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RU2011120055A - METHOD FOR TREATING HEAVY AND BITUMINOUS OIL PRODUCTS - Google Patents

METHOD FOR TREATING HEAVY AND BITUMINOUS OIL PRODUCTS Download PDF

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RU2011120055A
RU2011120055A RU2011120055/04A RU2011120055A RU2011120055A RU 2011120055 A RU2011120055 A RU 2011120055A RU 2011120055/04 A RU2011120055/04 A RU 2011120055/04A RU 2011120055 A RU2011120055 A RU 2011120055A RU 2011120055 A RU2011120055 A RU 2011120055A
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reactor
liquid product
bituminous oil
oil
gas
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RU2011120055/04A
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RU2495079C2 (en
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Джерард МОНАГАН
Стивен ПОРТЕР
Росс ХОЛАК
Роберт СУГИЯМА
Уэйн БРАУН
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ИТиИкс СИСТЕМЗ ИНК.
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/002—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal in combination with oil conversion- or refining processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/36—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with fluidised bed through which there is an essentially horizontal flow of particles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/02—Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by distillation
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G11/14—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts
    • C10G11/18—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts according to the "fluidised-bed" technique
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G51/00—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only
    • C10G51/02—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only plural serial stages only
    • C10G51/023—Treatment of hydrocarbon oils, in the absence of hydrogen, by two or more cracking processes only plural serial stages only only thermal cracking steps
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G7/00—Distillation of hydrocarbon oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G70/00—Working-up undefined normally gaseous mixtures obtained by processes covered by groups C10G9/00, C10G11/00, C10G15/00, C10G47/00, C10G51/00
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G9/00—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
    • C10G9/28—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid material
    • C10G9/32—Thermal non-catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid material according to the "fluidised-bed" technique
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2400/00—Products obtained by processes covered by groups C10G9/00 - C10G69/14
    • C10G2400/02—Gasoline

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  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Combustion & Propulsion (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

1. Способ облагораживания битуминозной нефти, добытой из нефтяного пласта, без обработки водородом, содержащий:(a) контактирование добываемой битуминозной нефти в колонне фракционирования с нагретыми газами из реактора с псевдоожиженным слоем и фракционирование битуминозной нефти и нагретых газов на отдельные продукты, включающие по меньшей мере жидкую смолу, нестабильные фракции и облагороженный жидкий продукт;(b) введение жидкой смолы в реактор для получения паровой фазы жидкого продукта, причем реактор содержит твердые частицы, перемещающиеся через реактор, и сжижающий газ, осуществляющий псевдоожижение твердых частиц при температуре превращения, достаточной для химического превращения по крайней мере некоторой части жидкой смолы в паровую фазу жидкого продукта;(c) направление нагретых газов, содержащих паровую фазу жидкого продукта и сжижающий газ, из реактора в колонну фракционирования для контактирования с потоком битуминозной нефти; и(d) сжигание отделенных нестабильных фракций в количестве, достаточном для того, чтобы жидкий продукт и остаток нестабильных фракций удовлетворяли требованиям трубопроводной транспортировки без обработки водородом остатка нестабильных фракций.2. Способ по п.1, в котором во время этапа фракционирования битуминозной нефти и нагретых газов вырабатывается также неконденсирующийся газ, по крайней мере некоторая часть которого используется в реакторе в качестве сжижающего газа.3. Способ по п.1, в котором реактор вырабатывает кокс, когда жидкая смола превращается в паровую фазу жидкого продукта, при этом способ дополнительно содержит использование по крайней мере неко1. A method for upgrading bituminous oil produced from an oil reservoir without hydrogen treatment, comprising: (a) contacting the produced bituminous oil in a fractionation column with heated gases from a fluidized bed reactor and fractionating the bituminous oil and heated gases into separate products, including at least liquid resin, unstable fractions and refined liquid product; (b) introducing a liquid resin into a reactor to obtain a vapor phase of a liquid product, the reactor contains solid particles moving through the reactor, and a liquefying gas that fluidizes the solid particles at a transformation temperature sufficient to chemically converting at least some of the liquid resin to the vapor phase of the liquid product; (c) directing heated gases containing the vapor phase of the liquid product and liquefying gas from the reactor to the fractionation column for contact with the bituminous oil stream; and (d) incinerating the separated unstable fractions in an amount sufficient to ensure that the liquid product and the remainder of the unstable fractions meet pipeline transportation requirements without hydrogenating the unstable fractions. 2. The method according to claim 1, wherein during the step of fractionating the bituminous oil and heated gases, a non-condensable gas is also generated, at least some of which is used in the reactor as a liquefying gas. The method according to claim 1, in which the reactor produces coke when the liquid resin is converted into the vapor phase of the liquid product, and the method further comprises using at least some

Claims (15)

1. Способ облагораживания битуминозной нефти, добытой из нефтяного пласта, без обработки водородом, содержащий:1. A method for upgrading bituminous oil produced from an oil reservoir without treatment with hydrogen, comprising: (a) контактирование добываемой битуминозной нефти в колонне фракционирования с нагретыми газами из реактора с псевдоожиженным слоем и фракционирование битуминозной нефти и нагретых газов на отдельные продукты, включающие по меньшей мере жидкую смолу, нестабильные фракции и облагороженный жидкий продукт;(a) contacting the produced bituminous oil in the fractionation column with heated gases from a fluidized bed reactor and fractionating the bituminous oil and heated gases into separate products, including at least a liquid resin, unstable fractions and an upgraded liquid product; (b) введение жидкой смолы в реактор для получения паровой фазы жидкого продукта, причем реактор содержит твердые частицы, перемещающиеся через реактор, и сжижающий газ, осуществляющий псевдоожижение твердых частиц при температуре превращения, достаточной для химического превращения по крайней мере некоторой части жидкой смолы в паровую фазу жидкого продукта;(b) introducing a liquid resin into the reactor to obtain a vapor phase of the liquid product, wherein the reactor contains solid particles moving through the reactor and a liquefying gas fluidizing the solid particles at a conversion temperature sufficient to chemically convert at least some of the liquid resin to steam liquid product phase; (c) направление нагретых газов, содержащих паровую фазу жидкого продукта и сжижающий газ, из реактора в колонну фракционирования для контактирования с потоком битуминозной нефти; и(c) directing heated gases containing the vapor phase of the liquid product and the fluidizing gas from the reactor to the fractionation column for contacting with the bituminous oil stream; and (d) сжигание отделенных нестабильных фракций в количестве, достаточном для того, чтобы жидкий продукт и остаток нестабильных фракций удовлетворяли требованиям трубопроводной транспортировки без обработки водородом остатка нестабильных фракций.(d) burning the separated unstable fractions in an amount sufficient to ensure that the liquid product and the remainder of the unstable fractions satisfy the requirements of pipeline transportation without hydrogen treatment of the remainder of the unstable fractions. 2. Способ по п.1, в котором во время этапа фракционирования битуминозной нефти и нагретых газов вырабатывается также неконденсирующийся газ, по крайней мере некоторая часть которого используется в реакторе в качестве сжижающего газа.2. The method according to claim 1, wherein during the fractionation stage of tar oil and heated gases, non-condensable gas is also generated, at least some of which is used in the reactor as a fluidizing gas. 3. Способ по п.1, в котором реактор вырабатывает кокс, когда жидкая смола превращается в паровую фазу жидкого продукта, при этом способ дополнительно содержит использование по крайней мере некоторой части кокса для выработки пара с целью использования при добыче битуминозной нефти.3. The method according to claim 1, in which the reactor produces coke when the liquid resin is converted into the vapor phase of the liquid product, the method further comprises using at least some of the coke to generate steam for use in the production of bituminous oil. 4. Способ по п.1, в котором на операции сжигания нестабильных фракций вырабатывается пар с целью использования при добыче битуминозной нефти.4. The method according to claim 1, in which the operation of burning unstable fractions produces steam for use in the extraction of bituminous oil. 5. Способ по п.4, в котором нестабильные фракции включают крекинг-нафту, по крайней мере часть которой улавливается в виде жидкой нафты для использования в качестве облагороженного жидкого продукта.5. The method according to claim 4, in which the unstable fractions include cracked naphtha, at least a portion of which is captured in the form of liquid naphtha for use as a refined liquid product. 6. Способ по п.3 или 4, в котором битуминозная нефть извлекается посредством гравитационного дренажа с закачкой пара или циклического возбуждения закачкой пара.6. The method according to claim 3 or 4, in which the bituminous oil is extracted by gravity drainage with steam injection or cyclic excitation by steam injection. 7. Способ по п.3 или 4, в котором пар вырабатывается посредством циркуляционного парогенератора с псевдоожиженным слоем и средствами очистки.7. The method according to claim 3 or 4, in which the steam is generated by means of a circulating fluidized bed steam generator and cleaning agents. 8. Способ по п.7, дополнительно содержащий частичное окисление по крайней мере некоторой части кокса для получения тепла, направление дымового газа, образующегося в результате частичного окисления, в циркуляционный парогенератор с псевдоожиженным слоем и средствами очистки, и контактирование дымового газа с известью для очистки дымового газа.8. The method according to claim 7, further comprising partially oxidizing at least some of the coke to produce heat, directing the flue gas resulting from the partial oxidation to a circulating fluidized-bed steam generator and cleaning agents, and contacting the flue gas with lime for cleaning flue gas. 9. Способ по п.8, дополнительно содержащий частичное окисление по крайней мере некоторой части кокса для получения тепла, в котором тепло используется для нагрева твердых частиц, сжижающего газа и низкосортного пара.9. The method of claim 8, further comprising partially oxidizing at least some of the coke to produce heat, in which heat is used to heat solid particles, a liquefying gas, and low-grade steam. 10. Способ по п.9, в котором продукция реактора подбирается таким образом, чтобы вырабатываемые количества кокса или нафты были достаточны для удовлетворения всех потребностей в энергии циркуляционного парогенератора с псевдоожиженным слоем и средствами очистки.10. The method according to claim 9, in which the reactor products are selected so that the generated amounts of coke or naphtha are sufficient to satisfy all the energy needs of the circulating fluidized bed steam generator and cleaning agents. 11. Способ по п.10, в котором продукция реактора подбирается таким образом, чтобы вырабатываемые количества кокса или нафты были достаточны для удовлетворения всех потребностей в энергии для нагрева твердых частиц и сжижающего газа, достаточного для использования их в реакторе.11. The method according to claim 10, in which the reactor products are selected so that the generated amounts of coke or naphtha are sufficient to satisfy all energy requirements for heating solid particles and liquefying gas, sufficient for use in the reactor. 12. Способ по п.1, в котором в колонне фракционирования нагретые газы контактируют с битуминозой нефтью таким образом, что температура кипения летучих веществ в битуминозной нефти уменьшается, благодаря чему становится возможным фракционирование без использования атмосферных и вакуумных перегонных колонн.12. The method according to claim 1, in which the heated gas in the fractionation column is contacted with bituminous oil in such a way that the boiling point of volatile substances in the bituminous oil is reduced, which makes fractionation possible without the use of atmospheric and vacuum distillation columns. 13. Способ по п.1, в котором нефть извлекается из пласта битуминозного песка.13. The method according to claim 1, in which the oil is extracted from a layer of tar sand. 14. Способ по п.1, в котором реактор представляет собой поперечно-поточный реактор с псевдоожиженным слоем.14. The method according to claim 1, in which the reactor is a cross-flow reactor with a fluidized bed. 15. Способ по п.1, в котором все нестабильные фракции сжигаются, так что остается только жидкий продукт, который удовлетворяет требованиям трубопроводной транспортировки. 15. The method according to claim 1, in which all unstable fractions are burned, so that only a liquid product remains that meets the requirements of pipeline transportation.
RU2011120055/04A 2008-11-14 2008-11-14 Method of refining heavy and bituminous oil products RU2495079C2 (en)

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EP (1) EP2361292A4 (en)
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AU (1) AU2008364184B2 (en)
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CA2737410C (en) 2011-04-15 2013-10-15 Fort Hills Energy L.P. Heat recovery for bitumen froth treatment plant integration with sealed closed-loop cooling circuit
CA2738700C (en) 2011-04-28 2013-11-19 Fort Hills Energy L.P. Tsru with inlet spray system configurations for distribution of solvent diluted tailings
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