KR0170110B1 - Antidandruff hair care composition - Google Patents
Antidandruff hair care composition Download PDFInfo
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- KR0170110B1 KR0170110B1 KR1019960001045A KR19960001045A KR0170110B1 KR 0170110 B1 KR0170110 B1 KR 0170110B1 KR 1019960001045 A KR1019960001045 A KR 1019960001045A KR 19960001045 A KR19960001045 A KR 19960001045A KR 0170110 B1 KR0170110 B1 KR 0170110B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4926—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having six membered rings
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4906—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom
- A61K8/4933—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with one nitrogen as the only hetero atom having sulfur as an exocyclic substituent, e.g. pyridinethione
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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Abstract
본 발명은 비듬방지 성분, 예를 들어 피록톤올아민(piroctone olamine), 아연피리치온(zinc pyrithione) 등을 티트리오일과 함께 사용함으로써 각각을 단독으로 사용하는 경우에 비해 비듬방지 및 치료효과와 두피 가려움 제거 효과가 탁월한 모발제품 조성물에 관한 것이다.The present invention by using anti-dandruff components, for example, pyroctone olamine, zinc pyrithione (zinc pyrithione) in combination with tea tree oil, anti-dandruff and therapeutic effects and scalp compared to the case of using each alone It relates to a hair product composition having an excellent itch removal effect.
Description
본 발명은 티트리오일(Tea tree oil)을 비듬방지 성분과 함께 함유함을 특징으로 하는 비듬방지용 모발제품 조성물에 관한 것이다. 좀더 구체적으로 본 발명은 비듬방지 성분, 예를 들어 피록톤올아민(piroctone olamine), 아연피리치온(zinc pyrithione) 등을 티트리오일과 함께 사용함으로써 각각을 단독으로 사용하는 경우에 비해 비듬방지 및 치료효과와 두피 가려움 제거 효과가 탁월한 모발제품 조성물에 관한 것이다.The present invention relates to an anti-dandruff hair product composition comprising tea tree oil together with an anti-dandruff component. More specifically, the present invention uses anti-dandruff components, for example, pyroctone olamine, zinc pyrithione, and the like with tea tree oil, thereby preventing and treating dandruff, respectively. The present invention relates to a hair product composition having an excellent effect on scalp and itching.
비듬은 두피의 죽은 세포가 자연적으로 떨어져 나가는 것으로 일반 피부에서 때와 같은 것이다. 따라서 정상적인 비듬은 눈에 보이지 않을 정도로 작아 문제가 되지 않는다. 그러나, 통상 비듬이라 불리는 것은 두피의 각질 세포가 두피에서 분비되는 피지, 땀 등과 뭉쳐 덩어리로 된 것으로서 이러한 비듬은 피지 성분이 분해되어 생성되는 산패 지방산이 두피 기저층 세포를 자극하여 세포 과증식을 유발시킴으로써 발생되며 보통 가려움증을 수반한다. 특히, 두피상제균으로서 비듬의 원인균으로 알려진 피티로스포룸 오발레(Pityrosporum ovale)가 피지 성분의 산패를 촉진하는 것으로 알려져 있다.Dandruff is a natural release of dead cells from the scalp, just like normal skin. Therefore, normal dandruff is invisible and small. However, what is commonly referred to as dandruff is a clump of keratinocytes secreted from the scalp and sebum, sweat, etc. These dandruff occurs when rancid fatty acids produced by decomposition of sebum components stimulate the scalp basal layer cells to cause cell hyperproliferation. Usually accompanied by itching. In particular, Pytirosporum ovale, known as a causative agent of dandruff as a scalp fungus, is known to promote rancidity of sebum components.
따라서, 이러한 비정상적인 비듬을 예방 및 치료하기 위해 여러 성분이 시험 연구되어 왔으나, 비듬방지 성분들은 인체 안전성에 문제가 있어 그 사용량이 법적으로 제한됨에 따라 소기의 효과를 거두기 어려운 문제가 있다.Therefore, although various components have been tested and studied to prevent and treat such abnormal dandruff, the anti-dandruff components have a problem in human safety, and their usage is legally restricted, and thus, it is difficult to achieve the desired effect.
이에 본 발명자들은 천연의 방부제 및 살균제로 사용되어왔던 티트리오일의 항균력에 대한 연구를 수행하던 중, 이를 비듬방지 성분들과 혼합하여 사용하면 비듬의 원인균으로 알려진 피티로스포룸 오발레에 대하 살균 효과가 상승적으로 증가하며, 특히 인체 안전성에 문제가 있어 법적으로 사용량이 제한되는 통상의 비듬방지 성분들의 사용량을 줄여도 탁월한 비듬방지 및 치료 효과와 두피 가려움 제거 효과가 발휘됨을 발견하여 본 발명을 완성하게 되었다.Therefore, the present inventors are studying the antimicrobial activity of tea tree oil, which has been used as a natural preservative and fungicide, and when used in combination with anti-dandruff ingredients, the bactericidal effect against Pytilosporum obale known as the causative agent of dandruff Has been synergistically increased, and in particular, the present invention has been found to have excellent anti-dandruff and therapeutic effects and scalp itch removal even though the use of conventional anti-dandruff ingredients, which are legally limited due to problems in human safety, is exerted. .
이하, 본 발명의 구성을 상세히 설명한다.Hereinafter, the configuration of the present invention will be described in detail.
본 발명은 티트리오일(Tea tree oil)을 비듬방지 성분과 함께 함유함을 특징으로 하는 비듬방지용 모발제품 조성물에 관한 것이다.The present invention relates to an anti-dandruff hair product composition comprising tea tree oil together with an anti-dandruff component.
본 발명에 따른 모발제품 조성물에서 유효성분으로 사용하는 티트리오일은 학명이 멜랄루카 알테르니폴리아(Melaleuca alternifolia)인 식물의 오일 성분으로서 α-투젠(α-Thujene), α-피넨(α-Pinene), α-테르피넨(α-Terpinene), 1,8-시네올(1,8-Cineole), α-테르피놀렌(α-Terpinolene), γ-테르피넨(γ-Terpinene), 테르피넨-4-올(Terpinene-4-ol)을 주요 성분으로 한다. 또한, 티트리오일은 호주(Australia)등에서 60여년 동안 천연의 방부제와 살균제로 사용되어 왔으며, 특히 박테리아 및 진균류에 대하여 억제 및 제거 능력을 보유하고 있는 것으로 보고되어 있다.Tea tree oil used as an active ingredient in the hair product composition according to the present invention is an oil component of plants of the scientific name Melaleuca alternifolia (α-Thujene), α-Pinene (α-Pinene) ), α-Terpinene, 1,8-cineol, 1,8-Cineole, α-Terpinolene, γ-Terpinene, terpinene- 4-ol (Terpinene-4-ol) is the main ingredient. In addition, tea tree oil has been used as a natural preservative and fungicide for more than 60 years in Australia, etc., and has been reported to have the ability to inhibit and eliminate bacteria and fungi.
비듬방지 및 두피 가려움의 제거를 목적으로 비듬방지 성분과 배합하여 사용하는 경우에 티트리오일의 사용량은 0.1 내지 5.0중량%가 바람직하다. 0.1중량% 미만으로 사용하는 경우에는 그 효과가 미약하고 5.0중량% 초과 사용시에는 사용량의 증가에 비례적인 효과의 상승이 나타나지 않는다.When used in combination with an anti-dandruff component for the purpose of preventing dandruff and scalp itch, the amount of tea tree oil is preferably 0.1 to 5.0% by weight. If the amount is less than 0.1% by weight, the effect is insignificant. If the amount is more than 5.0% by weight, there is no increase in the proportional effect.
티트리오일과 함께 사용할 비듬방지 성분으로는 피록톤올아민[piroctoneolamine, 상품명:Octopirox(Hoechst)] 또는 아연피리치온[zine pyrithione, 상품명:Zinc Omadine(Oline)]등을 언급할 수 있고, 이들의 사용량은 제한하지 않는다.Anti-dandruff components to be used with tea tree oil may include piroctoneolamine (Octopirox (Hoechst)) or zine pyrithione (Zinc Omadine (Oline)), and the like. Does not limit.
또한, 본 발명에 따른 모발제품은 샴푸, 헤어컨디셔너, 헤어토닉, 헤어크림, 헤어스프레이 또는 헤어무쓰 등의 형태로 사용할 수 있다.In addition, the hair product according to the present invention can be used in the form of shampoo, hair conditioner, hair tonic, hair cream, hair spray or hair mousse.
이하, 본 발명을 하기 실시예 및 실험예에 의가하여 보다 구체적으로 설명한다. 그러나, 이들 실시예는 본 발명에 대한 이해를 돕기 위한 것일 뿐, 어떤 의미로든 본 발명의 범위가 이들 실시예로 한정되는 것은 아니다.Hereinafter, the present invention will be described in more detail with reference to the following Examples and Experimental Examples. However, these examples are only for the understanding of the present invention, and the scope of the present invention in any sense is not limited to these examples.
[실시예 1 내지 4 및 비교예 1 내지 4][Examples 1 to 4 and Comparative Examples 1 to 4]
하기 표 1에 나타낸 바와 같은 조성비율로 30% 라우릴황산나트륨 수용액, 30% 폴리옥시에틸렌라우릴황산나트륨(n=3) 수용액, 야자유지방산디에탄올아미드 및 프로필렌글리콜을 물에 첨가한 후, 혼합물에 피록톤올아민을 첨가하고 60℃로 될 때까지 가온하여 균일하게 용해시킨 다음 40℃로 냉각시켰다. 혼합물에 아연피리치온, 티트리오일, 색소, 파라옥시안식향산에스테르, 향료 및 구연산을 가하고 혼합한 후 냉각시켜 샴푸를 제조하였다.30% sodium lauryl sulfate solution, 30% polyoxyethylene lauryl sulfate (n = 3) aqueous solution, palm oil fatty acid diethanolamide and propylene glycol were added to the water at the composition ratio as shown in Table 1 below, Tonolamine was added and warmed up to 60 ° C to dissolve uniformly and then cooled to 40 ° C. Zinc pyrithione, tea trioil, pigment, paraoxybenzoic acid ester, fragrance and citric acid were added to the mixture, mixed and cooled to prepare a shampoo.
상기 실시예 1 내지 4 및 비교예 1 내지 4의 샴푸 조성물에 대한 비듬방지 효과 및 가려움 제거 효과는 하기 시험예 1, 2 및 3의 방법으로 평가하였으며, 그 결과를 표 2 내지 4에 나타내었다.The anti-dandruff effect and the itch removal effect of the shampoo compositions of Examples 1 to 4 and Comparative Examples 1 to 4 were evaluated by the methods of Test Examples 1, 2, and 3 below, and the results are shown in Tables 2 to 4 below.
[시험예 1][Test Example 1]
비교적 비듬이 많은 40명의 피험자를 선정하여 하기 설명하는 바의 방식으로 표1의 샴푸 조성물의 효과를 1개월 동안 시험하였다.Forty subjects with relatively high dandruff were selected and tested for one month for the effect of the shampoo composition of Table 1 in the manner described below.
시험개시 전에 통상의 샴푸로 세발하고 3일간 누적된 비듬을 채집하여 채집된 비듬의 중량을 측정하였으며, 표 1의 샴푸 조성물로 1개월 동안 세발하고 시험 종료 후 3일간 누적된 비듬의 중량을 측정한 다음 시험전의 결과와 비교하였다. 이때 누적된 비듬은 진공 흡입 장치를 사용하여 두피로 부터 직접 채취하였고, 하기 식에 의거하여 비듬 감소율을 구한 다음 그 결과를 표 2에 나타내었다.The weight of the collected dandruff was measured by triturating with a conventional shampoo and collecting the dandruff accumulated for 3 days before starting the test. The weight of the collected dandruff was triturated for 1 month with the shampoo composition of Table 1 and the weight of the dandruff accumulated for 3 days after the end of the test. The results were compared with the results before the next test. At this time, the accumulated dandruff was collected directly from the scalp using a vacuum suction device, and the dandruff reduction rate was calculated based on the following equation, and the results are shown in Table 2.
단, 비듬방지 효과는 비듬 감소율이 30% 이상인 경우에만 실제로 효과가 있는 것으로 판정하였다.However, it was determined that the anti-dandruff effect was actually effective only when the dandruff reduction rate was 30% or more.
[시험예 2][Test Example 2]
표 1의 각 샴푸를 콘오일(corn oil)이 함유된 와이엠 액체배지(Ym broth)에 각각 5, 1, 0.5 및 0.1중량%로 첨가하고 피티로스포름 오발레를 10 -10 CFU(Colony Forming Unit)/ml의 양으로 접종하여 2일간 배양한 다음, 최소 미생물 억제농도(MIC, Minimal Inhibitory Concentration)와 최소 미생물 사멸농도(MBC, Minimal Bactericidal Concentration)를 구하였다. 그 결과는 표 3에 나타내었다.Each shampoo of Table 1 is added to Ym broth containing corn oil at 5, 1, 0.5 and 0.1% by weight, respectively, and Pytirosporum Ovale is added 10 -10 After inoculating CFU (Colony Forming Unit) / ml incubated for 2 days, the minimum microbial inhibitory concentration (MIC) and minimum microbial killing concentration (MBC) was determined. The results are shown in Table 3.
[시험예 3][Test Example 3]
평소 가려움을 느끼는 사람중 무작위로 선정된 남녀 40명에게 표 1의 샴푸를 2일에 1회씩 8주간 사용하게 한 후, 면접을 통하여 가려움중 완화 여부를 조사하였다. 평가는 하기 표 4의 기준에 의하여 피험자가 주관적으로 평점을 매긴 후 이를 평균하여 표 5에 나타내었다.Forty men and women randomly selected from among those who felt itching were given the shampoo shown in Table 1 once every two days for eight weeks, and then interviewed to find out whether itching was eased. Evaluation was based on the subject of the following Table 4 subjects are subjectively rated and then averaged it is shown in Table 5.
상기 표 2, 3, 5의 결과로 부터 알 수 있는 바와 같이, 티트리오일 및 비듬방지 성분이 동시에 함유된 본 발명의 실시예 1 내지 4의 샴푸 조성물은 티트리오일 또는 비듬방지 성분이 전혀 포함되지 않거나, 이들중 1가지 성분만이 함유된 비교예 1 내지 4의 샴푸 조성물에 비해 비듬방지 및 가려움 제거 효과가 탁월한 것으로 나타났다. 따라서, 이러한 결과를 통하여 티트리오일 또는 비듬방지 성분이 단독으로 함유되면 큰 효과를 기대할 수 없는 반면, 양 성분을 동시에 사용하면 이들이 상호 상승적으로 작용함으로써 만족스러운 효과가 나타남을 알 수 있었다.As can be seen from the results of Tables 2, 3, and 5, the shampoo composition of Examples 1 to 4 of the present invention simultaneously containing tea tree oil and anti-dandruff components contains no tea tree oil or anti-dandruff components. It was found that the anti-dandruff and anti-itch effects were superior to the shampoo compositions of Comparative Examples 1 to 4 containing only one component thereof. Therefore, it can be seen from these results that a great effect can not be expected if the tea tree oil or anti-dandruff ingredients are contained alone, while using both components at the same time, they show a satisfactory effect.
[실시예 5 내지 8 및 비교예 5 내지 8][Examples 5 to 8 and Comparative Examples 5 to 8]
하기 표 6에 나타낸 바와 같은 조성비율로 세탄올, 자기유화형 모노스테아린산글리세린, 파라옥시안식향산에스테르, 75% 염화디스테아릴디메틸암모늄, 프로필렌글리콜, 피록톤올아민을 물에 첨가한 후, 이 혼합물의 온도가 65℃로 될 때까지 가온하여 균일하게 용해시킨 다음 40℃로 냉각시켰다. 이어서, 상기 혼합물에 아연피리치온, 티트리오일, 색소, 향료 및 구연산을 가하고 혼합하여 헤어컨디셔너를 제조하였다.Cetanol, self-emulsifying glycerin monostearate, paraoxybenzoic acid ester, 75% distearyl dimethylammonium chloride, propylene glycol, and pyroxtonolamine were added to the composition ratio as shown in Table 6 below, followed by It was warmed up to 65 ° C., dissolved uniformly, and cooled to 40 ° C. Subsequently, zinc pyrithione, teatrioil, pigment, flavoring and citric acid were added to the mixture and mixed to prepare a hair conditioner.
상기 실시예 5 내지 8 및 비교예 5 내지 8의 헤어컨디셔너 조성물에 대한 비듬방지 효과 및 가려움 제거 효과는 하기 시험예 4 및 5의 방법으로 평가하였으며, 그 결과를 표 7 및 8에 나타내었다.The anti-dandruff effect and the itch removal effect on the hair conditioner compositions of Examples 5 to 8 and Comparative Examples 5 to 8 were evaluated by the methods of Test Examples 4 and 5, and the results are shown in Tables 7 and 8.
[시험예 4][Test Example 4]
비교적 비듬이 많은 40명의 피험자를 선정하여 하기 설명하는 바의 방식으로 표 6의 헤어컨디셔너의 조성물의 효과를 1개월 동안 시험하였다.Forty subjects with relatively high dandruff were selected and tested for one month on the effect of the composition of the hair conditioner of Table 6 in the manner described below.
시험개시 전에 통상의 샴푸로 세발하고 통상의 헤어컨디셔너를 사용한 후, 3일간 누적된 비듬을 채집하여 채집된 비듬의 중량을 측정하였다. 또한, 통상의 샴푸로 세발하고 표 6의 헤어컨디셔너 조성물을 1개월 동안 사용하게 한 다음 시험 종료 후 3일간 누적된 비듬의 중량을 측정하여 시험전의 결과와 비교하였다. 그 결과는 표 7에 나타내었다.Before starting the test, the hair was collected with a conventional shampoo and used with a conventional hair conditioner, and the weight of the collected dandruff was measured by collecting the dandruff accumulated for 3 days. In addition, the hair was shampooed with a conventional shampoo and allowed to use the hair conditioner composition of Table 6 for one month, and then the weight of the dandruff accumulated for three days after the end of the test was measured and compared with the results before the test. The results are shown in Table 7.
[시험예 5][Test Example 5]
표 6의 각 헤어컨디셔너를 콘오일(corn oil)이 함유된 와이엠 액체배지(Ym broth)에 각각 5, 1, 0.5 및 0.1중량%로 첨가하고 피티로스포름 오발레를 10 -10 CFU(Colony Forming Unit)/ml의 양으로 접종하여 2일간 배양한 다음, 최소 미생물 억제농도(MIC, Minimal Inhibitory Concentration)와 최소 미생물 사멸농도(MBC, Minimal Bactericidal Concentration)를 구하였다. 그 결과는 표 8에 나타내었다.Each hair conditioner of Table 6 was added to Ym broth containing corn oil at 5, 1, 0.5 and 0.1% by weight, respectively, and Pytirosporum Ovale was added 10 -10 After inoculating CFU (Colony Forming Unit) / ml incubated for 2 days, the minimum microbial inhibitory concentration (MIC) and minimum microbial killing concentration (MBC) was determined. The results are shown in Table 8.
상기 표 7 및 8의 결과로 부터 알 수 있는 바와 같이, 티트리오일 및 비듬방지 성분이 함께 함유된 본 발명의 실시예 5 내지 8의 헤어컨디셔너 조성물이 비교예 5 내지 8의 헤어컨디셔너 조성물에 비해 비듬방지 효과가 탁월할 뿐아니라 비듬의 원인균인 피티로스포름 오발레에 대해서도 살균력이 강한 것으로 나타났다.As can be seen from the results of Tables 7 and 8, the hair conditioner compositions of Examples 5 to 8 of the present invention together with tea tree oil and anti-dandruff components are compared to the hair conditioner compositions of Comparative Examples 5 to 8. In addition to its excellent anti-dandruff effect, it also showed strong antiseptic power against phytirosporum obale, the causative agent of dandruff.
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