JP7623575B2 - Method and device for preventing adhesion of kneaded raw materials in a vertical vacuum chamber of a vacuum extrusion molding device - Google Patents
Method and device for preventing adhesion of kneaded raw materials in a vertical vacuum chamber of a vacuum extrusion molding device Download PDFInfo
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Description
本発明は、高炉に用いる含炭塊成鉱などの真空押出成型装置の、真空室の付着抑制方法およびその装置に係る技術に属する。 The present invention relates to a method for suppressing adhesion in the vacuum chamber of a vacuum extrusion molding device for carbon-containing agglomerates used in blast furnaces, and to the technology related to that device.
高炉では、炉上部から原料鉱石と塊状コークスを投入しつつ炉下部から送風し、塊状コークスと送風エアから生成する還元ガスを炉下部から炉上部へと通風しながら、原料鉱石中の酸化鉄を還元溶解している。炉内での還元ガスの通風性を確保するため、原料鉱石には炉内で粉化しない強度を持つことが要求されている。このため、高炉では通常、焼結鉱や焼成ペレットのように、事前に高温で焼成した原料が用いられている。 In a blast furnace, raw ore and lump coke are fed into the top of the furnace while air is blown in from the bottom. The reducing gas generated from the lump coke and the blown air is blown from the bottom to the top of the furnace, reducing and dissolving the iron oxide in the raw ore. To ensure the ventilation of the reducing gas in the furnace, the raw ore must be strong enough not to be pulverized in the furnace. For this reason, blast furnaces usually use raw materials that have been fired at high temperatures in advance, such as sintered ore or fired pellets.
これに対し、セメントなどの水硬性バインダーを用いて焼成に必要なエネルギー消費を抑え、地球温暖化ガスである炭酸ガスの発生量を抑制する非焼成塊成鉱が開発されている。この非焼成塊成鉱の原料には、焼結性が低く、塊状に成型することが難しいとされてきた劣質な粉鉱石も用いることができる可能性がある。 In response to this, non-calcined agglomerates have been developed that use hydraulic binders such as cement to reduce the energy consumption required for calcination and reduce the amount of carbon dioxide, a greenhouse gas, produced. As the raw material for non-calcined agglomerates, it may be possible to use inferior fine ores that have been considered difficult to sinter and mold into agglomerates.
また、特許文献1に記載あるように、非焼成塊成鉱には、粒径が小さく高炉へ直接装入するのが困難な粉コークスや、価格は安いが粘結性が低くコークス化困難な無煙炭も還元材として配合できる可能性があり、高炉の還元材比を削減できると期待されている。最新の知見では、非焼成塊成鉱に内装されるカーボン含有率(T.C.)は、酸化鉄を還元して金属鉄とするために必要な理論炭素量の120~200質量%(T.C.換算で15~25質量%に相当)とすることで、高炉での還元材比低減効果が最大になることが明らかとなっている。 As described in Patent Document 1, it is possible to incorporate coke fines, which has a small particle size and is difficult to directly charge into a blast furnace, and anthracite, which is inexpensive but has low caking properties and is difficult to turn into coke, as reducing agents into non-calcined agglomerates, and it is expected that the reducing agent ratio in the blast furnace can be reduced. According to the latest findings, it is clear that the effect of reducing the reducing agent ratio in the blast furnace can be maximized by setting the carbon content (T.C.) incorporated in the non-calcined agglomerates to 120 to 200 mass% (equivalent to 15 to 25 mass% in T.C.) of the theoretical carbon amount required to reduce iron oxide to metallic iron.
水硬性バインダーの硬化反応により形成される非焼成塊成鉱中の水和物は、高炉内で約400℃以上に加熱されると吸熱反応により分解される。このため、非焼成塊成鉱の強度は炉内で著しく低下し、粉化する懸念がある。非焼成塊成鉱が高炉内で粉化すると、炉内の通気性を悪化させるため、高炉用非焼成塊成鉱には一定の熱間強度が求められる。一方で、熱間強度確保のために水硬性バインダーを大量に使うと、吸熱反応により奪われる熱を補填するために高炉への還元材投入量が増加し、溶銑コストが増加してしまう。 Hydrates in non-sintered agglomerates formed by the hardening reaction of hydraulic binders are decomposed by an endothermic reaction when heated to approximately 400°C or higher in a blast furnace. This causes the strength of non-sintered agglomerates to decrease significantly in the furnace, raising concerns that they may pulverize. If non-sintered agglomerates pulverize in a blast furnace, it will worsen the air permeability inside the furnace, so a certain level of hot strength is required for non-sintered agglomerates for blast furnaces. On the other hand, if a large amount of hydraulic binder is used to ensure hot strength, the amount of reducing material input to the blast furnace will increase to compensate for the heat lost by the endothermic reaction, which will increase the cost of molten iron.
以上より、非焼成含炭塊成鉱の製造方法では、なるべく少ない水硬性バインダーで高炉使用に必要な熱間強度を発現できる製造方法が求められている。 For these reasons, there is a demand for a manufacturing method for unsintered carbon-containing agglomerates that can achieve the hot strength required for blast furnace use with as little hydraulic binder as possible.
高炉使用に必要な熱間強度を発現できる製造方法として、最近では、真空押出成型法を用いた高炉用の非焼成含炭塊成鉱製造技術がある。 Recently, a manufacturing method that can achieve the hot strength required for blast furnace use has been developed that uses vacuum extrusion to produce unfired carbon-containing agglomerates for blast furnaces.
真空押出成型機は、図1の例に示すように第一の押出部(混練部)と第二の押出部(押出成型部)からなる。また第一の押出部(混練部)の出側から第二の押出部(押出成型部)までは、成型体の必要強度を確保するため―40kPaG以下に真空脱気され、真空押出成型を安定的に継続するためには、混練部と押出成型部の内部の混練原料充填率を適正範囲に維持する必要がある。なお、混練部の混練原料充填率の適正値は50体積%以上90体積%以下であり、50体積%以上65体積%以下であれば最適である。また、押出成型部の混練原料充填率の適正値は50体積%以上95体積%以下であり、50体積%以上60体積%以下であれば最適である。 As shown in the example of Figure 1, the vacuum extrusion molding machine consists of a first extrusion section (mixing section) and a second extrusion section (extrusion molding section). In addition, the area from the outlet of the first extrusion section (mixing section) to the second extrusion section (extrusion molding section) is vacuum degassed to -40 kPaG or less to ensure the necessary strength of the molded body, and in order to stably continue vacuum extrusion molding, it is necessary to maintain the mixing raw material filling rate inside the mixing section and the extrusion molding section within an appropriate range. The appropriate value for the mixing raw material filling rate of the kneading section is 50 volume% to 90 volume%, and optimally, 50 volume% to 65 volume%. The appropriate value for the mixing raw material filling rate of the extrusion molding section is 50 volume% to 95 volume%, and optimally, 50 volume% to 60 volume%.
ここで、押出成型部7の混練原料充填率の監視は、一般的に、作業者が真空室6上部に設置されている覗き窓10から実施している。しかし、真空室6内は大量の湿潤粉体の混練原料20が通過するため、その壁面に混練原料20が付着成長していく。この混練原料20の付着がある一定以上成長すると覗き窓10からの視野を塞いでしまい、押出成型部7を観察することができなくなる。この場合、操業を停止して真空室6内部を清掃する必要が発生し(数hr~十数hr)、設備の稼働率が低下する。 The filling rate of the raw material in the extrusion molding section 7 is generally monitored by an operator through a sight glass 10 installed at the top of the vacuum chamber 6. However, because a large amount of wet powder raw material 20 passes through the vacuum chamber 6, the raw material 20 adheres to the walls of the chamber and grows. When the adhesion of the raw material 20 grows beyond a certain level, it blocks the view from the sight glass 10, making it impossible to observe the extrusion molding section 7. In this case, it becomes necessary to stop operations and clean the inside of the vacuum chamber 6 (several hours to a dozen hours), which reduces the operating rate of the equipment.
これは、定期監視ができなくなると、混練原料充填率が95%を超えたのに気づかずに操業を続けて設備が過負荷停止したり、破損したりして長期の設備休止(十数hr~数day)を引き起こす懸念があるからである。さらに、真空室6壁面への混練原料20の付着が進行して真空室6が閉塞すると、混練堰4dから供給される混練原料が、押出成型部7に到達しなくなり、操業不可となる。この場合も内部清掃のために設備を止める必要がある。したがって、混練成型を安定的に継続するためには、真空室6壁面への混練原料20の付着を抑制する必要がある。なお、一般的に、本発明が対象とする真空押出成型装置は定期的に(十数hr~数dayごと)に内部を清掃するため、この清掃周期の間、付着を許容可能な範囲(内部観察可能なレベル)抑制できれば良い。 This is because if regular monitoring becomes impossible, there is a concern that the equipment will continue to operate without noticing that the raw material filling rate has exceeded 95%, causing overloading or damage, resulting in a long-term equipment shutdown (several tens of hours to several days). Furthermore, if the raw material 20 adheres to the wall of the vacuum chamber 6 and the vacuum chamber 6 becomes blocked, the raw material supplied from the kneading weir 4d will no longer reach the extrusion molding section 7, making operation impossible. In this case, the equipment must also be stopped for internal cleaning. Therefore, in order to continue kneading molding stably, it is necessary to suppress the adhesion of the raw material 20 to the wall of the vacuum chamber 6. In general, the vacuum extrusion molding device to which the present invention is directed is cleaned inside periodically (every tens of hours to several days), so it is sufficient to suppress adhesion to an acceptable range (a level at which the inside can be observed) during this cleaning cycle.
次に、真空室6壁面の付着抑制対策の難しさについて説明する。真空室6は、製品の品質確保に必要な真空脱気条件(≦-40kPaG)を維持するため、高い気密性が求められる。したがって、真空室6の壁面を覆うようにゴム板11などを取り付けたとしても、外部からゴム板11などを機械的な力で、または、流体(空気等)の送入による圧力等で脈動させることは困難である。また、比較的短い間隔で定期的(例えば、数hr毎)に真空室6を開放して清掃することは、稼働率低下につながるため避けたい。 Next, the difficulty of preventing adhesion to the walls of the vacuum chamber 6 will be explained. The vacuum chamber 6 is required to be highly airtight in order to maintain the vacuum degassing conditions (≦-40 kPaG) necessary to ensure product quality. Therefore, even if a rubber plate 11 or the like is attached to cover the walls of the vacuum chamber 6, it is difficult to pulsate the rubber plate 11 from the outside using mechanical force or pressure caused by the introduction of a fluid (air, etc.). In addition, it is desirable to avoid opening and cleaning the vacuum chamber 6 periodically at relatively short intervals (for example, every few hours) as this leads to a decrease in the operating rate.
よって、真空室6壁面の付着抑制には、真空室6外部から機械的、圧空等の力を加えることなく実施できる方法が必要である。さらに、本発明が対象とする混練原料20は、湿潤(水分数%~十数%)かつ微粉(例えば、≦100μm粉)を多量に含むため、装置壁面へ容易に付着する。 Therefore, in order to prevent adhesion to the walls of the vacuum chamber 6, a method is required that can be implemented without applying mechanical or compressed air forces from outside the vacuum chamber 6. Furthermore, the raw material 20 that is the subject of the present invention is wet (a few percent to a dozen percent moisture) and contains a large amount of fine powder (for example, powder of ≦100 μm), so it easily adheres to the walls of the device.
真空室6壁面は、従来、定期的(十数hr~数day)または付着成長を確認するごと(最短で定期清掃後数hr)に設備を止めて、作業者が清掃している。何らかの理由(原料の水分が高い、微粉分が多い等)により短期間(例えば、数hr)で清掃する必要が出た場合は、大きな作業負荷の増加と設備稼働率の低下につながってしまう。 Conventionally, the walls of the vacuum chamber 6 are cleaned by operators by shutting down the equipment periodically (every 10 hours to several days) or whenever adhesion growth is confirmed (at the earliest several hours after the regular cleaning). If cleaning becomes necessary in a short period of time (for example, several hours) due to some reason (high moisture content of raw materials, high fine powder content, etc.), this leads to a large increase in the workload and a decrease in the equipment operating rate.
そこで、様々な付着抑制策が検討されている。例えば、特許文献2~特許文献7のようにシュートやコンベア乗継部に設置したライナーやシートを何らかの方法で振動または揺動させる方法がある。 Therefore, various measures to prevent adhesion have been considered. For example, as described in Patent Documents 2 to 7, there is a method in which liners or sheets installed in chutes or conveyor transfer sections are vibrated or rocked in some way.
具体的なシートやライナーの動かし方としては、例えば、特許文献2、特許文献3のように、一部のみを固定したシートやライナーを外部から機械的に衝撃を加える方法がる。 Specific methods for moving the sheet or liner include, for example, a method in which a sheet or liner that is only partially fixed is mechanically impacted from the outside, as described in Patent Documents 2 and 3.
しかし、外部から機械的にシートを押しているため、真空室6では気密性が保持されず適用は困難である。また、振動発生装置や機械的に稼働する装置を新たに設置することは、装置スペース上困難だったり、粉塵固着により稼働装置がすぐに稼働できなくなる懸念が高かったりするため、現実的ではない。 However, because the sheet is mechanically pressed from the outside, the vacuum chamber 6 does not maintain airtightness, making this difficult to apply. In addition, it is not realistic to install new vibration generating devices or mechanically operated devices, as it would be difficult in terms of equipment space and there is a high concern that operating devices will soon become inoperable due to dust adhesion.
また、特許文献5~7のように装置内壁とシートまたはライナーの間に流体を出し入れしてシートまたはライナーを動かして付着物を剥落させる方法がある。 Also, as described in Patent Documents 5 to 7, there is a method in which a fluid is introduced between the inner wall of the device and the sheet or liner to move the sheet or liner and remove the deposits.
しかし、真空室内は真空脱気条件を維持するため強い負圧条件(おおよそ-100kPa~40kPa)であるため、真空室内に流体がリークすると大きな圧力変動で装置(真空室や押出成型装置だけではなく、真空ポンプ等の周辺設備を含む)が破損するおそれがあるため好ましくない。 However, the vacuum chamber is under strong negative pressure (approximately -100 kPa to 40 kPa) to maintain vacuum degassing conditions, so if fluid leaks into the vacuum chamber, the equipment (including not only the vacuum chamber and extrusion molding device, but also peripheral equipment such as the vacuum pump) may be damaged due to large pressure fluctuations, which is not desirable.
さらに、特許文献4では、コンベア乗り継ぎ部にて上端のみ固定したシート材を後方から支持し、前方から衝突してくるコンベア搬送原料の衝撃によりシート材が撓み、衝突してくる原料が付着しにくくなるようにしている。 Furthermore, in Patent Document 4, the sheet material, whose upper end is fixed only at the conveyor transfer section, is supported from the rear, so that the sheet material is deflected by the impact of the conveyor-transported raw material colliding with it from the front, making it difficult for the colliding raw material to adhere to it.
しかし、混練原料がほぼ垂直に落下する真空室6では、原料の衝突力のみではシート材を十分に撓ませることができず、本方法の付着抑制効果は十分ではない。 However, in the vacuum chamber 6 where the raw material falls almost vertically, the impact force of the raw material alone is not enough to bend the sheet material sufficiently, and the adhesion suppression effect of this method is not sufficient.
本発明に係る非焼成塊成鉱の混練成型について具体的な一例を説明する。粉体の混練成型では、混練部内に非焼成塊成鉱製造に必要な原料と、必要に応じて適度な水分を投入し、装置内の混練羽根やスクリューで粉体の混練原料を混練する。 A specific example of the kneading and molding of non-sintered agglomerates according to the present invention will be described below. In the kneading and molding of powder, the raw materials required for the production of non-sintered agglomerates and, if necessary, an appropriate amount of moisture are added to the kneading section, and the powdered raw materials are kneaded with the kneading blades and screws in the device.
その後、後工程の押出成型部にて当該混練原料を押出成型する。混練成型装置には様々なタイプがあるが、混練原料を連続的かつ大量(例えば数ton/hr以上)に混練成型する場合は、一般的に、前述の図1の例に示すような、水平に設置された1軸または多軸の混練シャフト4bに取り付けられた混練羽根4c(スクリューの場合もある)を用いて、混練原料20を水平方向に連続的に搬送しながら混練する形式の混練部4と、混練原料20を押出成型羽根7c(スクリューの場合もある)で押出成型堰7dから押し出して成型する形式の押出成型部7から成る非焼成塊成鉱混練成型機が使用されることが多い。なお、図1に示す例では押出成型部7はケーシング7aの内側で押出成型羽根7cにより混練原料が搬送されるが、この押出成型羽根7cは回転可能な押出成型部シャフト7bに備えられている。 The raw material is then extruded in the extrusion molding section in the subsequent process. There are various types of kneading and molding devices, but when kneading and molding raw materials continuously and in large quantities (for example, several tons/hr or more), a non-calcined agglomerate kneading and molding machine is often used, which is composed of a kneading section 4 that uses kneading blades 4c (sometimes a screw) attached to a horizontally installed single-shaft or multi-shaft kneading shaft 4b to continuously transport and knead the raw material 20 in the horizontal direction, and an extrusion molding section 7 that extrudes the raw material 20 from an extrusion molding weir 7d with an extrusion molding blade 7c (sometimes a screw) to mold it, as shown in the example in Figure 1. In the example shown in Figure 1, the extrusion molding section 7 transports the raw material by the extrusion molding blade 7c inside the casing 7a, and this extrusion molding blade 7c is provided on the rotatable extrusion molding section shaft 7b.
本発明は、高炉用の含炭塊成鉱などの真空押出成型装置において、真空室壁面への混練原料の付着を抑制できる容易かつ低コストな混練原料付着抑制方法およびその装置を提供する。 The present invention provides an easy and low-cost method and device for preventing adhesion of mixed raw materials to the vacuum chamber walls in a vacuum extrusion molding device for carbon-containing agglomerates for blast furnaces.
上記課題を解決するための真空押出成型装置の垂直真空室における混練原料の付着抑制方法は、
(1)非焼成塊成鉱用真空押出成型装置の垂直真空室内に、1乃至複数のゴムまたは樹脂製の長尺板を、垂直真空室上部に当該長尺板上端のみ固定し、かつ当該長尺板と垂直真空室内壁とは間隔を空けて垂下させ、前記垂直真空室内壁に混練原料が付着することを防止することを特徴とする。
A method for suppressing adhesion of a kneaded raw material in a vertical vacuum chamber of a vacuum extrusion molding apparatus for solving the above problems includes the following steps:
(1) In a vertical vacuum chamber of a vacuum extrusion molding apparatus for non-sintered agglomerates, one or more long rubber or resin plates are fixed at only their upper ends to the upper part of the vertical vacuum chamber, and the long plates are hung down with a gap between them and the vertical vacuum chamber inner wall, thereby preventing the raw materials from adhering to the vertical vacuum chamber inner wall.
また、
(2)(1)において、真空押出成型装置に設置されている混練シャフトの垂直真空室内部分には、前記長尺板と回転接触する回転羽根を設置し、これにより前記長尺板を叩き、前記長尺板に付着した混練原料を落下させることを特徴とする。
Also,
(2) In (1), a rotating blade that comes into rotating contact with the long plate is installed in the vertical vacuum chamber of the kneading shaft installed in the vacuum extrusion molding device, thereby striking the long plate and causing the kneaded raw material adhering to the long plate to fall.
また、
(3)(1)または(2)において、前記長尺板の下端は真空押出成型装置の混練堰の下端より下、かつ押出成型シャフト中央より上とすることを特徴とする。
Also,
(3) In (1) or (2), the lower end of the long plate is lower than the lower end of the kneading gate of the vacuum extrusion molding device and higher than the center of the extrusion molding shaft.
さらに、真空押出成型装置の垂直真空室における混練原料の付着抑制装置としては、
(4)非焼成塊成鉱用真空押出成型装置の垂直真空室内に、1乃至複数のゴムまたは樹脂製の長尺板が、垂直真空室上部に当該長尺板上端のみ固定され、かつ当該長尺板と垂直真空室内壁とは間隔を空けて垂下されていることを特徴とする。
Furthermore, as a device for suppressing adhesion of the kneaded raw material in the vertical vacuum chamber of the vacuum extrusion molding device,
(4) In a vertical vacuum chamber of a vacuum extrusion molding apparatus for non-sintered agglomerates, one or more long plates made of rubber or resin are fixed to an upper portion of the vertical vacuum chamber at only their upper ends, and the long plates are hung down with a gap between them and an inner wall of the vertical vacuum chamber.
さらに、
(5)(4)において、真空押出成型装置に設置されている混練シャフトの垂直真空室内部分には、前記長尺板と回転接触する回転羽根を設置されていることを特徴とする。
moreover,
(5) In the above (4), a rotating blade that comes into rotating contact with the long plate is installed in the vertical vacuum chamber of a kneading shaft installed in the vacuum extrusion molding device.
さらに、
(6)(4)または(5)において、前記長尺板の下端は真空押出成型装置の混練堰の下端より下、かつ押出成型シャフト中央より上に位置することを特徴とする。
moreover,
(6) In (4) or (5), the lower end of the long plate is located below the lower end of the kneading gate of the vacuum extrusion molding device and above the center of the extrusion molding shaft.
本発明により、真空押出成型装置の真空室の付着抑制方法およびその装置が提供され、真空室壁面への混練原料の付着を大幅に抑制できる、例えば十数hr以上の連続稼働を安定的に実施できるなど、稼働日が大幅に増加し、その技術的意義は大きい。 The present invention provides a method and device for suppressing adhesion in the vacuum chamber of a vacuum extrusion molding device, which can significantly suppress adhesion of mixed raw materials to the walls of the vacuum chamber, allowing stable continuous operation for more than 10 hours, for example, and significantly increasing the number of operating days, which is of great technical significance.
以下に発明を実施するための形態を示す。 The following is a form for implementing the invention.
本発明では、真空室6内壁に上端のみ固定して設置する1乃至複数のゴム板等11(天然ゴム板、合成ゴム板、薄い樹脂板、その他可撓性があるシートやライナー等)の長尺板と、さらに好ましくは混練シャフト4bの真空室6部分に設置してゴム板等11の付着原料をそぎ落としつつゴム板等11全体を脈動させてゴム板等11全体の付着原料を剥落させる機能を持つ回転羽根12とにより、真空室6壁面への混練原料の付着を抑制する方法を提供する。 The present invention provides a method for preventing the adhesion of raw materials to the walls of the vacuum chamber 6 by using one or more long rubber plates 11 (natural rubber plates, synthetic rubber plates, thin resin plates, other flexible sheets or liners, etc.) fixed to the inner wall of the vacuum chamber 6 with only their upper ends fixed thereto, and more preferably by using a rotating blade 12 that is installed in the vacuum chamber 6 portion of the kneading shaft 4b and has the function of scraping off the raw materials adhering to the rubber plates 11 while pulsating the entire rubber plates 11, causing the raw materials adhering to the entire rubber plates 11 to peel off.
なお、本技術の混練部4付近の構造の例は図1に示した通りであり、ミキサ1から送られた混練原料20が混練原料投入口2に投入される。混練原料投入口2に投入された混練原料20は接続管3を通って混練部4へと導かれ、シャフト4bに備えられた混練羽根4cなどを用いて混練される。混練原料が押し出される堰4dの手前には混練原料圧密部4eが設けられている。また、混練部4の上部にはグレーチングなどの内部観察部4fが設けられており、この部分を通して加水ノズル5よりケーシング4a内の混練原料20に散水できる。混練部4の先には押出成型部7に続く真空室6が設けられており、この真空室6には真空ポンプ接続管9を介して真空ポンプ8が接続されている。覗き窓10はこの真空室6の上部に設けられている。以下で、真空室6に設けたゴム板等11と回転羽根12について説明する。 An example of the structure near the kneading section 4 of this technology is as shown in FIG. 1, where the raw material 20 sent from the mixer 1 is fed into the raw material inlet 2. The raw material 20 fed into the raw material inlet 2 is led to the kneading section 4 through the connecting pipe 3, and is kneaded using the kneading blades 4c and other components provided on the shaft 4b. A raw material compaction section 4e is provided in front of the weir 4d from which the raw material is pushed out. In addition, an internal observation section 4f such as a grating is provided at the top of the kneading section 4, and water can be sprayed from the water-adding nozzle 5 through this section onto the raw material 20 in the casing 4a. A vacuum chamber 6 leading to the extrusion molding section 7 is provided beyond the kneading section 4, and a vacuum pump 8 is connected to this vacuum chamber 6 via a vacuum pump connection pipe 9. A viewing window 10 is provided at the top of this vacuum chamber 6. Below, a rubber plate or the like 11 and a rotating blade 12 provided in the vacuum chamber 6 will be described.
1)ゴム板等11について
図2に、真空室6内の混練原料の付着状況の概略を示す。真空室6内部において混練原料20が付着した付着混練原料21は、混練堰4dに対して左右の壁面(左右壁面)で最も著しい。これは、混練堰4dから排出される混練原料20が左右に広がるように落下するからである。特に、混練堰4d中央~下端に範囲に相当する位置の左右壁面は、混練堰4dから排出される微粉原料や水蒸気が飛散して付着しやすく、混練原料20の付着成長が全ての壁面の中で最も顕著である。
1) Rubber plates, etc. 11 Fig. 2 shows an outline of the adhesion state of the raw material in the vacuum chamber 6. The adhering raw material 21 to which the raw material 20 adheres inside the vacuum chamber 6 is most noticeable on the left and right wall surfaces (left and right wall surfaces) of the kneading weir 4d. This is because the raw material 20 discharged from the kneading weir 4d falls so as to spread out to the left and right. In particular, the left and right wall surfaces at the position corresponding to the range from the center to the lower end of the kneading weir 4d are prone to adhesion due to scattering of fine powder raw material and water vapor discharged from the kneading weir 4d, and the adhesion and growth of the raw material 20 is most noticeable on all the wall surfaces.
一方で、常に大量の混練原料20が通過する真空室6の混練堰4d側壁面(入側壁面)と、混練堰4dから比較的距離がある出側壁面(入側壁面と向かい合う面)は付着原料が比較的少ない。したがって、真空室6壁面の付着対策は、左右壁面で最も必要とされ、ゴム板等11は少なくとも左右壁面の2か所に設置するのが望ましい。 On the other hand, the wall surface (entrance side wall surface) of the vacuum chamber 6 facing the kneading weir 4d, through which a large amount of raw material 20 always passes, and the outlet side wall surface (the surface facing the inlet side wall surface) that is relatively far from the kneading weir 4d, have relatively little raw material adhering to them. Therefore, measures to prevent adhesion to the wall surfaces of the vacuum chamber 6 are most necessary on the left and right walls, and it is desirable to install rubber plates, etc. 11 in at least two places on the left and right walls.
なお、入側壁面や出側壁面へゴム板等11を設置しても良く、設置する場合は混練堰4dや混練シャフト4bを避けるようにゴム板等11の形状を加工すれば良い。 In addition, rubber plates or the like 11 may be installed on the inlet wall surface or the outlet wall surface. If they are installed, the shape of the rubber plates or the like 11 may be processed so as to avoid the kneading weir 4d and the kneading shaft 4b.
2)付着混練原料
図3にゴム板等11の設置方法を示す。ゴム板等11は1乃至複数で構成され、1枚のゴム板等11に複数の切れ目またはスリットを入れて複数垂下するような形態としても構わない。このゴム板等11は上端のみで真空室6内壁に固定され、その他の部分はフリー(真空室6内壁に固定していない)である。尚、前記上端は完全に上端でなくても構わず、状況に応じて数mm~数十mm程度上端から下がった上端部であっても構わない。
2) Attached raw material to be kneaded Fig. 3 shows a method of installing the rubber plate 11. One or more rubber plates 11 may be used, and a single rubber plate 11 may have multiple cuts or slits to hang down. This rubber plate 11 is fixed only at its upper end to the inner wall of the vacuum chamber 6, and the other part is free (not fixed to the inner wall of the vacuum chamber 6). The upper end does not have to be completely the upper end, and may be an upper end part that is lower than the upper end by several mm to several tens of mm depending on the situation.
ゴム板等11の詳細については後述するが、このゴム板等11を設置するだけでも、落下する混練原料20はゴム板等11に衝突し、その衝撃でゴム板等11に付着した付着混練原料21が剥落するので、一定の効果が発生する。さらに後述する回転羽根12の接触によってゴム板等11を脈動させ、ゴム板等11上の付着混練原料21を剥落させれば、より大きな効果が得られる。 Details of the rubber plate 11 will be described later, but simply installing this rubber plate 11 will have a certain effect, as the falling raw material 20 collides with the rubber plate 11 and the raw material 21 adhering to the rubber plate 11 falls off due to the impact. Furthermore, if the rubber plate 11 is pulsated by contact with the rotating blades 12 (described later) and the raw material 21 adhering to the rubber plate 11 falls off, an even greater effect can be obtained.
以下、本発明について詳細に説明する。ゴム板等11が脈動するためには、真空室6内壁とゴム板等11との間には間隙(例えば、数mm~数十mm程度、真空室6の容量も考慮して、真空室6内壁と5~50mm程度の間隔が好ましい)を設ける必要がある。 The present invention will be described in detail below. In order for the rubber plate or the like 11 to pulsate, it is necessary to provide a gap (for example, a few mm to a few tens of mm; taking into account the capacity of the vacuum chamber 6, a gap of about 5 to 50 mm from the inner wall of the vacuum chamber 6 is preferable) between the rubber plate or the like 11 and the inner wall of the vacuum chamber 6.
次に、ゴム板等11の固定位置(上端)と下端の上下限について説明する。ゴム板等11上端の固定位置(上端)の下限は、混練シャフト4b中央より高い位置である。これは、原料付着が最も著しい位置(混練堰4d中央~下端)をカバーするためである。 Next, the upper and lower limits of the fixed position (upper end) and lower end of the rubber plate, etc. 11 will be explained. The lower limit of the fixed position (upper end) of the upper end of the rubber plate, etc. 11 is higher than the center of the kneading shaft 4b. This is to cover the position where the raw material adhesion is most severe (from the center to the lower end of the kneading weir 4d).
ゴム板等11の固定位置(上端)の上限は設備の構造上、真空室6上端になる。この範囲内(混練シャフト4b中央~真空室6上端)であれば、ゴム板等11上端の固定位置(上端)は任意で決めてよいが、回転羽根12がゴム板等11の固定と接触し装置が破損するリスクの低減や、壁面への混練原料20の付着抑制を考慮すると、固定位置(上端)は真空室6上端~混練堰4d上端の範囲にすることがより好ましい。 Due to the structure of the equipment, the upper limit of the fixed position (upper end) of the rubber plate, etc. 11 is the upper end of the vacuum chamber 6. The fixed position (upper end) of the upper end of the rubber plate, etc. 11 may be determined arbitrarily as long as it is within this range (from the center of the kneading shaft 4b to the upper end of the vacuum chamber 6), but considering the reduction of the risk of the rotating blades 12 coming into contact with the fixed rubber plate, etc. 11 and damaging the device, and the prevention of adhesion of the raw material 20 to the wall surface, it is more preferable to set the fixed position (upper end) in the range from the upper end of the vacuum chamber 6 to the upper end of the kneading weir 4d.
次に、ゴム板等11の下端の位置について説明する。ゴム板等11の下端は、最低でも、混練堰4dの下端より下でなければならない。これは、上述のように、混練堰4d中央~下端に相当する壁面に最も混練原料20が付着しやすいからである。 Next, the position of the bottom end of the rubber plate 11 will be explained. The bottom end of the rubber plate 11 must be at least lower than the bottom end of the kneading weir 4d. This is because, as mentioned above, the raw material 20 is most likely to adhere to the wall surface corresponding to the center to the bottom end of the kneading weir 4d.
一方で、ゴム板等11の下端は、押出成型シャフト7b中央より上に位置することが望ましい。これは、ゴム板等11が押出成型羽根7cや押出成型シャフト7bの回転に巻き込まれて破損するのを防止するためである。ゴム板等11の下端位置は、この範囲(混練堰4d下端~押出成型シャフト7b中央)で任意に決めてよい。 On the other hand, it is desirable that the lower end of the rubber plate 11 be located above the center of the extrusion shaft 7b. This is to prevent the rubber plate 11 from being caught in the rotation of the extrusion blade 7c or the extrusion shaft 7b and being damaged. The position of the lower end of the rubber plate 11 may be determined arbitrarily within this range (the lower end of the kneading weir 4d to the center of the extrusion shaft 7b).
ここで、ゴム板等11の材質は、天然ゴム、合成ゴム、薄い樹脂、その他可撓性があるシートやライナーであれば特に制限はない。ゴム板等11は継ぎ目やその他の凹凸が無い一体物がより好ましい。これは、ゴム板等11に凹凸部分があれば、そこが混練付着原料21の起点となりやすいからである。 The material of the rubber plate 11 is not particularly limited as long as it is natural rubber, synthetic rubber, thin resin, or any other flexible sheet or liner. It is preferable that the rubber plate 11 is a one-piece material without seams or other irregularities. This is because if the rubber plate 11 has irregularities, these will likely become the starting points for the kneaded and attached raw material 21.
本発明のゴム板等11は、メンテナンス性にも優れている。本ゴム板等11は、真空室6上部を開放することで容易に装置外に取り外すことができ、清掃することができる。これは、本ゴム板等11が上端のみで固定されているため、上端固定部のみを外せば、真空室6上部から引き揚げ可能だからである。通常、真空室6の下部は強固なライナーで覆われており、大きな点検窓の設置は難しいため、真空室6下部でゴム板等11を固定してしまうと取り外しに大きな時間と労力がかかってしまう。一方で、一般的に、真空室6の上部は点検や清掃のために開放できる構造になっている。 The rubber plate 11 of the present invention is also easy to maintain. The rubber plate 11 can be easily removed from the device by opening the top of the vacuum chamber 6, and can be cleaned. This is because the rubber plate 11 is fixed only at the top end, and can be lifted up from the top of the vacuum chamber 6 by removing only the top fixing part. Usually, the bottom of the vacuum chamber 6 is covered with a strong liner, and it is difficult to install a large inspection window, so if the rubber plate 11 is fixed at the bottom of the vacuum chamber 6, it takes a lot of time and effort to remove it. On the other hand, the top of the vacuum chamber 6 is generally designed to be openable for inspection and cleaning.
3)回転羽根12について
本発明の好ましい形態の一つである回転羽根12およびその使用について説明する。回転羽根12の形状は任意であり、ゴム板等11に周期的に衝撃を与えられる構造になっていればよい。
3) Rotating blade 12 The rotating blade 12, which is one of the preferred embodiments of the present invention, and its use will be described. The shape of the rotating blade 12 is arbitrary, and it is sufficient that the blade has a structure that can apply impact periodically to the rubber plate 11 or the like.
ここで、回転羽根12のうち、ゴム板等11が接触する先端部分については、幅が広いほうがより好ましい。これは、回転羽根12の先端がゴム板等11に接触するときに、ゴム板等11を脈動させて付着混練原料21を剥落させるのみならず、ゴム板等11上の付着混練原料21をそぎ落とす効果も期待できるためである。 Here, it is preferable that the tip portion of the rotating blade 12 that comes into contact with the rubber plate or the like 11 is wider. This is because when the tip of the rotating blade 12 comes into contact with the rubber plate or the like 11, not only does it pulsate the rubber plate or the like 11 to cause the adhering raw material 21 to peel off, but it is also expected to have the effect of scraping off the adhering raw material 21 on the rubber plate or the like 11.
一方で、回転羽根12のうちゴム板等11と接触する部分以外の面積は、必要な構造強度を保持できる範囲でなるべく小さい方が好ましい。これは、作業者が覗き窓10から観察するときの視認性を向上させるためである。回転羽根12の枚数については、少なくとも1枚以上必要である。一方で、回転羽根12の枚数が多いと、覗き窓10から作業者が真空室6内部や押出成型部7を監視するときに、回転羽根12が作業者の視野に干渉しやすくなるため、監視作業が難しくなる。さらに、回転羽根12自体が混練シャフト4bへの混練原料付着の起点となる懸念がある。したがって、回転羽根12は少ないほうが好ましい。調査の結果、回転羽根12は1~4枚程度が最も好ましい。 On the other hand, it is preferable that the area of the rotating blades 12 other than the part that contacts the rubber plate or the like 11 is as small as possible within the range that maintains the necessary structural strength. This is to improve visibility when the worker observes through the sight window 10. At least one or more rotating blades 12 are required. On the other hand, if there are a large number of rotating blades 12, the rotating blades 12 tend to interfere with the field of view of the worker when monitoring the inside of the vacuum chamber 6 or the extrusion molding section 7 through the sight window 10, making the monitoring work difficult. Furthermore, there is a concern that the rotating blades 12 themselves may become the starting point for the adhesion of the raw material to be kneaded to the kneading shaft 4b. Therefore, it is preferable to have fewer rotating blades 12. As a result of the investigation, it is most preferable to have about 1 to 4 rotating blades 12.
ここで、回転羽根12のサイズについては、真空室6内で回転可能なサイズ以内であれば良く、少なくともゴム板等11に衝撃を与えられる程度のサイズ(最低でもゴム板等11に接するサイズ)があれば良い。 The size of the rotating blades 12 need only be within a size that allows them to rotate within the vacuum chamber 6, and at least be large enough to impact the rubber plate 11 (at least large enough to come into contact with the rubber plate 11).
図4に回転羽根12の例を4例、示す。尚、回転羽根12は、この4例に限る必要は無い。図4の1)は平板状の回転羽根12が1枚設置されている。図4の2)と3)は、円柱状または角柱状の回転羽根12がそれぞれ、2本、4本取り付けられている。図4の4)は、ゴム板等11と接触する部分のみを幅広にした特殊形状の回転羽根12であり、回転羽根12とゴム板等11の接触時に付着混練原料21のそぎ落とし効果を享受しつつ、作業者の目視監視時の視認性を高めている。 Figure 4 shows four examples of the rotating blades 12. However, the rotating blades 12 are not limited to these four examples. 1) in Figure 4 has one flat rotating blade 12 installed. 2) and 3) in Figure 4 have two and four cylindrical or prismatic rotating blades 12 installed, respectively. 4) in Figure 4 is a rotating blade 12 with a special shape in which only the part that comes into contact with the rubber plate or the like 11 is widened, which has the effect of scraping off the adhering raw material 21 when the rotating blade 12 comes into contact with the rubber plate or the like 11, while also improving visibility when the worker visually monitors.
なお、真空室6の入側壁面と出側壁面にゴム板等11を設置した場合は、回転羽根12でゴム板等11に衝撃を与えることは難しいが、入側壁面と出側壁面への混練原料20の付着は左右面に比べて少ないので、混練原料20がゴム板等11に衝突して発生する程度の脈動で十分に混練原料20の付着を抑制すことができる。 When rubber plates or the like 11 are installed on the inlet and outlet walls of the vacuum chamber 6, it is difficult for the rotating blades 12 to impact the rubber plates or the like 11. However, the adhesion of the raw material 20 to the inlet and outlet walls is less than that to the left and right walls. Therefore, the adhesion of the raw material 20 to the inlet and outlet walls can be sufficiently suppressed by the pulsation generated by the raw material 20 colliding with the rubber plates or the like 11.
本発明では、混練シャフト4bに設置する回転羽根12を用いることにより、真空室6の外部からゴム板等11に衝撃を加えるような機構が無くてもゴム板等11に力を加えることができる。したがって、真空室6の気密性を維持したままゴム板等11を脈動させることができる。また、回転羽根12自体は小さくすることができ真空室6の限られたスペースに十分に導入でき、設置および維持にかかるコストも小さい。 In the present invention, by using the rotating blades 12 installed on the kneading shaft 4b, it is possible to apply force to the rubber plate 11, etc., without a mechanism that applies an impact to the rubber plate 11 from outside the vacuum chamber 6. Therefore, it is possible to pulsate the rubber plate 11 while maintaining the airtightness of the vacuum chamber 6. In addition, the rotating blades 12 themselves can be made small, so they can be easily installed in the limited space of the vacuum chamber 6, and the costs of installation and maintenance are low.
以上のゴム板等11と回転羽根12による簡易かつ低コストで導入可能な付着防止方法により、真空室6壁面への原料付着を抑制することができ、真空押出成型を安定継続することができる。 The above-mentioned anti-adhesion method using rubber plates 11 and rotating blades 12 can be easily and inexpensively implemented to prevent the raw material from adhering to the walls of the vacuum chamber 6, allowing for stable and continuous vacuum extrusion molding.
図5に実施例を示す。図5の1)は操業前のゴム板等11の設置状態である。図5の2)、3)は操業中の真空室6の状態で、3)は回転羽根12がゴム板等11に接触し、衝撃を与えている瞬間である。尚、図5は、前述の図4の1)の回転羽根12が1枚取り付けられた形態で、毎分20~30回転している。 Figure 5 shows an example. 1) in Figure 5 shows the state in which the rubber plate 11 is installed before operation. 2) and 3) in Figure 5 show the state of the vacuum chamber 6 during operation, and 3) shows the moment when the rotating blade 12 comes into contact with the rubber plate 11 and gives an impact. Note that Figure 5 shows the configuration in which one rotating blade 12 is installed as in 1) of Figure 4 above, and is rotating at 20 to 30 revolutions per minute.
1 ミキサ
2 投入口
3 接続管
4 混練部
4a ケーシング
4b 混練シャフト
4c 混練羽根
4d 混練堰
4e 混練原料圧密部(堰手前で混練原料が圧密され、混練が特に顕著に実施される場所)
4f 混練機上面の内部観察部(グレーチング、ガラス窓、開口等)
5 加水ノズル
6 真空室
7 押出成型部
7a ケーシング
7b 押出成型シャフト
7c 押出成型羽根
7d 押出成型堰
8 真空ポンプ
9 真空ポンプ接続管
10 覗き窓
11 ゴム板等
12 回転羽根
20 混練原料
REFERENCE SIGNS LIST 1 Mixer 2 Feeding port 3 Connecting pipe 4 Kneading section 4a Casing 4b Kneading shaft 4c Kneading blade 4d Kneading weir 4e Kneading raw material consolidation section (where the raw material is consolidated before the weir and kneading is particularly prominently performed)
4f Internal observation section on the top of the kneader (grating, glass window, opening, etc.)
5 Water adding nozzle 6 Vacuum chamber 7 Extrusion molding section 7a Casing 7b Extrusion molding shaft 7c Extrusion molding blade 7d Extrusion molding gate 8 Vacuum pump 9 Vacuum pump connection tube 10 Sight window 11 Rubber plate, etc. 12 Rotating blade 20 Raw material to be kneaded
Claims (4)
真空押出成型装置に設置されている混練シャフトの垂直真空室内部分には、前記長尺板と回転接触する回転羽根を設置し、
これにより前記長尺板を叩き、前記長尺板に付着した混練原料を落下させることを特徴とする真空押出成型装置の垂直真空室における混練原料の付着抑制方法。 In a vertical vacuum chamber of a vacuum extrusion molding apparatus for non-calcined agglomerates, one or more long rubber or resin plates are fixed at only the upper ends of the long plates to an upper portion of the vertical vacuum chamber, and the long plates are hung down with a gap between them and a wall of the vertical vacuum chamber to prevent the raw material to be kneaded from adhering to the wall of the vertical vacuum chamber ;
A rotating blade that is in rotational contact with the long plate is installed in a vertical vacuum chamber of a kneading shaft installed in a vacuum extrusion molding device,
This method for suppressing adhesion of kneaded raw material in a vertical vacuum chamber of a vacuum extrusion molding device is characterized in that the long plate is struck and the kneaded raw material adhering to the long plate falls .
真空押出成型装置に設置されている混練シャフトの垂直真空室内部分には、前記長尺板と回転接触する回転羽根を設置されていることを特徴とする真空押出成型装置の垂直真空室における混練原料の付着抑制装置。 In a vertical vacuum chamber of the vacuum extrusion molding apparatus for non-calcined agglomerates, one or more long rubber or resin plates are fixed at only their upper ends to an upper portion of the vertical vacuum chamber, and the long plates are hung down with a gap between them and an inner wall of the vertical vacuum chamber ;
A device for suppressing adhesion of kneaded raw materials in a vertical vacuum chamber of a vacuum extrusion molding device, characterized in that a rotating blade that rotates and comes into contact with the long plate is installed in the vertical vacuum chamber portion of a kneading shaft installed in the vacuum extrusion molding device.
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| WO2017140832A1 (en) | 2016-02-18 | 2017-08-24 | Nordic Elements Ab | Process for producing molybdenum-containing units |
| JP2020200489A (en) | 2019-06-06 | 2020-12-17 | 日本製鉄株式会社 | Manufacturing method of non-calcined coal-containing mass ore for blast furnace and manufacturing apparatus |
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| JPS61130428A (en) * | 1984-11-30 | 1986-06-18 | Nippon Kokan Kk <Nkk> | Production of mini-briquette |
| JPH0285190A (en) * | 1988-09-21 | 1990-03-26 | Nippon Shinkinzoku Kk | Transfer pipe |
| JPH07410Y2 (en) * | 1990-05-24 | 1995-01-11 | 住金鹿島鉱化株式会社 | Raw material supply chute for vertical roller mill |
| JP2660498B2 (en) * | 1995-06-12 | 1997-10-08 | 住金鹿島鉱化株式会社 | Vertical roller mill |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2017140832A1 (en) | 2016-02-18 | 2017-08-24 | Nordic Elements Ab | Process for producing molybdenum-containing units |
| JP2020200489A (en) | 2019-06-06 | 2020-12-17 | 日本製鉄株式会社 | Manufacturing method of non-calcined coal-containing mass ore for blast furnace and manufacturing apparatus |
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