KR20190087863A - Composition for washing hair and scalp to prevent hair losing and to promote hair growth and method for preparing the same - Google Patents

Abstract

The present invention relates to a hair and scalp cleansing composition which is excellent in scalp moisturizing, hair loss prevention and hair growth promoting function, including an extract of a natural medicinal plant exhibiting hair loss preventing function, copexil and a hydrolized sponge, ≪ / RTI >

Description

BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a composition for cleansing hair and scalp,

The present invention relates to a hair and scalp cleansing composition having a function of preventing hair loss and promoting hair growth, and a method of manufacturing the hair and scalp.

Typically, the hair of a human body protects the human body from external shocks such as ultraviolet rays, cold winds, and the like, and protects the human body from arsenic (As), mercury (Hg), zinc (Zn) It absorbs unnecessary heavy metals in the same body and discharges them to the outside of the body.

Ordinary adults have about 100,000 to 150,000 hairs, and each hair grows and degenerates through processes including anagen, catagen, and telogen, Hair hair maintains a lifespan of about 1,000 days, which normally causes 50-100 hairs per day to fall off normally, and new hairs are produced in areas where hair is missing.

However, hair loss that does not result in new hair at the site of hair loss due to unbalanced eating habits, excessive drinking and smoking, drug abuse, sleep deprivation, excessive stress, childbirth, menopausal disorders, frequent perm and dyeing, hormone imbalance In order to prevent hair loss as described above, there has been a tendency to use a hair removing agent made of a natural extract which is not harmful to the human body, a skin external preparation for preventing or alleviating hair loss by washing waste products of the scalp and supplying artificial nutrients , And natural detergents (shampoos).

For example, Korean Patent No. 10-1263181 discloses a herbal medicine extract of a mixture of herbal medicines containing a certain ratio of Hassuo, Ginseng, Pine Needle, Angelicae radix, Medicinal wormwood, The present invention relates to a scalp care composition for promoting hair growth and preventing hair loss.

As another example, Korean Patent No. 10-0805692 discloses a shampoo for preventing hair loss, which comprises a herbal extract, which is a mixed hot-water extract of Baekjiae, Chuncheon, Youngryungbyeol, Tangguk, There is a bar.

However, most of the hair loss is due to the action of male hormone androgen (androgen) type of hair loss caused by the hair loss method to prevent dihydrotestosterone (DHT) is known to be the most effective and is currently the medical DHT production inhibitors that have been proven to be effective against hair growth are only hair growth promoters such as finasteride, dutasteride, minoxidil and the like. Such compositions derived from natural materials can create a positive environment for maintaining hair health There is a problem that it is difficult to expect hair growth, and it is known that the hair growth promoting agents cause various side effects. Therefore, it is necessary to study a new composition or method that can complement the above.

Korean Patent Registration No. 10-1263181 (Publication Date: 2013.05.10) Korean Patent No. 10-0805692 (Publication Date: Feb. 21, 2008)

Disclosure of Invention Technical Problem [8] Accordingly, the present invention has been made in an effort to solve the problems of the prior art as described above, and it is an object of the present invention to provide a cosmetic composition which is free from side effects and contains safflower extract and copexil as an active ingredient, The present invention provides a composition for cleansing hair and scalp, which is excellent in scalp moisturizing, hair loss prevention and hair growth promoting function, and a method for producing the same.

In order to accomplish the above object, the present invention provides a medicinal plant extract and a 2,4-diamino pyrimidine-3-oxide extracted from medicinal plants including Hanshiku, 3-oxide, Kopexil) as an active ingredient.

According to one embodiment of the present invention, the hair and scalp cleansing composition comprises 1 to 10 parts by weight of the medicinal plant extract and 0.1 to 10 parts by weight of the 2,4-diaminopyrimidine-3-oxide, based on 100 parts by weight of the composition. And may further comprise 0.5 to 5 parts by weight of the hydrolized sponge powder.

According to one embodiment of the present invention, the composition for cleaning hair and scalp may contain at least one selected from the group consisting of herbal extracts, mushroom extracts, vitamins, moisturizers, surfactants, foam stabilizers, pH adjusters, pearlizers, preservatives, And at least one additive selected from the group consisting of the following.

In addition, the present invention provides a method for producing hair and scalp cleansing composition as described above, comprising the steps of: (a) feeding a mixture of medicinal plants containing hanchikcho, hansuo, and hyphae and water to a vacuum low temperature extractor, To produce a medicinal plant extract; (b) supplying purified water and Polyquaternium-10 to a mixing tank and heating the mixture to a temperature of 60 to 80 占 폚 to prepare a first mixture; (c) heating the first mixture to a temperature of 60 to 80 ° C and adding disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose, cocoamidoproply betaine, and cocoyl monoethanolamine to prepare a second mixture, respectively; (d) heating the second mixture to a temperature of 40 to 60 DEG C to produce a third mixture by feeding PEG-120 methyl glucose dioleate; (e) heating the third mixture to a temperature of 30 to 50 DEG C and adding glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt ), Linoleamidopropyl PG-dimonium chloride phosphate, and the above-mentioned medicinal plant extract to prepare a fourth mixture; And (f) preparing a composition for cleaning hair and scalp by sequentially mixing a fourth mixture with a grapefruit extract, sodium benzoate, and a perfume to prepare a hair and scalp cleansing composition do.

According to an embodiment of the present invention, the step (e) may further include the step of supplying the hydrolyzed sponge to the fourth mixture after the fourth mixture is prepared.

The composition for cleaning hair and scalp according to the present invention is characterized in that it comprises a medicinal plant extract exhibiting excellent hair-dressing-preventing performance such as a herb medicine, a hansoo, a hyacinth, etc. promoting blood circulation and scalp regeneration, and Kopexil, And thus has excellent hair growth promoting and hair loss prevention performance.

In addition, the composition according to the present invention further comprises a hydrolysed sponge capable of penetrating the active ingredient to the deep region of the scalp, thereby exhibiting excellent moisturizing effect, Can be improved.

1 is a conceptual diagram schematically illustrating a high-speed vacuum low-temperature extraction system used for producing a medicinal plant extract according to an embodiment of the present invention.
Fig. 2 shows the result of measuring the rate of change of moisture on the scalp during 6 hours after washing the hair and scalp with the shampoo composition prepared by the method according to Example 1, Example 2, and Comparative Example 1. Fig.

Hereinafter, the present invention will be described in detail.

The present invention relates to a pharmaceutical composition comprising a medicinal plant extract and 2,4-diamino pyrimidine-3-oxide (Kopexil) extracted from a medicinal plant including Hansuccho, A hair, and a scalp.

The medicinal plant extract may be an extract obtained from a medicinal plant including herbaceous basidiomycetes, herbaceous moths and hyacinthae which exhibits an effect of promoting hair growth and preventing hair loss. In addition to the above-mentioned medicinal plants, It may be constituted to further include extracts extracted from various medicinal plants.

In addition, the medicinal plant extract may be extracted by using a mixture of medicinal plants such as Hanshikoshi, Hassuo, and Hwasoji by various methods such as hot water extraction, ethanol extraction, reflux extraction, heating and pressure extraction, Can be used.

Preferably, the medicinal plant extract is obtained by supplying the medicinal plant mixture to a high-speed vacuum low-temperature extraction apparatus to which a circulation-type steam cooling method is applied, extracting the medicinal plant mixture at a low temperature by a vacuum distillation method to prevent breakage of the active ingredient, May be used.

Among the medicinal plants, Eclipta prostrata L. is an annual plant of Asteraceae and contains saponin, nicotine, tannin, vitamin A, ecliptine, thiophene thiophene compound, etc. It is suitable for hair loss due to the upper heat of the young person and has a good property. It is excellent in hemostatic effect, and has antimicrobial, anti-inflammatory, anti-fungal effect and immune strengthening effect And the feet are made black, and hair loss prevention and hair growth promoting effect are effective.

The above-mentioned Pleuropterus multiflorus Turcz is a perennial plant having a round root root and having a vine nature, and the dewatering largely consists of Polygonum multiflorum Thunberg and Cynan chum wilfordii Hemsley ), which is mainly grown in our country, is a white sage. The above-mentioned diaphoresis contains a large amount of anthraquinone components such as chrysophanol, emodin, rhein and physcion, and lecithin, To promote blood circulation and blood supply to the scalp, to promote healthy hair, and to moisturize the skin.

Thuja orientalis L. is a medicinal herb prepared by drying the raw leaves obtained from a spruce tree, such as aromadendrin, quercetin, amenthoflavone, myricetin, hinokiflavone hinokiflavone, and the like, which are known to exhibit an effect of promoting the growth of hair and making gray hair black.

In addition, the composition for cleaning hair and scalp according to the present invention may contain the medicinal plant extract in a proportion of 1 to 10 parts by weight based on 100 parts by weight of the composition. When the content of the medicinal plant extract is less than 1 part by weight, The induction effect is insignificant and it is difficult to expect further improvement of the physical properties to exceed 10 parts by weight and the stability of the composition to be described later is low and the phase separation may be induced when stored for a long period of time.

In particular, the medicinal plant extract is preferably constituted so as to contain the medicinal plants of the present invention in a weight ratio of 2: 1: 1, good.

More preferably, the composition may comprise 6 to 9 parts by weight of a medicinal plant extract extracted from a mixture of medicinal plants containing 2: 1: 1, respectively, of Hanshikoshi, Hansuo and Hwasae.

Also, the 2,4-diamino pyrimidine-3-oxide (Kopexil) contained in the composition for cleaning hair and scalp according to the present invention can prevent hair loss As a derivative of minoxidil, a derivative of minoxidil, which is a kind of DHT production inhibitor, hair growth can be promoted by promoting the hair cycle from the resting period to the growing period by expanding blood vessels, and hair loss can be prevented, hair loss can be prevented, There is an effect of curing.

In the composition according to the present invention, it is preferable that the 2,4-diaminopyrimidine-3-oxide is contained in a proportion of 0.1 to 10 parts by weight, and the 2,4-diaminopyrimidine- When the content is less than 0.1 part by weight, it is difficult to expect a synergistic effect of blood flow enhancement due to vasodilation and it is difficult to realize hair growth promoting effect. When the content exceeds 10 parts by weight, it is difficult to expect further improvement of physical properties, , And more preferably, the composition may include 2,4-diaminopyrimidine-3-oxide in a ratio of 1 part by weight.

Meanwhile, the composition for cleaning hair and scalp according to the present invention may further comprise 0.5 to 5 parts by weight of hydrolyzed sponge (spicule) powder.

The hydrolyzed sponge is a bone tissue extracted from the sea surface, and a large number of minute pins are formed on the surface. Thus, various active ingredients contained in the medicinal plant extract and 2,4-diaminopyrimidine- Helps to penetrate the absorbed active ingredient to the deep area of the scalp and promotes blood circulation, promotes collagen production, eliminates keratin on the scalp and eliminates unnecessary skin fat to promote regeneration of scalp cells It is possible to exhibit an effect of increasing moisture and moisture.

In particular, the hydrolyzed sponge is generally prepared by a chemical purification process using an acid or a base, but the hydrolyzed sponge added to the composition according to the present invention is preferably a protease M Proteolytic enzymes such as protease A, protamex, neutrase, flavorzyme, and alcalase can be used as the proteolytic enzyme. have.

Specifically, the hydrolyzed sponge is prepared by drying and crushing the sponge animal, mixing the obtained sponge powder with distilled water to prepare a sponge mixture, adding protease M, protease A, Protease such as protease, protamex, neutrase, flavorzyme, alcalase and the like to decompose the protein and then heat the proteinase to inactivate the protease, May be used.

The hydrolized sponge may be powder having an average particle size of 0.01 to 2.0 mm. Preferably, the powder is pulverized to have a size of 0.1 to 0.5 mm. The hydrolized sponge When the average particle size of the sponge is less than 0.1 mm, the effect of the stimulation of the scalp is minimal, the amount of the active ingredient is reduced, and when the average particle size of the hydrolyzed sponge exceeds 0.5 mm, the scalp may be over stimulated. More preferably, powder particles having a size of 0.1 to 0.2 mm can be used.

The hydrolyzed sponge may be contained in a proportion of 0.5 to 5 parts by weight based on the total weight of the composition. When the content of the hydrolyzed sponge is less than 0.5 part by weight, the effect of stimulating the scalp is insignificant, It is difficult to completely remove the spucule in cleaning and further improvement of physical properties is difficult to be expected. More preferably, the composition may contain the hydrolyzed sponge in a ratio of 1 part by weight.

Furthermore, the hair and scalp cleansing compositions according to the present invention can be used for the hair and scalp cleansing composition of the present invention, which comprises a herbal extract, a mushroom extract, vitamins, a moisturizer, a surfactant, a foaming agent, a conditioning agent, a pH adjusting agent, a pearlizing agent, an antiseptic, So as to be used for hair and scalp cleaning.

The herbal extract is excellent in improving scalp diseases such as hair loss, seborrheic dermatitis, dandruff and the like, and also contains a natural herbal extract as an active ingredient to provide an excellent skin soothing effect and a unique aroma, It can help relieve stress, and it can also serve as a fragrance because it can play a role of imparting fragrance.

The herbal extracts may be exemplified by peppermint extract, lavender extract, basil extract, marshmallow extract, chamomile extract, tea tree extract, fennel extract or a mixture thereof.

Preferably, the composition according to the present invention can mix the herbal extract or the fragrance at a ratio of preferably 0.1 to 5 parts by weight, and when mixed at less than 0.1 part by weight, it is difficult to give a satisfactory fragrance and more than 5 parts by weight It is possible to give an excessively strong fragrance.

The mushroom extract may contain a large amount of vegetable vitamin D such as ergosterol or the like, thereby providing a large amount of vitamin D to the composition.

In particular, the mushroom extract is prepared by irradiating raw materials of mushroom with ultraviolet light to conduct a process of extracting mushrooms to produce a mushroom work product in which the content of vitamin D contained in the mushroom is significantly increased, and the produced mushroom work product is mixed with ethanol and citric acid Extracting ethanol with a solvent and extracting vitamin D with high yield can be used.

For example, the mushroom extract is prepared by drying shiitake mushroom under the condition of ultraviolet ray irradiation, powdering the dried shiitake mushroom, and concentrating the mushroom ethanol extract extracted from the mushroom powder with an extracting process such as ethanol, To 30 mg / L. The mushroom extract may be used to prepare a composition having a significantly increased vitamin D content. The mushroom extract may be contained in the composition in a proportion of preferably 0.5 to 5 parts by weight, more preferably 1 part by weight, so as to provide vitamin D to the scalp to impart the hair-loss preventing effect.

In addition, the composition according to the present invention may further comprise panthenol, glycerol, and the like as a moisturizing agent to further impart moisture.

In particular, the panthenol is a precursor substance which is converted into vitamin B5, penetrates deeply into the scalp and hair, can act as a carrier that effectively transfers various active ingredients, has excellent ability to bind moisture, It can be converted to nitric acid to produce vitamin B5.

Therefore, the above-mentioned panthenol effectively permeates the scalp, thereby preventing hair loss and easily inducing vasodilation. Further, since the panthenol exhibits a strong binding property with moisture, it penetrates into the hair follicle and hair follicle, And the like.

The panthenol is preferably mixed at a ratio of 0.5 to 2 parts by weight. When the content of the panthenol is less than 0.5 part by weight, it is difficult to expect a sufficient effect. When the content of the panthenol is more than 2 parts by weight, Hard. More preferably, the panthenol may be contained at a ratio of 1 part by weight, and D-panthenol is preferably used.

The surfactant and foaming agent serve to promote the formation of bubbles in the composition and to impart additional detergency, and may include an anionic surfactant, an amphoteric surfactant, or a mixture thereof, a surfactant obtained from a natural material, A foaming agent can be preferably used.

In particular, the foaming agent is selected from the group consisting of disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose, cocoamidoproply betaine, , Cocoyl monoethanolamine, and the like.

The composition according to the present invention may be constituted so as to include the foaming agent in a proportion of preferably 50 to 90 parts by weight, more preferably, the disodium laureth sulfolactinate, alkyl polyglycoside, sodium cocoyl amino acid -Fructose, cocoamidopropyl betaine, and cocoyl monoethanol amine in a ratio of 80 parts by weight can be used.

In addition, the viscosity controlling agent may control the viscosity of the composition and may be exemplified by PEG-120 methyl glucose dioleate (PEG-120 methyl glucose dioleate).

In addition, the water softening agent reacts with various metal ions present in the scalp or hair to inactivate it, and ethylenediamine tetraacetic acid (EDTA) disodium salt is a representative example. The disodium ethylenediaminetetraacetic acid disodium salt may be mixed in a proportion of 0.05 to 5 parts by weight, preferably 0.1 part by weight.

Wherein the conditioning agent provides styling and setting by applying an adhesive force to the hair, wherein the conditioning agent is selected from the group consisting of linoleamidopropyl PG-dimonium chloride phosphate and Polyquaternium-10, As a representative example.

In particular, the linoleamidopropyl diphenyl-dimonium chloride phosphate may act as an emulsifier, a hair conditioning agent, an antistatic agent, etc., and may be mixed in a proportion of 0.1 to 10 parts by weight, based on the total weight of the composition , And more preferably 0.5 parts by weight.

The polyquaternium-10 is a cationic polymer obtained by adding diglycidyltrimethylammonium chloride or 3-chloro-2-hydroxypropyltrimethylammonium chloride to hydroxyethylcellulose, as a stabilizer, a film-forming agent, An antistatic agent and the like, preferably 0.1 to 5 parts by weight, and more preferably 0.5 parts by weight.

The antimicrobial agent not only imparts antimicrobial properties to hair and scalp but also contributes to long-term stability of the composition, and may be exemplified by grapefruit extract, sodium benzoate, and the like.

Preferably, the antimicrobial agent may be mixed in a ratio of 0.1 to 5 parts by weight, more preferably 0.4 part by weight of a mixture of the grapefruit extract and sodium benzoate in a weight ratio of 1: 1 have.

The hair and scalp cleansing composition according to the present invention as described above can be used as a medicinal plant extract exhibiting excellent hair loss prevention performance such as hanwoncho, hansooo, myeonbyeop, etc. which promotes blood circulation and scalp regeneration, and Kopexil ) As an active ingredient and can penetrate the active ingredient to the deep region of the scalp and has a hydrolized sponge that imparts excellent moisturizing effect, and is excellent in moisturizing, promoting hair growth and preventing hair loss.

According to a preferred embodiment of the present invention, the hair and scalp cleansing compositions according to the present invention are prepared by extracting a mixture containing the above-mentioned Hanshincho, Hwaseo and Hwasoji at a weight ratio of 2: 1: 1, respectively, A composition having a shampoo formulation for hair and scalp washing can be prepared using a medicinal plant extract, a hydrolyzed sponge pretreated with a protein hydrolyzing enzyme, and a mushroom extract having a high content of vitamin D.

Specifically, the composition for cleaning hair and scalp was prepared by mixing 7 parts by weight of a medicinal plant extract prepared by the above method, 2,4-diamino pyrimidine-3-oxide, Kopexil ), 1 part by weight of hydrolyzed sponge, 1 part by weight of mushroom extract, 1 part by weight of panthenol, 35 parts by weight of disodium laureth sulfosuccinate, 10 parts by weight of alkylpolyglycosides, 10 parts by weight of sodium cocoyl amino acid fructose, 20 parts by weight of cocoamidoproply betaine, 10 parts by weight of cocoyl monoethanolamine, , 1 part by weight of PEG-120 methyl glucose dioleate, 0.5 part by weight of polyquaternium-10, 1 part by weight of glycerin, 1 part by weight of salicylic acid ), 0.1 part by weight of ethyl 0.1 part by weight of ethylenediamine tetra acetic acid (EDTA) disodium salt, 0.5 part by weight of linoleamidopropyl PG-dimonium chloride phosphate, 0.2 part by weight of grapefruit extract, 0.2 parts by weight of sodium benzoate, 0.5 parts by weight of fragrance, and the remaining purified water, respectively, to prepare a composition having a shampoo formulation.

The shampoo composition prepared as described above is excellent in hair loss prevention and hair growth promoting function, and has not only efficacy such as washing power, moisturizing effect but also excellent formulation stability and can be easily used for a long time for hair and scalp washing .

The present invention also provides a method for preparing a hair and scalp cleaning composition as described above.

The method for producing hair and scalp cleansing composition according to the present invention comprises the steps of: (a) supplying a mixture of medicinal plants including Hanshikoshi, Hashuo and Hwasobyeo and water to a vacuum low temperature extractor, and extracting the medicinal plant extract by vacuum distillation ; (b) supplying purified water and Polyquaternium-10 to a mixing tank and heating the mixture to a temperature of 60 to 80 占 폚 to prepare a first mixture; (c) heating the first mixture to a temperature of 60 to 80 ° C and adding disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose, cocoamidoproply betaine, and cocoyl monoethanolamine to prepare a second mixture, respectively; (d) heating the second mixture to a temperature of 40 to 60 DEG C to produce a third mixture by feeding PEG-120 methyl glucose dioleate; (e) heating the third mixture to a temperature of 30 to 50 DEG C and adding glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt ), Linoleamidopropyl PG-dimonium chloride phosphate, and the above-mentioned medicinal plant extract to prepare a fourth mixture; And (f) sequentially mixing a fourth mixture with a grapefruit extract, sodium benzoate, and a perfume to prepare a composition for hair and scalp cleansing, each of the raw materials comprising The composition for hair and scalp cleansing can be prepared.

In the step (a), a medicinal plant mixture including Hanshikoshi, Hassuo, and Hyacinth leaves and water are supplied to a vacuum low-temperature extractor and extracted by a vacuum distillation method to produce a medicinal plant extract.

The medicinal plant extract may be prepared by various conventional methods for producing an extract from a plant such as hot water extraction, ethanol extraction, reflux extraction, etc. Preferably, the extract is a vacuum low temperature extraction method using a circulating vapor cooling method, Can be constructed so as to produce a medicinal plant extract containing the active ingredient at a high yield while preventing destruction of the active ingredient.

For this purpose, the vacuum low-temperature extraction method can produce a medicinal plant extract through a vacuum distillation method using a high-speed vacuum low-temperature extraction system as described below to shorten the extraction time and minimize the destruction of the active ingredient.

1 is a conceptual diagram showing a high-speed vacuum low-temperature extraction system 10 used for producing a medicinal plant extract according to the present invention.

Referring to FIG. 1, the high-speed vacuum low-temperature extraction system 10 includes a housing space for supporting medicinal plants and water, and a heating unit 110 at a lower side thereof for heating the mixture of the medicinal plants and water And a first discharging part 150 provided at one side of the upper part to discharge the steam formed by heating and discharge the medicinal plant extract formed at the other side of the lower part, A second discharge unit 210 connected to the steam outlet 130 formed at one side of the upper side of the vacuum chamber 100 to cool the steam generated in the vacuum chamber 100 and to discharge the cooled steam, A first cooler 200 provided with a third discharge portion 230 for discharging condensed water formed in the cooled steam, a second cooler 200 connected to the first cooler 200 and connected to the first cooler 200 via the first cooler 200, Cooled by a water-cooled method, and a circulation pump (310) A second cooler 300 for transferring a vapor to the first cooler 200 and a storage space for storing distilled water therein. The first cooler 200 is connected to the third discharge unit 230, A distilled water storage tank 400 having a fourth discharge unit 410 for collecting condensed water generated in the distilled water storage tank 400 and discharging the distilled water, A vacuum pump 430 having a water separating filter 420 for forming a vacuum in the receiving space of the vacuum chamber 100 connected to the first cooler 200 and discharging the water introduced from the distilled water storage tank 400, And an extract storage tank 500 connected to the first discharge unit 150 and the fourth discharge unit 410 to store the medicinal plant extract and the distilled water discharged from the vacuum tank 100 and the distilled water storage tank 400 Structure.

The vacuum low-temperature extractor as described above can produce a medicinal plant extract by a vacuum distillation method, thereby shortening the extraction time and minimizing destruction of the active ingredient.

More specifically, the vacuum chamber 100 may have a receiving space formed therein to receive the medicinal plant and water, to seal the receiving space to form a vacuum-depressed space, (110) is provided to heat a mixture of the medicinal plant and water to produce a medicinal plant extract. The steam outflow part 130 is formed on one side of the upper part of the vacuum chamber 100 to allow the steam generated during the production of the medicinal plant extract to flow out to the first cooler 200 through heating, A first discharge unit 150 for discharging the plant extract is provided to discharge the medicinal plant extract to the extract storage tank 500 to be described later. In addition, the vacuum chamber 100 may include a discharge unit 170 capable of discharging the generated steam to the outside.

The first cooler 200 may be connected to the steam outlet 130 and may receive the steam discharged from the vacuum tank 100 to cool the first cooler 200. One side of the first cooler 200 may be connected to a distilled water storage tank 400, The condensed water formed by condensing the steam in the cooler 200 can be recovered to the distilled water storage tank 400 so that the structure for recovering the effective ingredient contained in the steam is formed, The extraction yield of the component can be maximized. In addition, the other side of the first cooler 200 may be connected to the second cooler 300 to transfer the vapor, which is first cooled in the first cooler 200, to the second cooler, And a circulation structure for cooling the hot air supplied from the vacuum tank 100 by receiving the steam cooled again by the heater 300 may be formed. To this end, the first cooler 200 may include a cooling compressor or a cooling fan to form a structure for cooling the steam in the vacuum chamber 100.

The second cooler 300 is connected to the first cooler 200 to receive the steam passing through the first cooler 200 to cool the steam again in a water-cooled manner, and the circulating pump 310 is provided, And the steam passing through the first cooler 300 may be transferred to the first cooler 200 so that the steam discharged from the vacuum tank 100 may be cooled. In addition, the second cooler 300 includes a cooling core 320 through which steam flows, and a cooling fan 330 provided outside the second cooler 300 so as to cool the water cooled cooling steam in the second cooler 300 again Can be configured.

The distilled water storage tank 400 connected to the other side of the first cooler 200 has an accommodation space for storing distilled water therein and is connected to the first cooler 200 to cool It is possible to form a structure for recovering the condensed water formed by the steam which is generated by the steam, thereby making it possible to form a structure for recovering the effective ingredient contained in the steam. In addition, a third discharge unit 410 for discharging the distilled water carrying the effective ingredient may be provided to discharge the distilled water carrying the effective ingredient into the extract storage tank 500 to be described later.

In particular, a vacuum pump 430 having a hydro-separation filter 420 for discharging water from the distilled water storage tank 400 is connected to one side of the distilled water storage tank 400 to reduce the distilled water storage tank 400 And the vacuum chamber 100 connected to the first cooler 200 may also be decompressed.

The extract storage tank 500 stores the medicinal plant extract and distilled water discharged from the vacuum tank 100 and the distilled water storage tank 400 by being connected to the first discharge unit 150 and the third discharge unit 410 And a fourth discharge part 510 is provided on one side to form a structure for discharging the medicinal plant extract carried on the inside.

Further, the vacuum tank 100, the first cooler 200, the second cooler 300, the distilled water storage tank 400, and the extract storage tank 500 are connected to each other by a connection pipe, And a structure for controlling the flow of steam, extract, and distilled water can be formed.

The high-speed vacuum low-temperature extraction system 10 as described above drives the heating means installed under the vacuum chamber 100 in a state in which the vacuum pressure continuously operates, thereby to extract the mixture of the medicinal plant and the water by hot water. The steam generated in the extraction process can be cooled by the first cooler 200 and the second cooler 300 to form a structure for recovering the effective ingredient.

The step (b) comprises the step of mixing the purified water and the polyquaternium 10 in a mixing tank to prepare a first mixture, wherein the purified water and the polyquaternium 10 are heated to a temperature of 60 to 80 캜 to completely dissolve the first mixture And preferably the purified water and the polyquaternium 10 are mixed and heated to a temperature of 70 캜 to prepare the first mixture.

The step (c) comprises sequentially supplying disodium laureth sulforocinate, alkyl polyglycoside, sodium cocoyl amino acid-fructose, cocoamidopropyl betaine and cocoyl monoethanolamine to the first mixture, The second mixture may be prepared by mixing at a temperature of 60 to 80 캜 in a heated state. Preferably, the second mixture may be prepared by heating at a temperature of 70 캜.

The step (d) may be performed by heating the second mixture to a temperature of 40 to 60 ° C and supplying a phage-120 methyl glucose diolate to produce a third mixture, preferably at a temperature of 50 ° C The third mixture can be prepared by heating.

Wherein step (e) comprises heating the third mixture to a temperature of 30 to 50 DEG C and adding glycerin, panthenol, salicylic acid, disodium ethylenediaminetetraacetate, linoleamidopropylpyi-dimonium chloride phosphate and the medicinal plant extract May be sequentially added to prepare a fourth mixture. Preferably, the fourth mixture may be prepared by heating at a temperature of 40 캜.

Further, in this step, it is possible to further comprise a step of supplying a hydrolized sponge to the fourth mixture after the fourth mixture is prepared, and a hydrolized sponge may be supplied to the fourth mixture And then reacted for a sufficient time to absorb the active ingredient.

In step (f), the composition for cleaning hair and scalp may be prepared by mixing the fourth mixture with a grapefruit extract, sodium benzoate, and a flavoring agent in sequence. Preferably, the composition is heated at a temperature of 40 ° C to prepare a composition Can be manufactured.

According to the method for preparing hair and scalp cleansing composition according to the present invention as described above, it is possible to prepare a composition that is stable without phase separation even when it is used for a long period of time by mixing the medicinal plant extract and various additives at specific temperature conditions, The compositions may be utilized in a variety of formulations, such as shampoos, conditioners, and the like, for hair and scalp washing.

Hereinafter, the present invention will be described in more detail with reference to examples.

The embodiments presented are only a concrete example of the present invention and are not intended to limit the scope of the present invention.

<Preparation Example> Preparation of medicinal plant extract

(Hwangcheon, Gyeongbuk, Yeongcheon, Daejeon-dong, Gyeongbuk, Yeongcheon, Gyeongbuk, Yeongju)

 In a high-speed vacuum low-temperature extractor equipped with a circulating-type steam cooling system, 500 g of Hansikucho, 250 g of Sasao, and 250 g of a lateral leaf were mixed and supplied at a weight ratio of 2: 1: 1, and 10 L of water was supplied to immerse the herbal medicine mixture , And kept at room temperature for about 12 hours to soften the herbal medicine mixture.

Then, the extraction process was carried out using a vacuum low-temperature extraction method in which a circulating-type steam cooling method was introduced using a vacuum low-temperature extractor as shown in FIG. 1 to produce a medicinal plant extract. The extract thus obtained was concentrated 10- The extract was prepared.

&Lt; Example 1 >

The medicinal plant extract prepared by the method according to Preparation Example was used and the extracts of grapefruit, fragrance, disodium laureth sulfosuccinate (LES / Miwon Company), alkylpolyglycosides (APG / Cocoamidopropyl betaine (Mitaine CA), cocoyl monoethanolamine (Cocoyl monoethanolamine), sodium cocoyl amino acid fructose (Oliveoel fruttoside / Kalichem italia, italy), cocoamidopropyl betaine (PEG-120 methyl glucose dioleate, DOE120 / Lubrizol), diaminopyrimidine oxide (Kopexil / Kumar), polyquaternium-10 (CME / Glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt), linoleic acid 1 part by weight of hydrolyzed sponge having an average particle size of 200 占 퐉 by protein hydrolysis treatment, 1 part by weight of shiitake mushroom extract (manufactured by Shimadzu Corporation), 1 part by weight of sodium dodecylbenzenesulfonate 20 mg / L) were mixed in the compositions shown in the following Table 1 to prepare a shampoo composition.

Specifically, purified water and polyquaternium 10 were fed into a batch batch and heated to 70 占 폚 and stirred sufficiently until completely dissolved. Then, disodium laurylsulfuronate, alkylpolyglycoside, sodium cocoyl amino acid-fructose, cocoamidopropyl betaine, and cocoyl monoethanol amine were sequentially fed and completely dissolved, and then diaminopyrimidine oxide To complete dissolution to prepare a mixture.

Thereafter, methyl glucoside diolate was added to the mixture and dissolved at a heating temperature of 50 ° C. After the heating temperature was lowered to 40 ° C, glycerin, panthenol, salicylic acid, ethylenediaminetetraacetic acid, -Dimonium chloride phosphate, a medicinal plant extract prepared by the method according to Preparation Example, and a mushroom extract were successively supplied and mixed. Thereafter, a hydrolized sponge having an average particle size of 200 占 퐉 was mixed , And grapefruit extract, sodium benzoate, and fragrance were finally supplied to prepare a shampoo composition.

&Lt; Example 2 >

A shampoo composition was prepared in the same manner as in Example 1 except that 4.9 parts by weight of a hydrolized sponge was used instead of purified water.

&Lt; Example 3 >

A shampoo composition was prepared in the same manner as in Example 1, except that 4.9 parts by weight of shiitake mushroom extract was mixed instead of purified water.

&Lt; Comparative Example 1 &

A shampoo composition was prepared in the same manner as in Example except that purified water was added instead of the hydrolized sponge.

&Lt; Comparative Example 2 &

A shampoo composition was prepared in the same manner as in Example except that 4.9 parts by weight of purified water was added instead of mushroom extract.

&Lt; Experimental Example 1 >

In order to confirm the effect of preventing the hair loss of the manufactured shampoo composition, the composition according to Examples and Comparative Examples 1 to 4 was used to clean hair and scalp once a day for 30 men with alopecia, The results are shown in Table 1 below. (The results are shown in Table 1 below. In Table 1, when the effect of decreasing hair loss was significant at 2 months after washing, 4 points for excellent, 3 points for normal, 2 points for unchanged, and 1 point for severe hair loss symptoms).

As shown in Table 2, it was confirmed that the compositions according to Examples 1 to 3 were superior to those of Comparative Examples 1 and 2 in preventing the hair loss, and in particular, the hair loss of the shampoo composition without the hydrolized sponge It was confirmed that the effect of preventing the hair loss was remarkably increased due to the addition of the hydrolized sponge.

In addition, in Comparative Example 2 in which mushroom extract was not used, it was confirmed that the effect of preventing hair loss was lower than those of Examples 1 to 3 in which mushroom extract was mixed. Thus, the effect of preventing vitamin D from being introduced due to the introduction of vitamin D contained in mushroom extract , Respectively.

<Experimental Example 2> Analysis of moisturizing effect

In order to analyze the moisturizing effect of the composition, 30 men were allowed to wash their hair and scalp for 2 months with the compositions of Examples 1 to 3 and Comparative Example 1, and finally washed at a point 2 months later The moisture change rate was measured for 1 to 6 hours, and the results are shown in Fig. 2 below.

As shown in FIG. 2, it was confirmed that the moisture content was maintained at a certain level in the scalp of a male washed with the shampoo compositions of Examples 1 and 2 as compared with the shampoo composition of Comparative Example 1, and it was confirmed that the moisturizing effect was excellent , And it was confirmed through this fact that the moisturizing effect was increased by the hydrolized sponge.

<Experimental Example 3> Analysis of dandruff removal effect

30 men in their thirties who were judged to have dandruff were selected and divided into 3 groups. The accumulated dandruff for 2 days was collected by a vacuum suction device and the weight of collected dandruff was measured. Then, hair and scalp were cleaned with hair and scalp cleansing composition once a day for two months for each formulation for each group, and the weight of dandruff accumulated at intervals of two days was compared, The dandruff reduction rate was calculated by comparing the weight of dandruff before washing with the weight of dandruff after two months of using the composition, and the results are shown in Table 3 below.

[Formula 1]

As shown in Table 3, it was confirmed that the compositions prepared by the methods according to Examples 1 to 3 were also excellent in anti-dandruff effect, whereas in the case of the composition of Comparative Example 1 not containing the hydrolized sponge , And the effect of preventing dandruff was the lowest.

<Experimental Example 4> Formulation stability analysis

In order to analyze the formulation stability of the shampoo compositions prepared by the methods according to Examples 1 to 3, the prepared shampoo compositions were allowed to stand at a high temperature (40 占 폚), a low temperature (3 占 폚) And observed changes over time for about 3 months. Especially, high temperature condition was observed and changes in color, flavor and the like were observed compared with low temperature conditions.

Lastly, the prepared shampoo composition was stored for 12 hours in a freezing condition (-20 占 폚), thawed at room temperature for 12 hours, and then stored again under refrigeration condition for 10 times, and the liquid change Freeze-thaw test was carried out to observe the temperature, sedimentation, formation of sediment, etc.).

As a result, it was confirmed that no phase separation occurred in the shampoo composition in all cases, and it was confirmed that each of the materials could be dissolved at a specific temperature to produce a shampoo composition excellent in formulation stability.

Claims (6)

Hair extracts containing medicinal plant extracts derived from medicinal plants including Hanshiku, Hassuo, and papaya and 2,4-diaminopyrimidine-3-oxide (Kopexil) Composition for cleaning scalp. The method according to claim 1,
1 to 10 parts by weight of the medicinal plant extract and 0.1 to 10 parts by weight of the 2,4-diaminopyrimidine-3-oxide based on 100 parts by weight of the composition. The method according to claim 1,
Wherein the composition further comprises 0.5 to 5 parts by weight of a hydrolysed sponge powder. The method according to claim 1,
And at least one additive selected from the group consisting of herbal extracts, mushroom extracts, vitamins, moisturizers, surfactants, foaming agents, conditioning agents, pH adjusting agents, pearlizing agents, preservatives, antibacterial agents, By weight of the composition. A method for producing a hair and scalp cleaning composition according to any one of claims 1 to 4,
(a) supplying a mixture of medicinal plants including Hanshikoshi, Hassuo and Hwasoji and water to a vacuum low temperature extractor, and extracting the medicinal plant extract by vacuum distillation;
(b) supplying purified water and Polyquaternium-10 to a mixing tank and heating the mixture to a temperature of 60 to 80 占 폚 to prepare a first mixture;
(c) heating the first mixture to a temperature of 60 to 80 ° C and adding disodium laureth sulfosuccinate, alkylpolyglycosides, sodium cocoyl amino acid fructose, cocoamidoproply betaine, and cocoyl monoethanolamine to prepare a second mixture, respectively;
(d) heating the second mixture to a temperature of 40 to 60 DEG C to produce a third mixture by feeding PEG-120 methyl glucose dioleate;
(e) heating the third mixture to a temperature of 30 to 50 DEG C and adding glycerin, panthenol, salicylic acid, ethylenediamine tetra acetic acid (EDTA) disodium salt ), Linoleamidopropyl PG-dimonium chloride phosphate, and the above-mentioned medicinal plant extract to prepare a fourth mixture; And
(f) preparing a composition for cleaning hair and scalp by sequentially mixing a fourth mixture with a grapefruit extract, sodium benzoate, and a flavoring agent to prepare a hair and scalp cleansing composition. 6. The method of claim 5,
Wherein the step (e) further comprises the step of supplying the hydrolyzed sponge to the fourth mixture after the fourth mixture is prepared.

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