2248160 C2 RU2248160 C2 RU 2248160C2
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- Prior art keywords
- shag
- extract
- rustic tobacco
- honey
- tobacco
- Prior art date
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- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 230000000391 smoking effect Effects 0.000 title claims description 5
- 235000002637 Nicotiana tabacum Nutrition 0.000 title abstract description 8
- 238000000034 method Methods 0.000 title abstract description 8
- 241000208125 Nicotiana Species 0.000 title abstract 5
- 239000000284 extract Substances 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000000843 powder Substances 0.000 claims abstract description 10
- 244000303040 Glycyrrhiza glabra Species 0.000 claims abstract description 8
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 claims abstract description 8
- 235000017443 Hedysarum boreale Nutrition 0.000 claims abstract description 8
- 235000007858 Hedysarum occidentale Nutrition 0.000 claims abstract description 8
- 239000001354 calcium citrate Substances 0.000 claims abstract description 8
- 235000013337 tricalcium citrate Nutrition 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000012907 honey Nutrition 0.000 claims abstract description 7
- 235000020374 simple syrup Nutrition 0.000 claims abstract description 7
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 4
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 4
- 229960005336 magnesium citrate Drugs 0.000 claims abstract description 4
- 239000004337 magnesium citrate Substances 0.000 claims abstract description 4
- 235000002538 magnesium citrate Nutrition 0.000 claims abstract description 4
- PLSARIKBYIPYPF-UHFFFAOYSA-H trimagnesium dicitrate Chemical compound [Mg+2].[Mg+2].[Mg+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O PLSARIKBYIPYPF-UHFFFAOYSA-H 0.000 claims abstract description 4
- 235000021384 green leafy vegetables Nutrition 0.000 claims abstract description 3
- 238000000605 extraction Methods 0.000 claims description 7
- 239000000679 carrageenan Substances 0.000 claims description 6
- 235000010418 carrageenan Nutrition 0.000 claims description 6
- 229920001525 carrageenan Polymers 0.000 claims description 6
- 229940113118 carrageenan Drugs 0.000 claims description 6
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 claims description 6
- 235000013311 vegetables Nutrition 0.000 claims description 5
- FNAQSUUGMSOBHW-UHFFFAOYSA-H calcium citrate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O FNAQSUUGMSOBHW-UHFFFAOYSA-H 0.000 claims description 4
- 235000003599 food sweetener Nutrition 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000003765 sweetening agent Substances 0.000 claims description 4
- 239000001649 glycyrrhiza glabra l. absolute Substances 0.000 claims description 3
- 229940051810 licorice root extract Drugs 0.000 claims description 3
- 235000020725 licorice root extract Nutrition 0.000 claims description 3
- 238000002360 preparation method Methods 0.000 claims description 3
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 2
- 229910052749 magnesium Inorganic materials 0.000 claims description 2
- 239000011777 magnesium Substances 0.000 claims description 2
- 229940091250 magnesium supplement Drugs 0.000 claims description 2
- 238000000465 moulding Methods 0.000 claims description 2
- 239000000126 substance Substances 0.000 abstract description 7
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 abstract description 6
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 5
- 229960002715 nicotine Drugs 0.000 abstract description 5
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 abstract description 5
- 239000001569 carbon dioxide Substances 0.000 abstract description 3
- 229910002092 carbon dioxide Inorganic materials 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 230000002035 prolonged effect Effects 0.000 abstract 1
- 239000008187 granular material Substances 0.000 description 5
- 244000061176 Nicotiana tabacum Species 0.000 description 3
- 235000001018 Hibiscus sabdariffa Nutrition 0.000 description 2
- 240000008415 Lactuca sativa Species 0.000 description 2
- 235000006679 Mentha X verticillata Nutrition 0.000 description 2
- 235000002899 Mentha suaveolens Nutrition 0.000 description 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 2
- 235000005291 Rumex acetosa Nutrition 0.000 description 2
- 240000007001 Rumex acetosella Species 0.000 description 2
- 235000003513 sheep sorrel Nutrition 0.000 description 2
- 235000019605 sweet taste sensations Nutrition 0.000 description 2
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 229930091371 Fructose Natural products 0.000 description 1
- 239000005715 Fructose Substances 0.000 description 1
- 235000003228 Lactuca sativa Nutrition 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- 244000300264 Spinacia oleracea Species 0.000 description 1
- 235000009337 Spinacia oleracea Nutrition 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- -1 citrate cation Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001947 glycyrrhiza glabra rhizome/root Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 235000012045 salad Nutrition 0.000 description 1
- 229930182490 saponin Natural products 0.000 description 1
- 150000007949 saponins Chemical class 0.000 description 1
- 235000017709 saponins Nutrition 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
Landscapes
- Manufacture Of Tobacco Products (AREA)
- Seasonings (AREA)
Abstract
FIELD: tobacco industry.
SUBSTANCE: one should prepare leaves of rustic tobacco according to the preset technology to be then extracted with carbon dioxide in supercritical state. Moreover, nicotine and fragrance-forming substances migrate into an extract's composition. Licorice roots should be, also, prepared according to the preset technique, reduced and extracted with liquid ammonia. The extracts obtained should be mixed with the powder obtained out of leaf vegetables, sugar syrup, honey, carraginan, calcium and/or magnesium citrate and water. The mixture obtained should be formed. The innovation enables to decrease the loss of valuable rustic tobacco components and improve organoleptic properties manufactured out of rustic tobacco.
EFFECT: more prolonged terms of storage period.
1 ex
Description
Изобретение относится к технологии производства некурительных никотинсодержащих изделий.The invention relates to a technology for the production of non-smoking nicotine-containing products.
Известен способ производства некурительного изделия из махорки, предусматривающий подготовку листьев махорки, СO2-экстрагирование с использованием двуокиси углерода в жидком состоянии, измельчение листьев махорки и их смешивание с порошком из корней солодки, пектином, фруктозой и СO2-экстрактом мяты перечной и формование смеси (Сакиев А.Э., Совершенствование технологии комплексной переработки табака и махорки в условиях Кыргызской республики. Автореферат дис. к.т.н. - Краснодар: КубГТУ-БГУ, 24.04.2003, с.13-15).A known method for the production of non-smoking items from shag, involving the preparation of leaves of shag, CO 2 -extraction using carbon dioxide in a liquid state, grinding leaves of shag and mixing them with powder from licorice roots, pectin, fructose and a CO 2 extract of peppermint and forming a mixture (Sakiev A.E., Improving the technology of integrated processing of tobacco and shag in the conditions of the Kyrgyz Republic. Abstract of thesis, Ph.D. - Krasnodar: KubGTU-BSU, 04.24.2003, p.13-15).
Недостатками этого способа являются высокие потери никотина и ароматобразующих веществ махорки, низкие органолептические свойства целевого продукта и малый срок его хранения.The disadvantages of this method are the high losses of nicotine and aroma-forming substances of shag, low organoleptic properties of the target product and its short shelf life.
Техническим результатом изобретения является сокращение потерь ценных компонентов махорки, улучшение органолептических свойств и увеличение срока хранения целевого продукта.The technical result of the invention is to reduce the loss of valuable components of shag, improve organoleptic properties and increase the shelf life of the target product.
Этот результат достигается тем, что в способе производства некурительного изделия из махорки, предусматривающем подготовку листьев махорки, СO2-экстрагирование, смешивание с препаратом из корней солодки и подслащивающим веществом и формование смеси, согласно изобретению, СO2-экстрагирование махорки осуществляют при надкритических параметрах экстрагента с получением экстракта, который смешивают с экстрактом, полученным после экстрагирования корней солодки жидким аммиаком, и при смешивании дополнительно вводят порошок из листовых овощей, каррагинан, цитрат кальция и/или магния и воду, а в качестве подслащивающего вещества используют сахарный сироп и мед, при этом смесь готовят при следующем соотношении компонентов с точностью ±5%, мас.ч:This result is achieved by the fact that in the method for producing a non-smoking product from shag, which involves preparing shag leaves, CO 2 extraction, mixing with a preparation from licorice roots and a sweetener and molding the mixture according to the invention, CO 2 extraction of shag is carried out under supercritical parameters of the extractant to obtain an extract, which is mixed with an extract obtained after extraction of licorice roots with liquid ammonia, and, when mixed, powder from sheet o oschey, carrageenan, calcium citrate and / or magnesium and water as well as the sweetener using sugar syrup and honey, and the mixture was prepared in the following ratio to within ± 5%, in parts by weight:
порошок из листовых овощей 290leaf vegetable powder 290
надкритический CO2-экстракт махорки 40supercritical CO 2 -shag extract 40
NН3-экстракт корней солодки 50NH 3- licorice root extract 50
сахарный сироп, в пересчете на 70% концентрацию 70sugar syrup, in terms of 70% concentration of 70
мед 10honey 10
каррагинан 30carrageenan 30
цитрат кальция и/или магния 400calcium and / or magnesium citrate 400
вода 100.water 100.
Способ реализуется следующим образом.The method is implemented as follows.
Пример 1.Example 1
Листья махорки подготавливают по общепринятой технологии и экстрагируют двуокисью углерода в надкритическом состоянии. Никотин и ароматобразующие вещества переходят в состав экстракта.Shag leaves are prepared according to generally accepted technology and extracted with supercritical carbon dioxide. Nicotine and aromatizing substances pass into the composition of the extract.
Корни солодки подготавливают по общепринятой технологии, измельчают, лепесткуют и экстрагируют жидким аммиаком. Мисцеллу отделяют и отгоняют экстрагент повышением температуры и/или снижением давления. В состав полученного экстракта входят, в основном, сапонины и тонизирующие вещества.Licorice roots are prepared according to conventional technology, crushed, lobed and extracted with liquid ammonia. Miscella is separated and the extractant is distilled off by increasing the temperature and / or reducing the pressure. The composition of the obtained extract consists mainly of saponins and tonic substances.
Полученные экстракты смешивают с порошком из листовых овощей, например салата, с сахарным сиропом, медом, каррагинаном, цитратом кальция и водой при следующем соотношении компонентов, мас.ч.:The obtained extracts are mixed with a powder from leafy vegetables, such as lettuce, with sugar syrup, honey, carrageenan, calcium citrate and water in the following ratio, wt.h .:
порошок салата 290salad powder 290
надкритический СO2-экстракт махорки 40supercritical CO 2 -shag extract 40
NН3-экстракт корней солодки 50NH 3- licorice root extract 50
сахарный сироп 70sugar syrup 70
мед 10honey 10
каррагинан 40carrageenan 40
цитрат кальция 400calcium citrate 400
вода 100.water 100.
В качестве порошка из листовых овощей можно использовать шпинат.As a powder from leafy vegetables, you can use spinach.
Точность соблюдения соотношения указана с учетом норм расхода сырья и точности существующего дозирующего оборудования. Полученную смесь формуют, например, в виде гранул, как традиционный водный насвай, от которого полученный продукт отличается выраженным сладким вкусом и характерным ароматом табака с цветочными тонами. Вид листовых овощей, за исключением щавеля, не оказывает заметного влияния на свойства целевого продукта. При использовании порошка из листьев щавеля во вкусе целевого продукта появляется пикантная кислинка. Выбор катиона кальция или магния цитрата не оказывает никакого влияния на свойства целевого продукта.The accuracy of the ratio is indicated taking into account the norms of consumption of raw materials and the accuracy of the existing dosing equipment. The resulting mixture is formed, for example, in the form of granules, like a traditional water nasvay, from which the resulting product has a distinct sweet taste and characteristic tobacco aroma with floral tones. The type of leafy vegetables, with the exception of sorrel, does not significantly affect the properties of the target product. When using powder from sorrel leaves in the taste of the target product, a spicy sourness appears. The choice of a cation of calcium or magnesium citrate does not have any effect on the properties of the target product.
По сравнению с наиболее близким аналогом потери никотина при переработке сокращены на 67-80%, ароматобразующих веществ на 73-92%.Compared with the closest analogue, the losses of nicotine during processing are reduced by 67-80%, of aromatizing substances by 73-92%.
Полученные по предлагаемому способу и наиболее близкому аналогу гранулы с диаметром около 2 мм расфасовывали в стеклянные пузырьки с резиновыми пробками по 50 г. Гранулы отбирали для дегустационной оценки непосредственно после изготовления через каждые 2 дня в течение 2 месяцев. Продукт, полученный по наиболее близкому аналогу, имел выраженный мятный сладкий вкус и легкий мятный запах с характерным оттенком солодкового корня, легко разжевывался, напоминая по консистенции помадные конфеты, терял вкус и аромат за 10-15 с, рассасывался до кашицы и терял вкус и аромат за 30-45 с, через 8 дней гранулы начали слипаться, через 10-12 дней комковались и прилипали к стенкам тары, то есть приходили в непригодное для употребления состояние.The granules with a diameter of about 2 mm obtained by the proposed method and the closest analogue were packaged in glass bubbles with rubber stoppers of 50 g each. Granules were selected for tasting evaluation immediately after production every 2 days for 2 months. The product obtained by the closest analogue had a pronounced mint sweet taste and a light mint smell with a characteristic shade of licorice root, was easily chewed, resembling fondant candies in consistency, lost taste and aroma in 10-15 seconds, resolved to gruel and lost taste and aroma after 30-45 s, after 8 days, the granules began to stick together, after 10-12 days they clumped and adhered to the walls of the container, that is, they came into an unusable state.
Продукт, полученный по предлагаемому способу, имел выраженные табачные тона с цветочным оттенком во вкусе и аромате, не разжевывался, рассасывался, теряя вкус и аромат за 2-4 минуты, гранулы не слипались в течение всего срока испытаний. Вид листовых овощей и выбор катиона цитрата на перечисленные свойства не оказывали влияния.The product obtained by the proposed method had pronounced tobacco tones with a floral hue in taste and aroma, did not chew, absorbed, losing taste and aroma in 2-4 minutes, the granules did not stick together during the entire test period. The type of leafy vegetables and the choice of citrate cation did not affect the listed properties.
Таким образом, предлагаемый способ позволяет сократить потери ценных веществ махорки и получить целевой продукт с улучшенными органолептическими свойствами и увеличенным сроком хранения.Thus, the proposed method allows to reduce the loss of valuable substances shag and to obtain the target product with improved organoleptic properties and increased shelf life.
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|---|---|---|---|
| RU2003114904/12A RU2248160C2 (en) | 2003-05-20 | 2003-05-20 | Method for manufacturing non-smoking products out of rustic tobacco |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| RU2003114904/12A RU2248160C2 (en) | 2003-05-20 | 2003-05-20 | Method for manufacturing non-smoking products out of rustic tobacco |
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| Publication Number | Publication Date |
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| RU2003114904A RU2003114904A (en) | 2004-11-20 |
| RU2248160C2 true RU2248160C2 (en) | 2005-03-20 |
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Cited By (154)
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| RU2429755C1 (en) * | 2010-11-23 | 2011-09-27 | Олег Иванович Квасенков | Method to produce non-smoking product from low-grade tobacco |
| RU2430634C1 (en) * | 2010-10-08 | 2011-10-10 | Олег Иванович Квасенков | Method to produce non-smoking product from low-grade tobacco |
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| RU2432843C1 (en) * | 2010-12-07 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
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| RU2438425C1 (en) * | 2011-01-20 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438422C1 (en) * | 2011-01-13 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438420C1 (en) * | 2011-01-11 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438480C1 (en) * | 2011-02-10 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2441420C1 (en) * | 2011-01-21 | 2012-02-10 | Олег Иванович Квасенков | Means to extract a non-smoking product from shag tobacco |
| RU2441505C1 (en) * | 2011-02-01 | 2012-02-10 | Олег Иванович Квасенков | Means to extract non-smoking product from shag tobacco |
| RU2441508C1 (en) * | 2011-02-01 | 2012-02-10 | Олег Иванович Квасенков | Means to extract non-smoking product from shag tobacco |
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| RU2441496C1 (en) * | 2011-01-21 | 2012-02-10 | Олег Иванович Квасенков | Means to manufacture non-smoking product from shag tobacco |
| RU2441506C1 (en) * | 2011-02-01 | 2012-02-10 | Олег Иванович Квасенков | Means to extract non-smoking product from shag tobacco |
| RU2443337C1 (en) * | 2010-12-15 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443339C1 (en) * | 2011-01-21 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443338C1 (en) * | 2010-12-23 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443332C1 (en) * | 2011-02-10 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443340C1 (en) * | 2011-01-21 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
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| RU2462120C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
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| RU2432804C1 (en) * | 2010-10-20 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432814C1 (en) * | 2010-11-18 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443333C1 (en) * | 2010-11-18 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2445860C1 (en) * | 2010-11-18 | 2012-03-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443334C1 (en) * | 2010-11-19 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443336C1 (en) * | 2010-11-23 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443335C1 (en) * | 2010-11-23 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2429755C1 (en) * | 2010-11-23 | 2011-09-27 | Олег Иванович Квасенков | Method to produce non-smoking product from low-grade tobacco |
| RU2434553C1 (en) * | 2010-11-26 | 2011-11-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2444960C1 (en) * | 2010-11-26 | 2012-03-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2444961C1 (en) * | 2010-11-30 | 2012-03-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2444962C1 (en) * | 2010-11-30 | 2012-03-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2446720C1 (en) * | 2010-11-30 | 2012-04-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432839C1 (en) * | 2010-11-30 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432842C1 (en) * | 2010-12-07 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432844C1 (en) * | 2010-12-07 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432843C1 (en) * | 2010-12-07 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2449674C1 (en) * | 2010-12-07 | 2012-05-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432845C1 (en) * | 2010-12-10 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432849C1 (en) * | 2010-12-10 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448591C1 (en) * | 2010-12-10 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432847C1 (en) * | 2010-12-10 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2449668C1 (en) * | 2010-12-10 | 2012-05-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2452348C1 (en) * | 2010-12-10 | 2012-06-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432848C1 (en) * | 2010-12-10 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432850C1 (en) * | 2010-12-10 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2432846C1 (en) * | 2010-12-10 | 2011-11-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443337C1 (en) * | 2010-12-15 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450591C1 (en) * | 2010-12-23 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448595C1 (en) * | 2010-12-23 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2449670C1 (en) * | 2010-12-23 | 2012-05-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443338C1 (en) * | 2010-12-23 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448586C1 (en) * | 2010-12-23 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2449669C1 (en) * | 2010-12-23 | 2012-05-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450590C1 (en) * | 2010-12-23 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2449671C1 (en) * | 2010-12-23 | 2012-05-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448594C1 (en) * | 2010-12-23 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450696C1 (en) * | 2010-12-23 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2436458C1 (en) * | 2010-12-23 | 2011-12-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448592C1 (en) * | 2010-12-23 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448593C1 (en) * | 2010-12-23 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448596C1 (en) * | 2010-12-23 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450593C1 (en) * | 2010-12-27 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2449672C1 (en) * | 2010-12-27 | 2012-05-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2452349C1 (en) * | 2010-12-27 | 2012-06-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450592C1 (en) * | 2010-12-27 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448597C1 (en) * | 2010-12-27 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450589C1 (en) * | 2010-12-27 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438419C1 (en) * | 2011-01-11 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443141C1 (en) * | 2011-01-11 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450595C1 (en) * | 2011-01-11 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2448588C1 (en) * | 2011-01-11 | 2012-04-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450594C1 (en) * | 2011-01-11 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438420C1 (en) * | 2011-01-11 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450619C1 (en) * | 2011-01-13 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450597C1 (en) * | 2011-01-13 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438421C1 (en) * | 2011-01-13 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450596C1 (en) * | 2011-01-13 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438422C1 (en) * | 2011-01-13 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438424C1 (en) * | 2011-01-20 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438425C1 (en) * | 2011-01-20 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450598C1 (en) * | 2011-01-20 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2441418C1 (en) * | 2011-01-21 | 2012-02-10 | Олег Иванович Квасенков | Means to extract a non-smoking product from shag tobacco |
| RU2441496C1 (en) * | 2011-01-21 | 2012-02-10 | Олег Иванович Квасенков | Means to manufacture non-smoking product from shag tobacco |
| RU2438428C1 (en) * | 2011-01-21 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443340C1 (en) * | 2011-01-21 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2441420C1 (en) * | 2011-01-21 | 2012-02-10 | Олег Иванович Квасенков | Means to extract a non-smoking product from shag tobacco |
| RU2450599C1 (en) * | 2011-01-21 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450704C1 (en) * | 2011-01-21 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443339C1 (en) * | 2011-01-21 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450709C1 (en) * | 2011-01-27 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443341C1 (en) * | 2011-01-27 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450638C1 (en) * | 2011-01-27 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2441506C1 (en) * | 2011-02-01 | 2012-02-10 | Олег Иванович Квасенков | Means to extract non-smoking product from shag tobacco |
| RU2441505C1 (en) * | 2011-02-01 | 2012-02-10 | Олег Иванович Квасенков | Means to extract non-smoking product from shag tobacco |
| RU2441508C1 (en) * | 2011-02-01 | 2012-02-10 | Олег Иванович Квасенков | Means to extract non-smoking product from shag tobacco |
| RU2450660C1 (en) * | 2011-02-01 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450656C1 (en) * | 2011-02-01 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2453253C1 (en) * | 2011-02-01 | 2012-06-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450615C1 (en) * | 2011-02-01 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2438480C1 (en) * | 2011-02-10 | 2012-01-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443332C1 (en) * | 2011-02-10 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2443248C1 (en) * | 2011-02-10 | 2012-02-27 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2450682C1 (en) * | 2011-02-10 | 2012-05-20 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2452299C1 (en) * | 2011-02-18 | 2012-06-10 | Олег Иванович Квасенков | Method for production of non-smoking products of rustic tobacco |
| RU2462125C1 (en) * | 2011-05-05 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco |
| RU2461330C1 (en) * | 2011-05-05 | 2012-09-20 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco |
| RU2459541C1 (en) * | 2011-05-11 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco |
| RU2461337C1 (en) * | 2011-05-17 | 2012-09-20 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460448C1 (en) * | 2011-05-17 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460447C1 (en) * | 2011-05-17 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2461338C1 (en) * | 2011-05-17 | 2012-09-20 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459542C1 (en) * | 2011-05-17 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462130C1 (en) * | 2011-05-17 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462154C1 (en) * | 2011-05-17 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2458600C1 (en) * | 2011-05-17 | 2012-08-20 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459545C1 (en) * | 2011-05-20 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459543C1 (en) * | 2011-05-20 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462132C1 (en) * | 2011-05-20 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459544C1 (en) * | 2011-05-20 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459551C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459547C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460426C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460438C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460430C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459552C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460439C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460429C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460436C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462106C1 (en) * | 2011-05-27 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460427C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460431C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460428C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460433C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459556C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462107C1 (en) * | 2011-05-27 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459553C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460434C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460424C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459549C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460437C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459550C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459554C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460432C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459548C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460435C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460425C1 (en) * | 2011-05-27 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2459555C1 (en) * | 2011-05-27 | 2012-08-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460423C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460420C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460422C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462115C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460421C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460419C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462111C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460440C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460441C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462112C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462117C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462113C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462108C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460417C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462114C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462110C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462109C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2460416C1 (en) * | 2011-06-10 | 2012-09-10 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462118C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462119C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462116C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462123C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462121C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462120C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
| RU2462122C1 (en) * | 2011-06-10 | 2012-09-27 | Олег Иванович Квасенков | Method for production of non-smoking products of tobacco (versions) |
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