RU2008115438A - Сферические зерна корунда на основе плавленого оксида алюминия, а также способ их получения - Google Patents
Сферические зерна корунда на основе плавленого оксида алюминия, а также способ их получения Download PDFInfo
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- RU2008115438A RU2008115438A RU2008115438/15A RU2008115438A RU2008115438A RU 2008115438 A RU2008115438 A RU 2008115438A RU 2008115438/15 A RU2008115438/15 A RU 2008115438/15A RU 2008115438 A RU2008115438 A RU 2008115438A RU 2008115438 A RU2008115438 A RU 2008115438A
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- 239000010431 corundum Substances 0.000 title claims abstract 8
- 229910052593 corundum Inorganic materials 0.000 title claims abstract 8
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 title abstract 2
- 239000006260 foam Substances 0.000 title 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract 4
- 238000010891 electric arc Methods 0.000 claims abstract 2
- 239000000155 melt Substances 0.000 claims abstract 2
- 238000000034 method Methods 0.000 claims abstract 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 2
- 239000011148 porous material Substances 0.000 claims 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims 1
- 239000000654 additive Substances 0.000 claims 1
- 230000000996 additive effect Effects 0.000 claims 1
- 238000002844 melting Methods 0.000 claims 1
- 230000008018 melting Effects 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 239000004576 sand Substances 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- KKCBUQHMOMHUOY-UHFFFAOYSA-N sodium oxide Chemical compound [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims 1
- 229910001948 sodium oxide Inorganic materials 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims 1
- 239000006004 Quartz sand Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
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Abstract
1. Сферические зерна корунда на основе плавленого оксида алюминия с диаметром зерен от 0,001 до 5 мм, максимальным содержанием оксида натрия 0,5 вес.% и максимальным содержанием оксида титана 0,5 вес.%, отличающиеся тем, что они имеют насыпной вес от 1,5 до 2,5 кг/л. ! 2. Сферические зерна корунда по п.1, отличающиеся тем, что они имеют удельную поверхность по БЭТ от 0,005 до 0,05 м2/г. ! 3. Сферические зерна корунда по п.1 или 2, отличающиеся тем, что у них прочность зерен на разрыв (по Vollstдdt) составляет ≥20 н, предпочтительно ≥40 н. ! 4. Сферические зерна корунда по п.1, отличающиеся тем, что они имеют объем пор, измеренный путем цифровой обработки изображения, менее 50%, предпочтительно менее 40%, особенно предпочтительно менее 30%. ! 5. Сферические зерна корунда по п.1, отличающиеся тем, что относительный объем, образованный микропорами размером менее 3 мкм, составляет у них больше 5%, предпочтительно больше 15%, в расчете на полный объем пор 30-40%. ! 6. Способ получения сферических зерен корунда по одному из пп.1-5, причем ! a) глинозем с добавкой от 0,1 до 1%, предпочтительно от 0,2 до 0,6% (от полного веса исходных материалов) кварцевого песка расплавляют в электродуговой печи, ! b) расплав разливают со скоростью разлива менее 100 кг/мин, ! c) плавленую струю разбивают сжатым воздухом при давлении от 3 до 10 бар, ! отличающийся тем, что плавку проводят в окислительных условиях.
Claims (6)
1. Сферические зерна корунда на основе плавленого оксида алюминия с диаметром зерен от 0,001 до 5 мм, максимальным содержанием оксида натрия 0,5 вес.% и максимальным содержанием оксида титана 0,5 вес.%, отличающиеся тем, что они имеют насыпной вес от 1,5 до 2,5 кг/л.
2. Сферические зерна корунда по п.1, отличающиеся тем, что они имеют удельную поверхность по БЭТ от 0,005 до 0,05 м2/г.
3. Сферические зерна корунда по п.1 или 2, отличающиеся тем, что у них прочность зерен на разрыв (по Vollstдdt) составляет ≥20 н, предпочтительно ≥40 н.
4. Сферические зерна корунда по п.1, отличающиеся тем, что они имеют объем пор, измеренный путем цифровой обработки изображения, менее 50%, предпочтительно менее 40%, особенно предпочтительно менее 30%.
5. Сферические зерна корунда по п.1, отличающиеся тем, что относительный объем, образованный микропорами размером менее 3 мкм, составляет у них больше 5%, предпочтительно больше 15%, в расчете на полный объем пор 30-40%.
6. Способ получения сферических зерен корунда по одному из пп.1-5, причем
a) глинозем с добавкой от 0,1 до 1%, предпочтительно от 0,2 до 0,6% (от полного веса исходных материалов) кварцевого песка расплавляют в электродуговой печи,
b) расплав разливают со скоростью разлива менее 100 кг/мин,
c) плавленую струю разбивают сжатым воздухом при давлении от 3 до 10 бар,
отличающийся тем, что плавку проводят в окислительных условиях.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005045180.2 | 2005-09-21 | ||
| DE102005045180A DE102005045180B4 (de) | 2005-09-21 | 2005-09-21 | Kugelförmige Korundkörner auf Basis von geschmolzenem Aluminiumoxid sowie ein Verfahren zu ihrer Herstellung |
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| Publication Number | Publication Date |
|---|---|
| RU2008115438A true RU2008115438A (ru) | 2009-10-27 |
| RU2378198C1 RU2378198C1 (ru) | 2010-01-10 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2008115438/15A RU2378198C1 (ru) | 2005-09-21 | 2006-09-13 | Сферические зерна корунда на основе плавленого оксида алюминия, а также способ их получения |
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| Country | Link |
|---|---|
| US (2) | US7654323B2 (ru) |
| EP (1) | EP1926686B1 (ru) |
| JP (1) | JP4834809B2 (ru) |
| CN (1) | CN101268014B (ru) |
| AT (1) | ATE425122T1 (ru) |
| BR (1) | BRPI0614845B1 (ru) |
| DE (2) | DE102005045180B4 (ru) |
| ES (1) | ES2323193T3 (ru) |
| MX (1) | MX2007009941A (ru) |
| PL (1) | PL1926686T3 (ru) |
| RU (1) | RU2378198C1 (ru) |
| SI (1) | SI1926686T1 (ru) |
| WO (1) | WO2007033787A1 (ru) |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8012533B2 (en) | 2005-02-04 | 2011-09-06 | Oxane Materials, Inc. | Composition and method for making a proppant |
| US7491444B2 (en) * | 2005-02-04 | 2009-02-17 | Oxane Materials, Inc. | Composition and method for making a proppant |
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- 2005-09-21 DE DE102005045180A patent/DE102005045180B4/de not_active Expired - Fee Related
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2006
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- 2006-09-13 PL PL06792037T patent/PL1926686T3/pl unknown
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| MX2007009941A (es) | 2009-02-18 |
| JP4834809B2 (ja) | 2011-12-14 |
| US8323792B2 (en) | 2012-12-04 |
| ES2323193T3 (es) | 2009-07-08 |
| BRPI0614845B1 (pt) | 2016-12-13 |
| RU2378198C1 (ru) | 2010-01-10 |
| EP1926686A1 (de) | 2008-06-04 |
| ATE425122T1 (de) | 2009-03-15 |
| DE102005045180B4 (de) | 2007-11-15 |
| CN101268014B (zh) | 2011-06-22 |
| CN101268014A (zh) | 2008-09-17 |
| EP1926686B1 (de) | 2009-03-11 |
| JP2009508788A (ja) | 2009-03-05 |
| PL1926686T3 (pl) | 2009-07-31 |
| WO2007033787A1 (de) | 2007-03-29 |
| SI1926686T1 (sl) | 2009-06-30 |
| DE502006003119D1 (de) | 2009-04-23 |
| BRPI0614845A2 (pt) | 2011-04-19 |
| US20090162656A1 (en) | 2009-06-25 |
| US20070062699A1 (en) | 2007-03-22 |
| US7654323B2 (en) | 2010-02-02 |
| DE102005045180A1 (de) | 2007-05-24 |
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