PH12019500606B1 - Improved solder and method for producing high purity lead - Google Patents
Improved solder and method for producing high purity leadInfo
- Publication number
- PH12019500606B1 PH12019500606B1 PH1/2019/500606A PH12019500606A PH12019500606B1 PH 12019500606 B1 PH12019500606 B1 PH 12019500606B1 PH 12019500606 A PH12019500606 A PH 12019500606A PH 12019500606 B1 PH12019500606 B1 PH 12019500606B1
- Authority
- PH
- Philippines
- Prior art keywords
- lead
- tin
- high purity
- producing high
- improved solder
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title 1
- 229910000679 solder Inorganic materials 0.000 title 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 abstract 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 abstract 2
- 229910052751 metal Inorganic materials 0.000 abstract 2
- 239000002184 metal Substances 0.000 abstract 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 abstract 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 1
- 239000005864 Sulphur Substances 0.000 abstract 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 229910052787 antimony Inorganic materials 0.000 abstract 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 239000011651 chromium Substances 0.000 abstract 1
- 229910052802 copper Inorganic materials 0.000 abstract 1
- 239000010949 copper Substances 0.000 abstract 1
- 238000001704 evaporation Methods 0.000 abstract 1
- 230000008020 evaporation Effects 0.000 abstract 1
- 229910052742 iron Inorganic materials 0.000 abstract 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 238000002203 pretreatment Methods 0.000 abstract 1
- 239000010936 titanium Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 abstract 1
- 229910052721 tungsten Inorganic materials 0.000 abstract 1
- 239000010937 tungsten Substances 0.000 abstract 1
- 238000005292 vacuum distillation Methods 0.000 abstract 1
- 229910052720 vanadium Inorganic materials 0.000 abstract 1
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 abstract 1
- 239000011701 zinc Substances 0.000 abstract 1
- 229910052725 zinc Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/04—Working-up slag
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/10—Vacuum distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/24—Selection of soldering or welding materials proper
- B23K35/26—Selection of soldering or welding materials proper with the principal constituent melting at less than 400 degrees C
- B23K35/268—Pb as the principal constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B13/00—Obtaining lead
- C22B13/06—Refining
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B25/00—Obtaining tin
- C22B25/06—Obtaining tin from scrap, especially tin scrap
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/10—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals with refining or fluxing agents; Use of materials therefor, e.g. slagging or scorifying agents
- C22B9/106—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals with refining or fluxing agents; Use of materials therefor, e.g. slagging or scorifying agents the refining being obtained by intimately mixing the molten metal with a molten salt or slag
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C11/00—Alloys based on lead
- C22C11/06—Alloys based on lead with tin as the next major constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C11/00—Alloys based on lead
- C22C11/08—Alloys based on lead with antimony or bismuth as the next major constituent
- C22C11/10—Alloys based on lead with antimony or bismuth as the next major constituent with tin
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Conductive Materials (AREA)
- Arc Welding In General (AREA)
Abstract
Disclosed is a metal mixture composition containing lead and tin, and comprising by weight at least 10% tin and 45% lead, at least 90% of tin and lead together, more lead than tin, from 1-5000 ppm of copper, at least 0.42% antimony and at least 0.0001%wt of sulphur, at most 0.1% of the total of chromium, manganese, vanadium, titanium and tungsten, and at most 0.1 % of each one of aluminium, nickel, iron and zinc. Disclosed is also a process comprising a pre-treatment step for producing this metal mixture composition, followed by a vacuum distillation step wherein lead is removed by evaporation and a bottom stream is obtained comprising at least 0.6%wt of lead.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP16190907 | 2016-09-27 | ||
| PCT/EP2017/074393 WO2018060202A1 (en) | 2016-09-27 | 2017-09-26 | Improved solder and method for producing high purity lead |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PH12019500606A1 PH12019500606A1 (en) | 2019-06-03 |
| PH12019500606B1 true PH12019500606B1 (en) | 2023-09-08 |
Family
ID=57018022
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PH1/2019/500606A PH12019500606B1 (en) | 2016-09-27 | 2017-09-26 | Improved solder and method for producing high purity lead |
Country Status (13)
| Country | Link |
|---|---|
| US (2) | US11839938B2 (en) |
| EP (1) | EP3519599A1 (en) |
| JP (1) | JP7123912B2 (en) |
| CN (1) | CN109923225B (en) |
| BE (1) | BE1024606B1 (en) |
| BR (1) | BR112019005833B1 (en) |
| CA (1) | CA3037611A1 (en) |
| MX (1) | MX2019003330A (en) |
| MY (1) | MY193399A (en) |
| PE (1) | PE20191162A1 (en) |
| PH (1) | PH12019500606B1 (en) |
| RU (1) | RU2753365C2 (en) |
| WO (1) | WO2018060202A1 (en) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102355322B1 (en) | 2017-04-10 | 2022-01-25 | 메탈로 벨지움 | Improved Method for Manufacturing Crude Solder |
| BE1025771B1 (en) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Improved copper production method |
| BE1025772B1 (en) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Improvement in copper / tin / lead production |
| BE1025770B1 (en) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Improved pyrorefining process |
| BE1025775B1 (en) | 2017-12-14 | 2019-07-11 | Metallo Belgium | Improved soldering production method |
| BE1025769B1 (en) | 2017-12-14 | 2019-07-08 | Metallo Belgium | Improved pyrometallurgical process |
| CA3126515A1 (en) * | 2019-01-30 | 2020-08-06 | Metallo Belgium | Improved method for producing high purity lead |
| MY201404A (en) | 2019-01-30 | 2024-02-21 | Metallo Belgium | Improved tin production, which includes a composition comprising tin, lead, silver and antimony |
| CN113366130B (en) * | 2019-01-30 | 2023-11-28 | 梅塔洛比利时公司 | Improved co-production of lead and tin products |
| CN110919233B (en) * | 2019-11-15 | 2021-06-04 | 东莞市输变电工程公司 | Welding flux, preparation method thereof and ignition agent |
| EP4061972B1 (en) | 2019-11-22 | 2023-10-11 | Aurubis Beerse | Improved copper smelting process |
| CN111607708B (en) * | 2020-07-14 | 2022-02-11 | 湖南金马冶金技术开发有限公司 | Continuous vacuum distillation dearsenification process and system for high-arsenic alloy |
| CN113528846A (en) * | 2021-06-18 | 2021-10-22 | 广西壮族自治区环境保护科学研究院 | Treatment method for resource utilization of arsenic-containing waste residues |
| CN115852167B (en) * | 2022-11-14 | 2025-06-06 | 昆明理工大学 | An environmentally friendly pyrometallurgical refining process for crude tin |
| CN116100187B (en) * | 2022-12-16 | 2024-07-23 | 无锡市斯威克科技有限公司 | Low-melting-point ternary alloy solder, ultralow-temperature solder strip, and preparation methods and applications thereof |
| WO2025041020A1 (en) * | 2023-08-21 | 2025-02-27 | Attero Recycling Pvt. Ltd. | A method for recovering metal values from solder dross |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3188199A (en) | 1962-06-25 | 1965-06-08 | Du Pont | Process for recovering lead from by-product lead materials |
| AT251301B (en) | 1962-09-27 | 1966-12-27 | Nat Smelting Co Ltd | Process for refining impure zinc |
| JPS5476461A (en) * | 1977-11-30 | 1979-06-19 | Nippon Almit Kk | Solder alloy for bonding capacitor end |
| US4153451A (en) | 1978-05-01 | 1979-05-08 | Ethyl Corporation | Lead recovery and waste disposal process |
| JPS5518505A (en) * | 1978-07-21 | 1980-02-08 | Senjiyu Kinzoku Kogyo Kk | Soldering alloy for attaching silver electrode leading wire |
| US4487638A (en) * | 1982-11-24 | 1984-12-11 | Burroughs Corporation | Semiconductor die-attach technique and composition therefor |
| CN1012046B (en) * | 1987-01-07 | 1991-03-20 | 天台县焊接材料厂 | Rare earth tin-lead solder |
| CN1104950A (en) * | 1993-10-04 | 1995-07-12 | 成都市焊料厂 | Low tin high efficient welding material |
| JPH07299584A (en) | 1994-05-02 | 1995-11-14 | Nippon Bell Parts Kk | Superplastic solder |
| JP3045453B2 (en) * | 1994-06-13 | 2000-05-29 | 日本アルミット株式会社 | High strength solder alloy |
| RU2114200C1 (en) | 1996-12-03 | 1998-06-27 | Институт металлургии Уральского отделения РАН | Method for processing lead wastes containing antimony, tin and copper |
| JP2002153990A (en) * | 2000-11-21 | 2002-05-28 | Senju Metal Ind Co Ltd | Alloy for solder ball |
| CN100566904C (en) | 2005-07-21 | 2009-12-09 | 沈阳黎明航空发动机(集团)有限责任公司 | A kind of inner and outer brazing process method of target material for coating |
| CN101570826A (en) | 2009-06-08 | 2009-11-04 | 昆明鼎邦科技有限公司 | Method for multilevel vacuum distilling and separating tin-lead alloy |
| CN101696475B (en) | 2009-10-29 | 2012-08-01 | 昆明理工大学 | Method for separating ternary alloy of lead, tin and stibium |
| CN102352443B (en) | 2011-10-31 | 2013-06-05 | 太仓市南仓金属材料有限公司 | Method for producing zinc sulfate heptahydrate, crude tin and crude lead by using tin smelting dust |
| CN102534249B (en) | 2012-02-22 | 2013-03-06 | 郴州丰越环保科技股份有限公司 | Method for refining tin from high-silver crude tin |
| RU2496894C1 (en) | 2012-06-14 | 2013-10-27 | Ирина Анатольевна Бобкова | Copper refining method |
| CN104141152A (en) | 2014-07-28 | 2014-11-12 | 蒙自矿冶有限责任公司 | Method for recycling tin from lead bullion |
| CN104593614A (en) | 2014-12-30 | 2015-05-06 | 郴州丰越环保科技有限公司 | Method for efficiently separating lead, tin and antimony from lead-tin-antimony ternary alloy of high antimony content |
| CN104651626A (en) | 2015-02-05 | 2015-05-27 | 昆明鼎邦科技有限公司 | Method for separating tin from tin-lead-stibium-arsenic alloy by vacuum distillation |
-
2017
- 2017-09-26 MX MX2019003330A patent/MX2019003330A/en unknown
- 2017-09-26 CA CA3037611A patent/CA3037611A1/en active Pending
- 2017-09-26 PH PH1/2019/500606A patent/PH12019500606B1/en unknown
- 2017-09-26 BE BE2017/5681A patent/BE1024606B1/en active IP Right Grant
- 2017-09-26 JP JP2019515894A patent/JP7123912B2/en active Active
- 2017-09-26 CN CN201780058893.7A patent/CN109923225B/en active Active
- 2017-09-26 EP EP17777863.6A patent/EP3519599A1/en active Pending
- 2017-09-26 PE PE2019000703A patent/PE20191162A1/en unknown
- 2017-09-26 RU RU2019110422A patent/RU2753365C2/en active
- 2017-09-26 US US16/335,892 patent/US11839938B2/en active Active
- 2017-09-26 MY MYPI2019001494A patent/MY193399A/en unknown
- 2017-09-26 BR BR112019005833-8A patent/BR112019005833B1/en active IP Right Grant
- 2017-09-26 WO PCT/EP2017/074393 patent/WO2018060202A1/en not_active Ceased
-
2022
- 2022-03-17 US US17/697,649 patent/US11992903B2/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| JP2019536892A (en) | 2019-12-19 |
| PH12019500606A1 (en) | 2019-06-03 |
| MX2019003330A (en) | 2019-09-27 |
| WO2018060202A1 (en) | 2018-04-05 |
| RU2753365C2 (en) | 2021-08-13 |
| CA3037611A1 (en) | 2018-04-05 |
| US11992903B2 (en) | 2024-05-28 |
| CN109923225A (en) | 2019-06-21 |
| PE20191162A1 (en) | 2019-09-09 |
| BE1024606B1 (en) | 2018-04-25 |
| CN109923225B (en) | 2021-08-10 |
| US20220203482A1 (en) | 2022-06-30 |
| EP3519599A1 (en) | 2019-08-07 |
| US20200023473A1 (en) | 2020-01-23 |
| RU2019110422A (en) | 2020-10-29 |
| MY193399A (en) | 2022-10-11 |
| BR112019005833A2 (en) | 2019-06-18 |
| BE1024606A1 (en) | 2018-04-19 |
| US11839938B2 (en) | 2023-12-12 |
| RU2019110422A3 (en) | 2020-11-30 |
| BR112019005833B1 (en) | 2022-06-07 |
| JP7123912B2 (en) | 2022-08-23 |
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