KR100861715B1 - Softener treatment method of silk material which can wash water - Google Patents
Softener treatment method of silk material which can wash water Download PDFInfo
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- KR100861715B1 KR100861715B1 KR1020070060039A KR20070060039A KR100861715B1 KR 100861715 B1 KR100861715 B1 KR 100861715B1 KR 1020070060039 A KR1020070060039 A KR 1020070060039A KR 20070060039 A KR20070060039 A KR 20070060039A KR 100861715 B1 KR100861715 B1 KR 100861715B1
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims abstract description 14
- 239000000463 material Substances 0.000 title abstract description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 20
- 230000018044 dehydration Effects 0.000 claims abstract description 16
- 238000006297 dehydration reaction Methods 0.000 claims abstract description 16
- VDFVNEFVBPFDSB-UHFFFAOYSA-N 1,3-dioxane Chemical compound C1COCOC1 VDFVNEFVBPFDSB-UHFFFAOYSA-N 0.000 claims abstract description 10
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical class CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 10
- 229960000583 acetic acid Drugs 0.000 claims abstract description 10
- 239000012362 glacial acetic acid Substances 0.000 claims abstract description 10
- 229920000570 polyether Polymers 0.000 claims abstract description 10
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims abstract description 10
- ULWHHBHJGPPBCO-UHFFFAOYSA-N propane-1,1-diol Chemical compound CCC(O)O ULWHHBHJGPPBCO-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000005406 washing Methods 0.000 claims abstract description 10
- 239000003673 groundwater Substances 0.000 claims abstract description 8
- 239000008399 tap water Substances 0.000 claims abstract description 8
- 235000020679 tap water Nutrition 0.000 claims abstract description 8
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 5
- 239000004902 Softening Agent Substances 0.000 abstract description 9
- QUSNBJAOOMFDIB-UHFFFAOYSA-O ethylaminium Chemical compound CC[NH3+] QUSNBJAOOMFDIB-UHFFFAOYSA-O 0.000 abstract description 3
- 229950004354 phosphorylcholine Drugs 0.000 abstract description 3
- 238000004383 yellowing Methods 0.000 abstract description 3
- GOJUJUVQIVIZAV-UHFFFAOYSA-N 2-amino-4,6-dichloropyrimidine-5-carbaldehyde Chemical group NC1=NC(Cl)=C(C=O)C(Cl)=N1 GOJUJUVQIVIZAV-UHFFFAOYSA-N 0.000 abstract 1
- 208000005156 Dehydration Diseases 0.000 description 10
- 239000004744 fabric Substances 0.000 description 5
- 239000000835 fiber Substances 0.000 description 4
- 238000007654 immersion Methods 0.000 description 4
- 235000021028 berry Nutrition 0.000 description 2
- 239000002979 fabric softener Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 1
- 239000003093 cationic surfactant Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2211/00—Protein-based fibres, e.g. animal fibres
- D10B2211/01—Natural animal fibres, e.g. keratin fibres
- D10B2211/04—Silk
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
- Y02P70/62—Manufacturing or production processes characterised by the final manufactured product related technologies for production or treatment of textile or flexible materials or products thereof, including footwear
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
본 발명은 서로 다른 다양한 종류의 유연제를 배합하여 처리함으로써 실크제품에 평활성을 부여하고, 백도가 저하되거나 황변을 없앨 수 있는 물세탁이 가능한 실크 소재의 유연제 처리방법에 관한 것으로, (a) 제조된 실크 제품을 지하수 또는 수도물을 사용하되, 온도가 15℃ 내지 25℃가 되도록 유지시키면서 15 내지 20분 침지시킨 후에 탈수하는 단계; (b) 상기 탈수 후, 제품 1kg당 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 제1 유연제 0.33g과, 실리콘변성폴리에테르로 이루어진 제2 유연제 1.30g과, 빙초산으로 이루어진 제3 유연제 40g을 각각 물 15리터와 혼합 투입하여 회전조에서 5 내지 15분간 회전시키는 단계;(c) 상기 (b)단계 후 상기 실크 제품을 지하수 또는 수도물 온도가 35℃ 내지 45℃가 유지되도록 하면서 15 내지 25분 정도 침지시킨 후에 탈수하는 단계;(d) 상기 탈수 후, 제품 1kg당 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 제1 유연제 0.67g과, 변성실리콘 폴리에테르로 이루어진 제2 유연제 2.50g과, 빙초산으로 이루어진 제3 유연제 60g을 각각 물 15리터와 혼합 투입하여 회전조에서 5 내지 15분간 회전시키는 단계;(e) 탈수 및 건조시키는 단계로 이루어진 물세탁이 가능하도록 한 실크제품의 유연제 처리방법을 제공한다.The present invention relates to a method of treating a softening agent of a silk material capable of washing water by adding various kinds of different softening agents to give smoothness to silk products and reducing whiteness or yellowing. Dewatering the silk product using groundwater or tap water for 15 to 20 minutes, while maintaining the temperature at 15 ° C to 25 ° C; (b) 0.33 g of a first softener composed of propanediol, ethanamine salt, 2-amino-N-hydroxyethylene sulfate, propanol, and 1,3-dioxane per kg of product after dehydration; 1.30 g of a second softener made of polyether and 40 g of a third softener made of glacial acetic acid are mixed with 15 liters of water and rotated in a rotary bath for 5 to 15 minutes; (c) after the step (b), the silk product Dehydration of the ground water or tap water while immersing for about 15 to 25 minutes while maintaining a temperature of 35 ℃ to 45 ℃; (d) after the dehydration, propanediol, ethanamine salt (Ethanaminium), 2-amino per kg product 15 liters of 0.67 g of a first softener consisting of -N-hydroxyethylene sulfate, propanol, 1,3-dioxane, 2.50 g of a second softener consisting of modified silicone polyether, and 60 g of a third softener consisting of glacial acetic acid Mixed with Provides (e) dewatering and drying step, a softening treatment of the silk washing water to be made up of; W rotating rotates 5 to 15 minutes in a tank.
Description
본 발명은 서로 다른 종류의 유연제를 배합하여 처리함으로써 실크 제품에 평활성을 부여하고, 백도가 저하되거나 황변을 없앨 수 있는 물세탁이 가능한 실크 소재의 유연제 처리방법에 관한 것이다. The present invention relates to a method for treating a softening agent of a silk material which is capable of washing water by combining different kinds of softening agents to impart smoothness to the silk product and reducing whiteness or yellowing.
일반적으로 섬유 유연제는 섬유의 올을 살려 옷감을 부드럽게 하고, 음이온인 섬유에 양이온 계면활성제를 흡착시켜 중화시킴으로써 정전기를 방지하는 기능을 한다. 또한 천의 색깔이 바래는 것을 방지하고 세제 찌꺼기가 남지 않도록 하는 역할을 한다. 최근에는 구김을 방지할 수 있는 링클이 없는 효과를 더한 다기능 섬유 유연제도 출시되고 있으나 그 기능이 단기능성이어서 실크 제품에는 적합하지 않는 경우가 많아 실 크소재의 세탁시에는 실크 소재가 손상되는 경우가 대부분이다. In general, fabric softeners function to soften the fabric by making use of the fibers of the fiber and to prevent static electricity by adsorbing and neutralizing a cationic surfactant on the anion fibers. It also serves to prevent the fabric from fading and to leave no detergent residues. Recently, multi-functional fabric softeners with wrinkle-free effects to prevent wrinkles have been released. However, since their functions are monofunctional, they are often not suitable for silk products, and silk materials are often damaged when washing silk materials. Mostly.
통상 실크 제품은 그 올이 매우 부드럽고 민감하여 실제로 물세탁을 할 경우 주름이 가게 되거나 실크 섬유표면을 손상시켜 옷감이 버리게 되어 세탁소에 맡겨 증기세탁이나 오일세탁을 해야하므로 실크 제품의 유지 관리에 비용이 많이 들어가 는 문제점이 있었다. 또한 유연제를 사용하더라도 특히 세탁기를 사용하여 탈수처리를 하거나 할 경우에는 옷감이 손상되는 문제점을 여전히 안고 있다.In general, silk products are very soft and sensitive, and the actual washing of water causes wrinkles or damages to the surface of silk fibers, causing the fabric to be discarded. There was a problem going into a lot. In addition, even if the softener is used, especially when dehydration treatment using a washing machine, there is still a problem that the cloth is damaged.
따라서 본 발명은 상기와 같은 문제점을 해결하기 위해서 여러 특징을 갖는 여러 종류의 유연제 적어도 3가지의 유연제를 적정량 배합하고, 적정 시간동안 침지 및 탈수를 반복하는 과정을 거치면서, 실크 제품을 물세탁이 가능하도록 하는 유연제 처리방법을 제공하는 것을 기술적 과제로 한다. Therefore, the present invention, in order to solve the above problems, by mixing a suitable amount of at least three softeners of various types of softeners having various characteristics, the process of repeating the immersion and dehydration for a suitable time, water washing the silk products It is a technical problem to provide a method of treating a softener to make it possible.
본 발명은 상기와 같은 기술적 과제를 해결하기 위해서, The present invention to solve the above technical problem,
(a) 제조된 실크 제품을 지하수 또는 수도물을 사용하되, 온도가 15℃ 내지 25℃가 되도록 유지시키면서 15 내지 20분 침지시킨 후에 탈수하는 단계; (b) 상기 탈수 후, 제품 1kg당 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 제1 유연제 0.33g과, 변성실리콘 폴리에테르로 이루어진 제2 유연제 1.30g과, 빙초산으로 이루어진 제3 유연제 40g을 각각 물 15리터와 혼합 투입하여 회전조에서 5 내지 15분간 회전시키는 단계; (c) 상기 (b)단계 후 상기 실크 제품을 지하수 또는 수도물 온도가 35℃ 내지 45℃가 유지되도록 하면서 15 내지 25분 정도 침지시킨 후에 탈수하는 단계; (d) 상기 탈수 후, 제품 1kg당 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 제1 유연제 0.67g과, 변성실리콘 폴리에테르로 이루어진 제2 유연제 2.50g과, 빙초산으로 이루어진 제3 유연제 60g을 각각 물 15리터와 혼합 투입하여 회전조에서 5 내지 15분간 회전시키는 단계;(e) 탈수 및 건조시키는 단계로 이루어진 물세탁이 가능하도록 한 실크 제품의 유연제 처리방법을 제공하는 것을 목적으로 한다.(a) dewatering the prepared silk product using groundwater or tap water for 15 to 20 minutes, while maintaining the temperature at 15 ° C to 25 ° C; (b) after dehydration, 0.33 g of a first softener composed of propanediol, ethanamine salt, 2-amino-N-hydroxyethylene sulfate, propanol, and 1,3-dioxane per kg of product; 1.30 g of a second softener made of polyether and 40 g of a third softener made of glacial acetic acid are mixed with 15 liters of water and rotated in a rotary bath for 5 to 15 minutes; (c) dehydrating the silk product after step (b) after immersing the silk product for about 15 to 25 minutes while maintaining the groundwater or tap water temperature of 35 ° C to 45 ° C; (d) after dehydration, 0.67 g of a first softener consisting of propanediol, ethanamine, 2-amino-N-hydroxyethylene sulfate, propanol, and 1,3-dioxane per kg of product, and modified silicone 2.50 g of a second softener made of polyether and 60 g of a third softener made of glacial acetic acid are mixed with 15 liters of water and rotated in a rotary bath for 5 to 15 minutes; (e) water washing comprising dehydrating and drying. It is an object of the present invention to provide a method for treating softeners in silk products.
또한 본 발명에서 실크제품에 유연성을 부여하기 위해서 사용하는 3가지 종류의 유연제는 제1, 제2, 제3 유연제로 표시한다. 상기 제1 유연제는 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 것으로 베리소프트(상품명 : VARI SOFT 222 LM90 : 골드쉬미드트 사제)이고, 제2유연제는 변성실리콘 폴리에테르로 이루어진 솔라 에스알에스(상품명 : SOLA SRS : 디보시바 사제)이고, 제3 유연제는 빙초산으로 이루어진 것임으로 밝혀둔다. In addition, the three types of softeners used to impart flexibility to the silk products in the present invention are referred to as first, second, third softeners. The first softening agent is composed of propanediol, ethanamine salt (Ethanaminium), 2-amino-N-hydroxyethylene sulfate, propanol, 1,3-dioxane, berry soft (trade name: VARI SOFT 222 LM90: Gold Schmid Ltd.), the second softener is Solar SLS (trade name: SOLA SRS: manufactured by Divoshiba), which is made of modified silicone polyether, and the third softener is made of glacial acetic acid.
본 발명에서는 통상적으로 제조된 실크 제품을 물을 이용하여 침지시키는 과정을 거치는데 이때 사용되는 물의 종류는 크게 제한되지 않으나. 지하수 또는 수도물을 사용하는 것이 바람직하다.In the present invention, the process of immersing a silk product manufactured using water is generally not limited. It is preferable to use groundwater or tap water.
또한 물 침지시 사용되는 물의 온도는 5℃ 내지 30℃ 범위내의 물을 사용해도 좋으나 가장 바람직하게는 15℃ 내지 25℃가 되도록 유지시키면서 침지시키는 것이 바람직하다. 실크 제품의 침지 시간은 통상적으로 10 내지 30분 정도이나 가장 바람직하게는 15 내지 20분 침지시킨 후에 1차 탈수하는 것이 좋다. In addition, the temperature of the water used during the water immersion may be water in the range of 5 ° C to 30 ° C, but most preferably it is immersed while maintaining the temperature to 15 ° C to 25 ° C. The immersion time of the silk product is usually about 10 to 30 minutes, but most preferably 15 to 20 minutes after the first dehydration.
이렇게 실크 제품을 1차 탈수시킨후에 실크 제품 1kg당 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 제1 유연제 0.33g과, 변성실리콘 폴리에테르로 이루어진 제2 유연제 1.30g과, 빙초산으로 이루어진 제3 유연제 40g을 각각 물 15리터와 혼합 투입하여 회전조에서 회전시켜 2차 탈수시키는 과정을 거친다. 이때 탈수시키는 시간은 통상 3 내지 20분 정도이나 바람직하게는 5 내지 15분간 회전시켜 탈수시키는 것이 바람직하다. After first dehydrating the silk product, 0.33 g of a first softener composed of propanediol, ethanamine, 2-amino-N-hydroxyethylene sulfate, propanol, and 1,3-dioxane per kg of silk product , 1.30 g of the second softener made of modified silicone polyether and 40 g of the third softener made of glacial acetic acid were mixed with 15 liters of water, and then rotated in a rotary tank to undergo secondary dehydration. At this time, the time for dehydration is usually about 3 to 20 minutes, preferably, it is preferable to spin and spin for 5 to 15 minutes.
이어서, 상기와 같이 제1,제2, 제3 유연제와 혼합투입하여 2차 탈수시킨 후에 상기 실크 제품을 재차 지하수 또는 수도물 온도가 30℃ 내지 48℃ 범위내에서 가장 바람직하게는 35℃ 내지 45℃내에서 유지되도록 하면서 15 내지 25분 정도 침지시킨 후에 3차 탈수하는 과정을 거치게 된다. Subsequently, after the second and second dehydration by mixing with the first, second, and third softeners as described above, the groundwater or tap water temperature is most preferably in the range of 30 ° C to 48 ° C, and most preferably 35 ° C to 45 ° C. After being immersed for about 15 to 25 minutes while being maintained in, it is subjected to the third dehydration process.
상기와 같이 실크제품을 3차례에 걸쳐 탈수시킨 후에, 실크 제품 1kg당 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 제1 유연제 0.67g과, 변성실리콘 폴리에테르로 이루어진 제2 유연제 2.50g과, 빙초산으로 이루어진 제3 유연제 60g을 각각 물 15리터와 혼합 투입하여 회전조에서 5 내지 15분간 회전시킨 후에 마지막으로 탈수시킨 후에 실크 제품을 통상의 건조방법으로 건조시켜 유연제 처리과정을 종료하게 된다. After dehydrating the silk product three times as described above, a product consisting of propanediol, ethanamine salt, 2-amino-N-hydroxyethylene sulfate, propanol, and 1,3-dioxane per kg of silk product 1 0.67 g of a softener, 2.50 g of a second softener made of modified silicone polyether, and 60 g of a third softener made of glacial acetic acid were mixed with 15 liters of water, rotated in a rotary bath for 5 to 15 minutes, and finally dehydrated. The silk product is dried by a conventional drying method to terminate the softener treatment process.
상기와 같이 다양한 종류의 유연제(1,2,3)를 적정량 혼합하고, 적정 온도의 물속에서 침지와 탈수를 반복함으로써 실크 제품 소재가 유연하게 변화되게 되면서, 물세탁이 가능하게 되는 것이다. As described above, by mixing a suitable amount of various kinds of softeners (1, 2, 3) and repeating the immersion and dehydration in the water of the appropriate temperature, the silk product material is changed flexibly, water washing is possible.
또한 본 발명에서 실크 제품에 유연성을 부여하기 위해서 사용하는 3가지 종류의 유연제는 제1,제2,제3 유연제로 표시한다. 상기 제1 유연제는 프로판디올, 에탄아민염(Ethanaminium), 2-아미노-N-하이드록시에틸렌설페이트, 프로판올, 1,3-디옥산으로 이루어진 것으로 베리소프트(상품명 : VARI SOFT 222 LM90 : 골드쉬미드트 사제)로서 코팅된 직물의 윤기를 향상시켜주는 기능한다. 또한 제2 유연제는 변성실리콘 폴리에테르로 이루어진 솔라 에스알에스(상품명 : SOLA SRS : 디보시바 사제)로서 유연 코팅처리가 미세하고 견고하게 이루어지는 기능을 한다. 또한 제3 유연제로서는 빙초산을 사용함을 밝혀둔다. In addition, the three types of softeners used to impart flexibility to the silk products in the present invention are referred to as first, second, third softeners. The first softening agent is composed of propanediol, ethanamine salt (Ethanaminium), 2-amino-N-hydroxyethylene sulfate, propanol, 1,3-dioxane, berry soft (trade name: VARI SOFT 222 LM90: Gold Schmid Co., Ltd.) to improve the gloss of the coated fabric. In addition, the second softening agent is a solar SLS (trade name: SOLA SRS: manufactured by Divoshiba) made of a modified silicone polyether, and has a function of making the soft coating treatment fine and firm. It is also found that glacial acetic acid is used as the third softener.
인장강도The tensile strength 실험예Experimental Example
본 발명의 처리방법으로 처리된 실크 스타킹에 대한 인장 강도를 측정하였다. 측정조건은 본 발명에 의한 처리전 시료는 시료 1로, 본 발명의 유연제처리방법으로 처리한 시료는 시료 2로 표시하였다. 인장강도 실험은 KS K 0815:2006 컷스트링법에 기준하여 측정하였다. Tensile strength for the silk stockings treated with the treatment method of the present invention was measured. In the measurement conditions, the sample before the treatment according to the present invention was represented by Sample 1, and the sample treated by the softening agent treatment method of the present invention was represented by Sample 2. Tensile strength experiments were measured based on KS K 0815: 2006 cutstring method.
측정결과는 시료1 에서는 22(N/3.0cm) 이었으나, 시료 2(본 발명의 처리시료)에서는 26(N/3.0cm)로서 처리전에 비해서 약 18% 정도 인장 강도가 향상되었음을 확인할 수 있었다. 시험결과는 아래 표1과 같다The measurement result was 22 (N / 3.0cm) in Sample 1, but 26 (N / 3.0cm) in Sample 2 (treated sample of the present invention), and it was confirmed that the tensile strength was improved by about 18% compared to before the treatment. The test results are shown in Table 1 below.
본 발명에 의한 실크제품의 유연제 처리 방법에 따르면, 실크 소재 사이가 엉겨붙는 검업(gum-up)현상이 제거되며, 소재 표면에 우수한 평활성을 제공하는 동시에 건조시 백도가 저하되고 황변이 발생하지 않는 제반 효과가 있다. According to the softening agent treatment method of the silk product according to the present invention, the gum-up phenomenon of tangling between the silk material is eliminated, providing excellent smoothness to the surface of the material, and at the same time, whiteness is reduced and yellowing does not occur during drying. It is effective.
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| KR101073157B1 (en) | 2011-03-15 | 2011-10-12 | 한국염색기술연구소 | Method for manufacturing protein-based textile fabrics that can be washed with water |
| US8292971B2 (en) | 2008-10-27 | 2012-10-23 | Man Soo Choi | Method of treating fabric conditioner for washable silk products |
| CN105484028A (en) * | 2015-12-18 | 2016-04-13 | 张莘蔓 | Silk bulking method |
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