RU2007110828A - Способ производства полиуретан(мет)акрилатов - Google Patents
Способ производства полиуретан(мет)акрилатов Download PDFInfo
- Publication number
- RU2007110828A RU2007110828A RU2007110828/04A RU2007110828A RU2007110828A RU 2007110828 A RU2007110828 A RU 2007110828A RU 2007110828/04 A RU2007110828/04 A RU 2007110828/04A RU 2007110828 A RU2007110828 A RU 2007110828A RU 2007110828 A RU2007110828 A RU 2007110828A
- Authority
- RU
- Russia
- Prior art keywords
- diols
- aliphatic
- diol
- omega
- combination
- Prior art date
Links
- 229920002635 polyurethane Polymers 0.000 title claims 4
- 239000004814 polyurethane Substances 0.000 title claims 4
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 150000002009 diols Chemical class 0.000 claims 8
- 238000000034 method Methods 0.000 claims 8
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 6
- 125000001931 aliphatic group Chemical group 0.000 claims 5
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 claims 4
- GHLKSLMMWAKNBM-UHFFFAOYSA-N dodecane-1,12-diol Chemical compound OCCCCCCCCCCCCO GHLKSLMMWAKNBM-UHFFFAOYSA-N 0.000 claims 4
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 claims 2
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 claims 2
- 229940043375 1,5-pentanediol Drugs 0.000 claims 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims 2
- ALQSHHUCVQOPAS-UHFFFAOYSA-N Pentane-1,5-diol Chemical compound OCCCCCO ALQSHHUCVQOPAS-UHFFFAOYSA-N 0.000 claims 2
- 150000001252 acrylic acid derivatives Chemical class 0.000 claims 2
- FOTKYAAJKYLFFN-UHFFFAOYSA-N decane-1,10-diol Chemical compound OCCCCCCCCCCO FOTKYAAJKYLFFN-UHFFFAOYSA-N 0.000 claims 2
- 125000005442 diisocyanate group Chemical group 0.000 claims 2
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims 2
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 claims 2
- 229920000166 polytrimethylene carbonate Polymers 0.000 claims 2
- 239000013638 trimer Substances 0.000 claims 2
- -1 aliphatic diols Chemical class 0.000 claims 1
- 239000011230 binding agent Substances 0.000 claims 1
- 239000008199 coating composition Substances 0.000 claims 1
- HLJDOURGTRAFHE-UHFFFAOYSA-N isocyanic acid;3,5,5-trimethylcyclohex-2-en-1-one Chemical compound N=C=O.N=C=O.CC1=CC(=O)CC(C)(C)C1 HLJDOURGTRAFHE-UHFFFAOYSA-N 0.000 claims 1
- 238000011403 purification operation Methods 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
- C09D175/16—Polyurethanes having carbon-to-carbon unsaturated bonds having terminal carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
- C08G18/3203—Polyhydroxy compounds
- C08G18/3206—Polyhydroxy compounds aliphatic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/671—Unsaturated compounds having only one group containing active hydrogen
- C08G18/672—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/721—Two or more polyisocyanates not provided for in one single group C08G18/73 - C08G18/80
- C08G18/722—Combination of two or more aliphatic and/or cycloaliphatic polyisocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/77—Polyisocyanates or polyisothiocyanates having heteroatoms in addition to the isocyanate or isothiocyanate nitrogen and oxygen or sulfur
- C08G18/78—Nitrogen
- C08G18/79—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates
- C08G18/791—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups
- C08G18/792—Nitrogen characterised by the polyisocyanates used, these having groups formed by oligomerisation of isocyanates or isothiocyanates containing isocyanurate groups formed by oligomerisation of aliphatic and/or cycloaliphatic isocyanates or isothiocyanates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G2150/00—Compositions for coatings
- C08G2150/20—Compositions for powder coatings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Polyurethanes Or Polyureas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Claims (8)
1. Способ получения полиуретан(мет)акрилатов, в котором тример (цикло)алифатического диизоцианата, 1,6-гександиизоцианат, диольный компонент и гидрокси-С2-С4-алкил(мет)акрилат, предпочтительно гидрокси-С2-С4-алкилакрилат, реагируют в мольном соотношении 1:х:x:3 в отсутствие растворителя и без последующих операций по очистке, где х означает любое желаемое значение от 1 до 6, желательно от 1 до 3, где диольный компонент представляет собой индивидуальный линейный алифатический альфа, омега-С2-С12 диол или комбинацию от двух до четырех, предпочтительно двух или трех, (цикло)алифатических диолов, где в случае комбинации диолов каждый из диолов составляет, по меньшей мере, 10 мол.% от диолов в комбинации диолов, а комбинация диолов состоит из, по меньшей мере, 80 мол.%, по меньшей мере, одного линейного алифатического альфа, омега-С2-С12 диола.
2. Способ по п.1, в котором х имеет любое значение от 1 до 3.
3. Способ по п.1, в котором тример (цикло)алифатического диизоцианата получают из диизоцианата, выбираемого из группы, состоящей из 1,4-циклогександиметилендиизоцианата, изофорондиизоцианата и 1,6-гександиизоцианата.
4. Способ по любому из пп.1-3, в котором комбинация диолов состоит из от двух до четырех линейных алифатических альфа, омега-С2-С12 диолов.
5. Способ по п.4, в котором линейный(ые) алифатический(ие) альфа, омега-С2-С12 диол(ы) выбирают из группы, состоящей из этиленгликоля, 1,3-пропандиола, 1,4-бутандиола, 1,5-пентандиола, 1,6-гександиола, 1,10-декандиола и 1,12-додекандиола.
6. Способ по любому из пп.1-3, в котором линейный(ые) алифатический(ие) альфа, омега-С2-С12 диол(ы) выбирают из группы, состоящей из этиленгликоля, 1,3-пропандиола, 1,4-бутандиола, 1,5-пентандиола, 1,6-гександиола, 1,10-декандиола и 1,12-додекандиола.
7. Полиуретан(мет)акрилаты, полученные способом по любому из пп.1-6.
8. Композиции порошковых покрытий, включающие в себя в качестве связующего полиуретан(мет)акрилаты, полученные способом по любому из пп.1-6.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/925,843 US20060047099A1 (en) | 2004-08-25 | 2004-08-25 | Process for the production of polyurethane (meth)acrylates |
| US10/925,843 | 2004-08-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2007110828A true RU2007110828A (ru) | 2008-10-10 |
Family
ID=35385440
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2007110828/04A RU2007110828A (ru) | 2004-08-25 | 2005-08-25 | Способ производства полиуретан(мет)акрилатов |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20060047099A1 (ru) |
| EP (1) | EP1791887A1 (ru) |
| CN (1) | CN101006115A (ru) |
| CA (1) | CA2576199A1 (ru) |
| NO (1) | NO20071551L (ru) |
| RU (1) | RU2007110828A (ru) |
| WO (1) | WO2006024037A1 (ru) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2648994C2 (ru) * | 2012-10-24 | 2018-03-29 | Басф Се | Радиационно отверждаемые, способные диспергироваться в воде полиуретан(мет)акрилаты |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060173122A1 (en) * | 2005-02-01 | 2006-08-03 | Carmen Flosbach | Non-aqueous, liquid coating compositions curable by free-radical polymerization of olefinic double bonds |
| US7714062B2 (en) * | 2006-12-22 | 2010-05-11 | Carmen Flosbach | Thermal curable powder coating composition |
| GB2447980B (en) * | 2007-03-30 | 2010-12-15 | Scott Bader Co | Thermosetting resin composition |
| US20090155462A1 (en) * | 2007-12-18 | 2009-06-18 | Carmen Flosbach | Thermal curable polyester powder coating composition |
| WO2013096195A1 (en) | 2011-12-21 | 2013-06-27 | U.S. Coatings Ip Co. Llc | Powder coating composition |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2189836C (en) * | 1995-12-04 | 2004-05-25 | Angela S. Rosenberry | Coating composition and floor covering including the composition |
| DE19933012A1 (de) * | 1999-07-14 | 2001-01-18 | Basf Ag | Härtbares Polyurethanpolymerisat |
| DE19947522A1 (de) * | 1999-10-02 | 2001-04-05 | Basf Ag | Polymerisierbare olefinisch ungesättigte Doppelbindungen enthaltende feste aliphatische Polyurethane auf der Basis linearer Diisocyanate und ihre Verwendung |
| DE19947523A1 (de) * | 1999-10-02 | 2001-04-05 | Basf Coatings Ag | Feststoff, enthaltend über Urethangruppen an die Grundstruktur gebundene Gruppen, die mit aktinischer Strahlung aktivierbare Bindungen enthalten, und ihre Verwendung |
| EP1336629A3 (de) * | 2002-02-16 | 2003-10-15 | Degussa AG | Verfahren zur Herstellung von Urethan(meth)acrylaten |
-
2004
- 2004-08-25 US US10/925,843 patent/US20060047099A1/en not_active Abandoned
-
2005
- 2005-08-25 WO PCT/US2005/030631 patent/WO2006024037A1/en not_active Ceased
- 2005-08-25 CA CA002576199A patent/CA2576199A1/en not_active Abandoned
- 2005-08-25 EP EP05792533A patent/EP1791887A1/en not_active Withdrawn
- 2005-08-25 CN CNA2005800286012A patent/CN101006115A/zh active Pending
- 2005-08-25 RU RU2007110828/04A patent/RU2007110828A/ru not_active Application Discontinuation
-
2007
- 2007-03-23 NO NO20071551A patent/NO20071551L/no not_active Application Discontinuation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2648994C2 (ru) * | 2012-10-24 | 2018-03-29 | Басф Се | Радиационно отверждаемые, способные диспергироваться в воде полиуретан(мет)акрилаты |
Also Published As
| Publication number | Publication date |
|---|---|
| CN101006115A (zh) | 2007-07-25 |
| US20060047099A1 (en) | 2006-03-02 |
| CA2576199A1 (en) | 2006-03-02 |
| WO2006024037A1 (en) | 2006-03-02 |
| EP1791887A1 (en) | 2007-06-06 |
| NO20071551L (no) | 2007-05-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA92 | Acknowledgement of application withdrawn (lack of supplementary materials submitted) |
Effective date: 20091016 |