JP4465675B2 - Production method of chlorophyll solute - Google Patents

Description

  The present invention relates to a method for producing a solute solution for extracting plant chlorophyll from leaves and stems of sweet tea, wasabi, and the like using alcohol, and a partition with a light emitting diode that recycles the residual squeezed.

  Generally, it is said that the leaves and stems of plants do not contain nutrients, but in fact, the chlorophyll contained in the leaves and stems of plants contains considerable nutrients, and human skin Some moisturize the skin. That is, leaves and stems have a lot of enzyme starch on the leaf surface by photosynthesis. Leaves from sweet tea, Apios, wasabi, and white sweet potato are sweeter than dark green tea and are sweetened by thermal decomposition. The highest quality green liquor is recovered if the leaf stems are distilled before and after the harvesting period.

  In other words, rich green tea is astringent during the late summer to autumn harvest season, but can be corrected by the distillation method. Alcohol extraction of green pigments in plant leaves and stems is already known, but green liquor is an alcoholic extract of leaf stems such as candy tea leaves, Apios, horseradish, white sweet potatoes, and potatoes. It was not possible with conventional methods. That is, in conventional high-pressure distillation and reduced-pressure distillation, if the time in the container is long, it becomes brownish gray and loses green color, and the purpose of the present application cannot be achieved.

  In the present invention, the leaves and stems of plants are poured into alcohol to form a mixed solution, which is evaporated and diffused to reduce the alcohol content to a required ratio and retained, and the extracted solute solution that is an innocuous extract is obtained. As a basic material liquid, it can be widely used for various purposes such as confectionery, noodles, health foods, drinking water, bathing liquid, pharmaceuticals, food processing, marine products processing, industrial paints.

  The green solute obtained by extracting chlorophyll, as in the past, is expensive in high-pressure distillation or reduced-pressure distillation for recovering the extract, and it becomes brown when the time is prolonged in the container. As a result, the steam-cooled extract has a problem that even if the alcohol component and the aqueous solution can be recovered, the green solute extracted from chlorophyll, which is the object of the present application, cannot be obtained. .

  The problem to be solved by the present invention is that, from the leaves and stems of plants that are conventionally considered not to contain nutrients, actually extract chlorophyll containing significant nutrients, Obtain green powder for drinking water, food processing, bathing solution containing soap shampoo, health pillow, and residual squeezed after solute extraction to recycle and reuse for antibacterial and deodorant products is there.

  That is, after a pretreatment process peculiar to the present plan is applied to the leaves and stems of plants, the alcohol component is evaporated and diffused using an induction current heating apparatus, and a green solute solution is extracted from chlorophyll having a specific content of alcohol component. It can be obtained, and the evaporation and diffusion of the alcohol component is surely free from danger and has no danger of electric power. The recovered liquid is effective for various kinds of drinking water and food processing.

  In the present invention, when extracting chlorophyll from leaves, stems, and roots of plants, the stems and roots are powdered with a moisture content of 30% by hand and placed in a copper container. In the case of astringency, after heating to 71 ° C. to 82 ° C., it is sandwiched between rice straw and fermented to give coarse powder, which is a 15% to 20% dry powder that does not reduce chlorophyll chromaticity. The solute solution obtained by immersing and precipitating as a mixed solution of 700 cc of alcohol with respect to 100 g of the coarse powder and extracting chlorophyll after taking out the residue is used as a stock solution mixture.

  Next, 800 cc of diluted water is added to 100 cc of this stock solution, and this is distilled and diffused by induction current heat to remove the alcohol component, and the residual mixture having an alcohol content of 0.3 degrees or less, ie, extracted chlorophyll color Obtain 220 cc of liquid. Furthermore, it is a product as a clear and transparent green liquid from which the brown lignin that has been polluted is removed by a filter to extract chlorophyll, and it is commercialized, improving blood flow, hypertension, diabetes, etc., food processing, health food, It is characterized in that it is used for health drinks, bathing liquids, etc., and the undiluted liquid mixture is distilled from the process of obtaining mixed solute liquid called wood squeezed liquid and bamboo squeezed liquid from which extracts from wood are extracted. After diffusion, it is filtered to produce a clear and transparent green liquid.

  Furthermore, the residual squeezed after extraction of the above mixed solute solution is reprocessed and reused to make a health partition with a light emitting diode combination that has antibacterial, deodorant, moisture, and dew condensation prevention effects. It is what.

  In the present invention, chlorophyll containing nutrients is extracted from the leaves and stems of plants as an inductive current heater as a green solute having an alcohol component frequency of 0.3 ° or less, and filtered to sufficiently contain chlorophyll. A clear and clear nutrient green liquid is obtained, which is effective for improving blood circulation, hypertension, diabetes, diuresis, constipation, atopic dermatitis and other health foods, health drinks, bathing liquids, etc. Recycled residual squeezed and obtained the effect of providing a health screen for antibacterial, deodorant, anti-condensation, and ventilation that incorporates a light emitting diode and serves as a light source.

  Plant chlorophylls in leaves and stems contain nutrients, and are used for sweet tea (snow lower family), apios, wasabi, amachazul, kumamushi, white sweet potato, blue purple su, Chinese herb, herb, black letter leaf, etc. The green leaves of the front and rear are vividly produced by the thermal decomposition process according to the present invention, so the sweetness is strong, gentle to the human skin, moisturizes the skin, and is sensitive and effective for children with atopic disease. There is nothing that is good, internal or external. Sweet saccharides were produced by thermal decomposition, and as a result, green liquefaction could be achieved without using chemical additives as in the past, and harmless extracts could be extracted.

  That is, when the leaves and stems are put in a copper container and the temperature is gradually raised, the sweetness and green color are improved, and when 5 to 7 mm chrome steel grains are mixed, the sweetness and green color are further improved. If it becomes thin and easy to drink, and it is used as a bath solution, even if the child contains it in the mouth, the effect of bathing is obtained without bitterness.

  According to the thermal decomposition process of the present invention, the sweet sugar is most often sweet tea (snow lower family), followed by Apios, white sweet potato, amachazuru, kumaimo, and wasabi. Most of the side dishes were blue shiso and others.

  The thermal decomposition step of the present invention is carried out as a pretreatment of plant chlorophyll leaves and stems with alcohol permeation, and uses a copper container in which green is strongly produced, and the container temperature is 50 to 90 degrees, that is, 50 ° C. in the case of sweetness. ~ 70 ° C, in the case of astringency, heat to 71 ° C to 82 ° C, and treat with a gentle atmosphere to increase the sweetness of the leaves and stems before and after the setting period. And sort. The sweetness from the leaf enzymes improves before and after the arrival period.

  As shown in FIG. 1, the thermal decomposition process of the present invention is held by a frame (1), and a heater (4) for heating is provided below a copper container (3) in which a temperature sensor (2) is set. In this case, the hand-held leaf stem (a) is placed in a copper container (3) and heated, and is divided into sweetness and astringency by adjusting the temperature. In this case, 100 sheets (115 g) having a leaf diameter of 10 cm or more and a width of 7 cm or more before and after the landing stage are washed with water, frozen after removing water droplets, and immediately after thawing, placed in a copper container and processed at a required temperature. That is, the temperature heat which is the copper plate temperature of the copper container at this time selects the range of 80 degrees to 90 degrees for producing tea astringency and the range of 40 degrees to 70 degrees for producing sweetness such as various drinking water. In this work process, squeezing with both hands, gradually increasing the temperature so as to make it mellow, heat it up and down, keeping it at the upper limit of the temperature range, and taking out the leaves and stems at the lower limit temperature of 60 degrees.

  Fig. 2 shows a fermentation apparatus for improving the olfactory taste. When the stalks of leaf stems (a) and rice straw (b) are alternately stacked in multiple stages in a container and fermented for three days and three nights, The scent and taste are improved without any discoloration by the action of microorganisms. FIG. 3 shows that a glass container (5), which is immersed in alcohol for extracting chlorophyll, has no chemical reaction, and is immersed and precipitated for one week as a mixture of 700 cc of alcohol with respect to 100 g of the coarse powder of leaf stem (a). A recovered solute solution (c) is obtained.

  FIG. 4 shows a distillation diffusion apparatus, in which a mixed liquid tank (7) heated by an induction current heater (6) is installed, and a steam suction pipe (8) leading to a vacuum pump is connected to the apparatus, which is necessary. In response to this, the inside of the apparatus is vacuumed to evaporate the alcohol, and the recovered solute solution (c) is placed in the mixed solution tank (7), and derived from the original solution solute solution in which 800 cc of diluted water is added to 100 cc. The current heat is adjusted to a required temperature and heated to evaporate the alcohol to obtain 220 cc of a solute solution containing chlorophyll having an alcohol content of 0.3 degrees or less.

  The brown lignin contaminated from the solute solution is removed by a filter to obtain a clear and transparent green solute solution. FIG. 5 shows a lignin removing cylinder (A) and a phenol removing cylinder (B) which are filtered by a filter. The lignin removing cylinder (A) for injecting a solute liquid, a wood squeezed liquid and a bamboo squeezed liquid from above is partitioned from above. Then, the ceramic sphere (I), diatomaceous earth (B), activated carbon (C), and ion resin exchange membrane (D) are laminated in this order, and the phenol removal cylinder that instills the liquid passing through the lignin removal cylinder (A) from above. (B) is formed by stacking activated carbon (e), a neutral ion ion resin exchange membrane (f), and a negative ion ion resin exchange membrane (g) by dividing each funnel from the top.

  Fig. 6 shows a screen using the residue, surrounded on three sides by a frame plate partially provided with an exhaust fan, and one side as a door sliding door provided with an intake fan. Charcoal bamboo charcoal adjustment charcoal (q) and diatomaceous earth particle size silica (r) are laminated and filled, and fumigation bamboo (s) is attached to the front and back surfaces. The hinokitiol solution and camphor fluid are injected from the upper funnel, which has a decorative property, antibacterial property and good odor adsorption, and can provide a screen that helps to eliminate Six House Syndrome in room air. The light-emitting diode (9) is projected on the shoji screen and is well-lighted, and is well ventilated by a ventilation fan, doubles as a room interior, and also supplements the lack of sunshine for agriculture.

  FIG. 7 shows a fumigation bamboo manufacturing apparatus in which a large number of bamboo materials (t), such as Takemune bamboo and Shinotake, are placed on a cylindrical rotary fence (12) in a fumigation chamber (11) equipped with several temperature sensors (10). The bark combustion material (u) on the lower grate is burned, and the bark fuel is replenished from the replenishment fuel replenishment box (13) that is divided stepwise by the isolation doors that block the air in the lateral direction. The exhaust pipe (14) for discharging smoke from the fumigation chamber was led to the outside, and refueling was performed at every stage temperature, that is, initially at 80 ° C. to 90 ° C. for 8 hours and after ignition for 40 hours, the middle period Extinguishes at 90-110 ° C for 40 hours, then heats up at 50 ° C, and in the latter period at 190 ° C-210 ° C for 5 hours, then quenches and cools to obtain a light brown moist and glossy fumigation bamboo with no surface unevenness Is.

  Alcohol shall be 95 degrees of first-grade fermentation, and leaves, stems, and roots from which plant chlorophyll is extracted are Apios, White Satsuma Mushroom, Sweet Tea, Wasabi, Kana, Herb, Black Letters, Park, Cherry, Sakura, Blue shiso, herbal medicines, and moss, and the plant chlorophyll extract is green.

  Apios uses improved Apios and native species, but it is classified into epidermis and cocoons, and the astringents of cocoons are extracted with alcohol to obtain a whitened powder after drying. Depending on the purpose, it can be used for confectionery, noodles, cold confectionery, various dishes, health foods, health drinks, pharmaceuticals, quasi-drugs, industrial paints, lactic acid processing, food processing, and fishery processing.

  Alcohol 20% is added to magnolia, cedar and bamboo, fermented lactic acid, acetic acid, left to stand, and filtered to obtain a filtered permeate. Squeeze with a compression screw mixer to make an extract from fermented lactic acid and acetic acid. This is an extract under the names of wood juice and bamboo juice.

  For removal of brown pigments of lignin and tanning, a clear clarified liquid can be obtained using a filter, whereby drinking water and bathing liquid can be obtained.

  As a recovery process for residual squeezing, after recovering the extract, candy tea green powder, wasabi powder, and Apios powder can be mixed with charcoal fine powder and processed into soap and health pillows. , Activated charcoal and diatomaceous earth are mixed, and as a device with a great effect of moisture, dew condensation prevention, antibacterial and deodorization, it is effective by constructing a partition that can be used for partition walls.

Industrial applicability

  The various residual squeezed powders after extraction of the solute solution of the present invention have great antibacterial and deodorizing effects, and prevent moisture and dew condensation as well as entrance entrances, room partitions, tea rooms, closet doors, and woodwork interiors besides screens. At the same time, it also has moisturizing, heat retaining, and heat insulating effects, so it can be used as a deodorizing device for the odor of livestock dung.

FIG. 3 is a cross-sectional view of a pyrolysis container set. These are sectional drawings of a fermentation device. FIG. 3 is a cross-sectional view of an alcohol immersion container. These are sectional drawings of a distillation diffusion device. FIG. 3 is a cross-sectional view of a filter. Fig. 3 is a side view of a partition. These are side views of a fumigation bamboo manufacturing apparatus.

Explanation of symbols

DESCRIPTION OF SYMBOLS 1 Frame body 2 Temperature sensor 3 Copper container 4 Electric heater 5 Glass container 6 Induction current heater 7 Mixing liquid tank 8 Steam suction pipe 9 Light emitting diode 10 Temperature sensor 11 Fumigation chamber 12 Cylindrical rotating rod 13 Supplementary fuel supply box 14 Exhaust tube a Leaf stalk b Rice straw c Recovery solute p Squeeze q Modified charcoal r Diatomaceous earth particle size silica s Fumigated bamboo t Bamboo material u Bark burning material A Lignin removal cylinder B Phenol removal cylinder B Ceramic sphere B Diatomaceous earth C Activated carbon Dion exchange membrane E Activated carbon F. Neutral ion ion resin exchange membrane G. Negative ion ion resin exchange membrane

Claims (1)

Plant leaves, stems, and roots hit the extract chlorophyll, stems, roots and the moisture content of 30% powder placed in a copper container by hand fir, in the case of sweetening material 50 ° C. to 70 ° C., astringent material In this case, after heating to 71 ° C. to 82 ° C., it is sandwiched between rice straw and fermented to give a coarse powder, and a dry powder having a water content of 15% to 20% is obtained in a glass container with 100 g of the coarse powder. The solute extracted from chlorophyll after removing the residue was used as a stock solution after being immersed and settled as a mixed solution of 95 cc of alcohol at 95 degrees, and 800 cc of diluted water was added to 100 cc of this stock solution. In addition, this is distilled and diffused by induction current heat to remove the alcohol component to obtain a residual mixed solution having an alcohol content of 0.3 ° C. or less, that is, an extracted chlorophyll color solution, and further, a contaminated brown lignin The leaf green is removed by a filter Commercialized as a green solution of the extracted clear transparent, which food processing, health foods, health drinks, solute solution preparation of chlorophyll that is characterized by utilizing the bathing solution.

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