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PT72208B - Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose - Google Patents

Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose

Info

Publication number
PT72208B
PT72208B PT72208A PT7220880A PT72208B PT 72208 B PT72208 B PT 72208B PT 72208 A PT72208 A PT 72208A PT 7220880 A PT7220880 A PT 7220880A PT 72208 B PT72208 B PT 72208B
Authority
PT
Portugal
Prior art keywords
galactosucrose
trideoxy
trichloro
preparation
Prior art date
Application number
PT72208A
Other languages
English (en)
Other versions
PT72208A (en
Original Assignee
Tate & Lyle Patent Holdings
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate & Lyle Patent Holdings filed Critical Tate & Lyle Patent Holdings
Publication of PT72208A publication Critical patent/PT72208A/pt
Publication of PT72208B publication Critical patent/PT72208B/pt

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Saccharide Compounds (AREA)
PT72208A 1979-12-20 1980-12-16 Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose PT72208B (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
GB7943933 1979-12-20
GB8010629 1980-03-28
GB8011086 1980-04-02
GB8016668 1980-05-20
GB8036711 1980-11-14

Publications (2)

Publication Number Publication Date
PT72208A PT72208A (en) 1981-01-01
PT72208B true PT72208B (en) 1981-10-28

Family

ID=27516402

Family Applications (1)

Application Number Title Priority Date Filing Date
PT72208A PT72208B (en) 1979-12-20 1980-12-16 Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose

Country Status (15)

Country Link
US (1) US4362869A (pt)
EP (1) EP0031651B1 (pt)
AU (1) AU532217B2 (pt)
CA (1) CA1152983A (pt)
DE (1) DE3062467D1 (pt)
DK (1) DK155946C (pt)
FI (1) FI68403C (pt)
GR (1) GR72482B (pt)
IL (1) IL61763A (pt)
NO (1) NO149389C (pt)
NZ (1) NZ195891A (pt)
PH (1) PH16877A (pt)
PT (1) PT72208B (pt)
SU (1) SU1176844A3 (pt)
YU (1) YU41010B (pt)

Families Citing this family (61)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0103479B1 (en) * 1982-09-13 1986-02-05 TATE & LYLE PUBLIC LIMITED COMPANY Sucrose derivatives
GB8525954D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Chlorination of carbohydrates &c alcohols
GB8525953D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Preparation of galactopyranoside
GB8525871D0 (en) * 1985-10-21 1985-11-27 Tate & Lyle Plc Chemical compound
GB8622342D0 (en) * 1986-09-17 1986-10-22 Tate & Lyle Plc Process
GB8622345D0 (en) * 1986-09-17 1986-10-22 Tate & Lyle Plc Sucrose derivatives
US4950746A (en) * 1988-07-18 1990-08-21 Noramco, Inc. Process for synthesizing sucrose derivatives by regioselective reaction
GB8818430D0 (en) * 1988-08-03 1988-09-07 Tate & Lyle Plc Process
DE68903624T2 (de) * 1988-09-16 1993-05-13 Tate & Lyle Plc Verfahren zur chlorierung von zucker.
GB8822673D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Selective acylation of sugars
GB8822674D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Preparation of acylated sucrose derivatives
US4980463A (en) * 1989-07-18 1990-12-25 Noramco, Inc. Sucrose-6-ester chlorination
US5089608A (en) * 1990-03-23 1992-02-18 Mcneil-Ppc, Inc. Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols
US5023329A (en) * 1990-04-23 1991-06-11 Noramco, Inc. Sucrose-6-ester production process
US5136031A (en) * 1990-07-09 1992-08-04 Tate & Lyle Public Limited Company Chlorination of sugars
NZ240818A (en) 1990-12-14 1993-08-26 Mcneil Ppc Inc Liquid sucralose concentrate compositions containing preservative, buffer and liquid
GB9110821D0 (en) 1991-05-21 1991-07-10 Tate & Lyle Plc Continuous process for the preparation of sucrose 6-esters
WO2002040495A2 (en) * 2000-11-17 2002-05-23 Mcneil-Ppc, Inc. Improved sucralose composition and process for the crystallization thereof
US6998480B2 (en) 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US7049435B2 (en) 2002-03-08 2006-05-23 Tate & Lyle Public Limited Company Extractive methods for purifying sucralose
US20040170735A2 (en) * 2002-04-05 2004-09-02 Mcneil-Ppc, Inc. Methods and compositions for altering the sweetness delivery profile of sucralose
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
US20040086605A1 (en) * 2002-10-30 2004-05-06 Sox Thomas E. Composition for delivering a high intensity sweetener
US6943248B2 (en) * 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
CA2558683A1 (en) * 2004-03-05 2005-09-22 Sunil Srivastava High-intensity sweetener-polyol compositions
US20050214425A1 (en) * 2004-03-23 2005-09-29 Roma Vazirani Sugar substitute prepared with nutritive and high-intensity sweeteners
CN101098972A (zh) * 2004-12-10 2008-01-02 法马德医疗保险私人有限公司 硅烷化硅胶色谱纯化6-乙酰基-4,1',6'三氯半乳蔗糖和4,1',6'三氯半乳蔗糖的改良方法
US20080125584A1 (en) * 2004-12-10 2008-05-29 Rakesh Ratnam Salts Assisted Selective Extraction Of 6-Acetyl- 4,1' , 6' Trichlorogalactosucrose And 4,1', 6' Trichlorogalactosucrosse From Aqueous Reaction Mixture
US20060188629A1 (en) * 2005-01-21 2006-08-24 Greg Liesen Method for the purification of sucralose
US7750146B2 (en) 2005-03-18 2010-07-06 Tate & Lyle Plc Granular sucralose
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
JP2008542199A (ja) * 2005-05-04 2008-11-27 ファームド メディケア プライヴェート リミテッド 五塩化リンとｄｍｆからの副生成物としてのオキシ塩化リンの生成及びビルスマイヤー・ハック試薬への変換による塩素化反応のためのその使用
CN101268091A (zh) * 2005-09-22 2008-09-17 法马德医疗保险私人有限公司 从无水氯化反应物料制备6-o-酰基氯化蔗糖的新型方法
US20070100139A1 (en) * 2005-10-31 2007-05-03 Healthy Brands, Llc Methods for chlorinating sucrose-6-ester
US7741477B2 (en) * 2006-01-10 2010-06-22 Alembic Limited Process for purification of sucralose
CN100395251C (zh) * 2006-01-12 2008-06-18 上海迪赛诺维生素有限公司 一种三氯蔗糖的合成方法
WO2007096726A2 (en) * 2006-02-20 2007-08-30 Emcure Pharmaceuticals Limited Process for the preparation of a glucose derivative
MX2008010982A (es) * 2006-02-28 2008-10-21 V B Medicare Private Ltd Reactivo novedosos de cloracion y proceso novedoso para la cloracion de azucares que usa cloruro de tionilo.
CN100418976C (zh) * 2006-04-03 2008-09-17 广州科宏食品添加物有限公司 一种三氯蔗糖的制备方法
AU2006345862A1 (en) * 2006-07-06 2008-01-10 Alembic Limited An improved process for the preparation of Sucralose of high purity
CN100567319C (zh) * 2006-07-12 2009-12-09 上海迪赛诺维生素有限公司 一种三氯蔗糖的结晶方法
CN100420697C (zh) * 2006-08-30 2008-09-24 河北苏科瑞科技有限公司 一种制备蔗糖-6-有机酸酯的方法
MX2009005889A (es) * 2006-12-05 2009-08-12 Tate & Lyle Technology Ltd Recuperacion de cloruro de tritilo.
CN101012253B (zh) * 2007-02-06 2010-04-14 启东东岳药业有限公司 6-pas的制备方法
WO2008099560A1 (ja) * 2007-02-16 2008-08-21 Masahiro Kajiwara アルドース誘導体の製造方法
US20080300392A1 (en) * 2007-06-04 2008-12-04 Polymed Therapeutics, Inc. Novel chlorination process for preparing sucralose
US20080300401A1 (en) * 2007-06-04 2008-12-04 Polymed Therapeutics, Inc. Novel chlorination process for preparing sucralose
CN101245085B (zh) 2007-12-19 2012-02-01 上海同辰生物科技有限公司 一种三氯蔗糖的合成及纯化工艺
US8436156B2 (en) * 2008-01-04 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
WO2009117317A1 (en) * 2008-03-20 2009-09-24 Tate & Lyle Technology Ltd Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
TW200946683A (en) * 2008-04-03 2009-11-16 Tate & Lyle Technology Ltd A process for the purification of aqueous feed streams containing sucralose extraction efficiency
US20090299055A1 (en) * 2008-04-03 2009-12-03 Tate & Lyle Technology Limited Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
US20090259036A1 (en) * 2008-04-03 2009-10-15 Tate & Lyle Technology Limited Extraction of less polar impurities from sucralose containing aqueous feed streams
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
CN102336786A (zh) * 2011-11-01 2012-02-01 安徽万和制药有限公司 一种三氯蔗糖的高效结晶方法
CN102336787B (zh) * 2011-11-01 2014-06-04 安徽万和制药有限公司 一种高效合成三氯蔗糖的方法
CN102942599B (zh) * 2012-11-28 2015-08-26 湖北益泰药业有限公司 一种蔗糖-6-乙酯的提纯方法

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4008218A (en) * 1972-08-25 1977-02-15 Meiji Seiki Kaisha, Ltd. 1-N-((S)-α-substituted-ω-aminoacyl)-neamine or -ribostamycin and the production thereof
US4117224A (en) * 1974-10-15 1978-09-26 Tate & Lyle Limited Preparation of sucrose 6,6'-dichloro hexa-acetate
DE2962239D1 (en) * 1978-10-18 1982-04-01 Tate & Lyle Patent Holdings A method for the preparation of 2-chloro-2-deoxy saccharides and some 2-chloro-2-deoxy saccharides

Also Published As

Publication number Publication date
YU317080A (en) 1983-02-28
PT72208A (en) 1981-01-01
DK155946B (da) 1989-06-05
DK155946C (da) 1989-10-23
YU41010B (en) 1986-10-31
NZ195891A (en) 1982-12-07
AU532217B2 (en) 1983-09-22
GR72482B (pt) 1983-11-14
PH16877A (en) 1984-04-02
NO149389B (no) 1984-01-02
AU6554380A (en) 1981-06-25
IL61763A0 (en) 1981-01-30
FI803982L (fi) 1981-06-21
EP0031651A1 (en) 1981-07-08
NO803851L (no) 1981-06-22
FI68403C (fi) 1985-09-10
EP0031651B1 (en) 1983-03-23
DK546080A (da) 1981-06-21
US4362869A (en) 1982-12-07
FI68403B (fi) 1985-05-31
DE3062467D1 (en) 1983-04-28
SU1176844A3 (ru) 1985-08-30
CA1152983A (en) 1983-08-30
IL61763A (en) 1984-10-31
NO149389C (no) 1984-04-11

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