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JP3727041B2 - Manufacturing method of Al-Mg-Si alloy extruded material for rotating parts and sliding parts with excellent surface roughness - Google Patents

Manufacturing method of Al-Mg-Si alloy extruded material for rotating parts and sliding parts with excellent surface roughness Download PDF

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JP3727041B2
JP3727041B2 JP11618597A JP11618597A JP3727041B2 JP 3727041 B2 JP3727041 B2 JP 3727041B2 JP 11618597 A JP11618597 A JP 11618597A JP 11618597 A JP11618597 A JP 11618597A JP 3727041 B2 JP3727041 B2 JP 3727041B2
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extruded material
surface roughness
parts
rotating parts
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JP11618597A
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JPH10298724A (en
Inventor
正 箕田
英雄 吉田
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Sumitomo Light Metal Industries Ltd
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Sumitomo Light Metal Industries Ltd
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Description

【0001】
【発明の属する技術分野】
本発明は、表面粗度に優れ、光輝性を有する回転部品、摺動部品用Al−Mg−Si合金押出材の製造方法に関する。
【0002】
【従来の技術】
JIS A6063、6N01、6061などに代表される6000系のAl−Mg−Si合金は、回転部品や摺動部品として使用されているが、これらの合金については、溶体化処理の省略によるコストダウンを目的として一般にプレス焼入れが行われている。プレス焼入れを行うためには、押出前のビレットの段階で強化元素のMg、Siを十分に固溶させておく必要があることから、均質化処理後の冷却速度を100℃/h以上に制御している。
【0003】
しかしながら、上記の均質化処理方法では、固溶成分が多い場合には変形抵抗が大きくなり、押出ダイスとの摩擦抵抗が上昇するため、押出材の表面粗度が大きく、外観上光沢性が要求される部品やクリアランスの小さい摺動部品に適用するには問題がある。
【0004】
【発明が解決しようとする課題】
本発明は、上記従来の問題点を解消するためになされたものであり、その目的は、Al−Mg−Si合金の熱間加工における変形抵抗を低減させることにより、表面粗度に優れた押出材を得ることを可能とする表面粗度に優れたAl−Mg−Si合金押出材の製造方法を提供することにある。
【0005】
【課題を解決するための手段】
上記の目的を達成するための請求項1による表面粗度に優れた回転部品、摺動部品用Al−Mg−Si合金押出材の製造方法は、Mg:0.4〜1.2%、Si:0.2〜0.8%を含有し、不純物としてのFeを0.5%以下に制限し、残部Alおよび不純物からなるアルミニウム合金鋳塊に対し、500〜600℃で1〜10時間加熱して、鋳塊温度が250℃になるまで50℃/h以下の冷却速度で徐冷する均質化処理を施したのち、300〜500℃の温度域で熱間押出を行うことによりRa:0.10μm以下の表面粗度を有する押出材とし、ついで500〜600℃で30分以上の溶体化処理後、焼入れを行い、150〜250℃で1〜12時間の人工時効処理を施し、205MPaを越える引張強さとすることを特徴とする。
【0006】
請求項2による表面粗度に優れた回転部品、摺動部品用Al−Mg−Si合金押出材の製造方法は、請求項1において、アルミニウム合金がさらにCr:0.5%以下、Mn:0.5%以下のうちの1種または2種を含有することを特徴とする。
【0007】
請求項3による表面粗度に優れた回転部品、摺動部品用Al−Mg−Si合金押出材の製造方法は、請求項 1 において、アルミニウム合金がさらにCr:0.5%以下、Mn:0.5%以下のうちの1種または2種、およびCu:0.5%を含有することを特徴とする。
【0008】
本発明によるAl−Mg−Si合金押出材の合金元素の意義、含有範囲について説明すると、MgおよびSiは強度を向上させるために機能する成分であり、好ましい含有量は、それぞれ0.4〜1.2%および0.2〜0.8%の範囲である。下限未満では強度向上の効果が小さく、それぞれ上限を越えると押出性が阻害される。不純物のFeは0.5%以下に制限する必要があり、0.5%を越えると押出材の表面粗度が低下し易くなる。
【0009】
Cr、Mnは、熱間押出材の結晶粒を微細化し、表面粗度の向上に有効に作用する。CrおよびMnの好ましい含有範囲は、それぞれ0.35%以下およびお.5%以下である。Cuは押出材の強度を高めるために添加される。好ましい含有量は0.5%以下の範囲である。なお、本発明においては、通常のアルミニウム合金に添加される0.1%以下のTi、0.02%以下のBを含んでいても、押出材の性能に影響することはない。
【0010】
【発明の実施の形態】
本発明によるAl−Mg−Si合金押出材の製造は、上記の組成を有するAl−Mg−Si合金を、常法に従って連続鋳造により造塊し、得られた押出用ビレットに対し、500〜600℃の温度で1〜10時間加熱して50℃/h以下の冷却速度で徐冷する均質化処理を施す。均質化処理後の冷却速度が50℃/hを越えると、Mg、Siの固溶量が多くなって熱間押出時の変形抵抗が増大し、押出材の表面粗度が大きくなり易い。なお、冷却速度50℃/h以下の徐冷は、ビレット温度が250℃になるまで行えばよい。
【0011】
ビレットの均質化処理を、500〜600℃で1〜10時間加熱した後、さらに300〜450℃で1〜10時間加熱する2段加熱により行っても本発明の目的を達成することができる。この場合には、加熱後の冷却速度を50℃/h以下に限定する必要はない。
【0012】
均質化処理後、300〜500℃の温度で熱間押出を行うことによって、Ra:0.10μm以下の表面粗度を有する押出材が得られる。押出温度が300℃未満では変形抵抗が高くなって押し詰まりを生じるおそれがあり、500℃を越える温度で押出加工を行うと、Mg、Siが固溶するため、変形抵抗が増大し、押出材の表面粗度が大きくなり易い。
【0013】
押出後、500〜600℃で、30分以上、好ましくは1時間以上の溶体化処理後、焼入れを行い人工時効処理を施す。溶体化処理温度が500℃未満では、Mg、Siの固溶が十分に行われ難く、600℃を越えると部分溶解が生じ易い。焼入れ後の人工時効処理は、150〜250℃で1〜12時間行うのが好ましい。
【0014】
【実施例】
以下、本発明の実施例を比較例と対比して説明する。
実施例1
Mg:0.58%、Si:0.42%、Mn:0.02%、Cu:0.02%、Ti:0.02%、Fe:0.20%、残部Alおよび不可避的不純物からなる組成を有するアルミニウム合金のビレット(直径200mm)を連続鋳造により造塊し、580℃の温度で2時間の均質化処理を行い、均質化処理後、ビレットを表1に示す条件で冷却した。
【0015】
ついで、表1に示す条件で、幅150mm、厚さ2mmの板状体に熱間押出加工し、得られた押出材を、520℃の温度で1時間溶体化処理後、強制空冷を行って焼入れ、175℃の温度で8時間の人工時効処理を施した。得られた試験材について、引張試験を行い、表面粗度を測定し、目視により光輝性の評価を行った。結果を表1に示す。表1にみられるように、本発明に従う試験材はいずれも205MPaを越える十分な強度、0.10μm以下の表面粗度をそなえ、優れた光輝性を示した。
【0016】
【表1】

Figure 0003727041
【0017】
比較例1
実施例1と同一組成を有するアルミニウム合金のビレット(直径200mm)を連続鋳造により造塊し、実施例1と同様、580℃の温度で2時間の均質化処理を行い、均質化処理後、ビレットを表2に示す条件で冷却した。
【0018】
ついで、表2に示す条件で、幅150mm、厚さ2mmの板状体に熱間押出加工し、得られた押出材を、表2に示す条件で溶体化処理し、強制空冷を行って焼入れ、175℃で8時間の人工時効処理を施した。得られた試験材について、引張試験を行い、表面粗度を測定し、目視により光輝性の評価を行った。結果を表3に示す。なお、表2において、本発明の条件を外れたものには下線を付した。
【0019】
【表2】
Figure 0003727041
【0020】
【表3】
Figure 0003727041
【0021】
表3に示すように、試験材No.6、No.7は均質化処理後の冷却速度が大き過ぎ、また試験材No.8は押出温度が高過ぎるため、いずれも熱間押出におて変形抵抗が大きく、押出材の表面粗度が劣っている。試験材No.9は溶体化処理温度が低く、また試験材No.10は溶体化処理時間が短いため、いずれも十分な強度が得られない。
【0022】
【発明の効果】
本発明によれば、表面粗度が小さく、光輝性に優れたAl−Mg−Si合金押出材が提供され、回転部品、摺動部品として有効である。[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a method for producing an Al-Mg-Si alloy extruded material for rotating parts and sliding parts having excellent surface roughness and glossiness.
[0002]
[Prior art]
6000 series Al-Mg-Si alloys represented by JIS A6063, 6N01, 6061, etc. are used as rotating parts and sliding parts. However, these alloys can reduce the cost by omitting solution treatment. In general, press hardening is performed for the purpose. In order to perform press quenching, it is necessary to sufficiently dissolve the strengthening elements Mg and Si at the billet stage before extrusion, so the cooling rate after homogenization is controlled to 100 ° C / h or more. are doing.
[0003]
However, in the above homogenization method, when there are many solid solution components, the deformation resistance increases, and the frictional resistance with the extrusion die increases, so the surface roughness of the extruded material is large, and the appearance must be glossy. However, there is a problem in applying to a sliding part having a small clearance.
[0004]
[Problems to be solved by the invention]
The present invention has been made in order to solve the above-mentioned conventional problems, and an object of the present invention is to reduce extrusion resistance in hot working of an Al-Mg-Si alloy, thereby extruding with excellent surface roughness. An object of the present invention is to provide a method for producing an Al—Mg—Si alloy extruded material having excellent surface roughness that enables obtaining a material.
[0005]
[Means for Solving the Problems]
In order to achieve the above object, the manufacturing method of the Al—Mg—Si alloy extruded material for rotating parts and sliding parts having excellent surface roughness according to claim 1 is Mg: 0.4 to 1.2%, Si : 0.2 to 0.8%, Fe as impurities is limited to 0.5% or less, and the aluminum alloy ingot composed of the remaining Al and impurities is heated at 500 to 600 ° C. for 1 to 10 hours. Then, after performing a homogenization treatment that gradually cools at a cooling rate of 50 ° C./h or less until the ingot temperature reaches 250 ° C., Ra: 0 is performed by performing hot extrusion in a temperature range of 300 to 500 ° C. .. Extruded material with a surface roughness of 10 μm or less, then solution treatment at 500-600 ° C. for 30 minutes or more , followed by quenching, artificial aging treatment at 150-250 ° C. for 1-12 hours , and 205 MPa It is characterized by having a tensile strength exceeding .
[0006]
The method for producing an Al-Mg-Si alloy extruded material for rotating parts and sliding parts having excellent surface roughness according to claim 2 is characterized in that the aluminum alloy further contains Cr: 0.5% or less, Mn: 0 It is characterized by containing one or two of 5% or less.
[0007]
The method for producing an Al-Mg-Si alloy extruded material for rotating parts and sliding parts having excellent surface roughness according to claim 3 is the method according to claim 1, wherein the aluminum alloy further contains Cr: 0.5% or less, Mn: 0 1 or 2 of 5% or less, and Cu: 0.5%.
[0008]
The meaning and content range of the alloy element of the Al—Mg—Si alloy extruded material according to the present invention will be described. Mg and Si are components that function to improve the strength, and preferred contents are 0.4 to 1 respectively. .2% and in the range of 0.2-0.8%. If it is less than the lower limit, the effect of improving the strength is small, and if the upper limit is exceeded, the extrudability is inhibited. Impurity Fe must be limited to 0.5% or less, and if it exceeds 0.5%, the surface roughness of the extruded material tends to decrease.
[0009]
Cr and Mn effectively refine the crystal grains of the hot extruded material and improve the surface roughness. The preferable content ranges of Cr and Mn are respectively 0.35% or less and. 5% or less. Cu is added to increase the strength of the extruded material. The preferred content is in the range of 0.5% or less. In the present invention, even if 0.1% or less of Ti and 0.02% or less of B added to a normal aluminum alloy are included, the performance of the extruded material is not affected.
[0010]
DETAILED DESCRIPTION OF THE INVENTION
The production of the extruded material of Al-Mg-Si alloy according to the present invention is performed by ingot-making the Al-Mg-Si alloy having the above composition by continuous casting according to a conventional method, and the obtained billet for extrusion is 500 to 600. A homogenization treatment is performed by heating at a temperature of 1 ° C. for 1 to 10 hours and gradually cooling at a cooling rate of 50 ° C./h or less. When the cooling rate after the homogenization treatment exceeds 50 ° C./h, the solid solution amount of Mg and Si increases, the deformation resistance during hot extrusion increases, and the surface roughness of the extruded material tends to increase. The slow cooling at a cooling rate of 50 ° C./h or less may be performed until the billet temperature reaches 250 ° C.
[0011]
The object of the present invention can be achieved even if the billet homogenization treatment is performed by heating at 500 to 600 ° C. for 1 to 10 hours and then by two-stage heating at 300 to 450 ° C. for 1 to 10 hours. In this case, it is not necessary to limit the cooling rate after heating to 50 ° C./h or less.
[0012]
After the homogenization treatment, an extruded material having a surface roughness Ra: 0.10 μm or less is obtained by performing hot extrusion at a temperature of 300 to 500 ° C. If the extrusion temperature is less than 300 ° C, the deformation resistance may increase and clogging may occur. If extrusion is performed at a temperature exceeding 500 ° C, Mg and Si will dissolve, and the deformation resistance will increase. The surface roughness of is likely to increase.
[0013]
After extrusion, solution treatment at 500 to 600 ° C. for 30 minutes or longer, preferably 1 hour or longer, followed by quenching and artificial aging treatment. When the solution treatment temperature is less than 500 ° C., Mg and Si are not sufficiently dissolved, and when it exceeds 600 ° C., partial dissolution is likely to occur. The artificial aging treatment after quenching is preferably performed at 150 to 250 ° C. for 1 to 12 hours.
[0014]
【Example】
Examples of the present invention will be described below in comparison with comparative examples.
Example 1
Mg: 0.58%, Si: 0.42%, Mn: 0.02%, Cu: 0.02%, Ti: 0.02%, Fe: 0.20%, balance Al and inevitable impurities A billet of aluminum alloy having a composition (diameter 200 mm) was ingoted by continuous casting, homogenized at a temperature of 580 ° C. for 2 hours, and after the homogenization, the billet was cooled under the conditions shown in Table 1.
[0015]
Next, under the conditions shown in Table 1, hot extrusion into a plate having a width of 150 mm and a thickness of 2 mm was performed, and the obtained extruded material was subjected to solution treatment at a temperature of 520 ° C. for 1 hour, followed by forced air cooling. Quenching and artificial aging treatment were performed at a temperature of 175 ° C. for 8 hours. About the obtained test material, the tension test was done, the surface roughness was measured, and the glossiness was evaluated visually. The results are shown in Table 1. As seen in Table 1, all of the test materials according to the present invention had sufficient strength exceeding 205 MPa and surface roughness of 0.10 μm or less, and exhibited excellent glitter.
[0016]
[Table 1]
Figure 0003727041
[0017]
Comparative Example 1
An aluminum alloy billet (200 mm in diameter) having the same composition as in Example 1 was ingoted by continuous casting, and was homogenized for 2 hours at a temperature of 580 ° C. in the same manner as in Example 1. Was cooled under the conditions shown in Table 2.
[0018]
Next, hot extrusion processing was performed on a plate-like body having a width of 150 mm and a thickness of 2 mm under the conditions shown in Table 2, and the obtained extruded material was subjected to a solution treatment under the conditions shown in Table 2, followed by forced air cooling and quenching. An artificial aging treatment was performed at 175 ° C. for 8 hours. About the obtained test material, the tension test was done, the surface roughness was measured, and the glossiness was evaluated visually. The results are shown in Table 3. In Table 2, those outside the conditions of the present invention are underlined.
[0019]
[Table 2]
Figure 0003727041
[0020]
[Table 3]
Figure 0003727041
[0021]
As shown in Table 3, the test material No. 6, no. No. 7 has too high a cooling rate after the homogenization treatment, and the test material No. Since the extrusion temperature of No. 8 is too high, all have high deformation resistance in hot extrusion, and the surface roughness of the extruded material is inferior. Test material No. No. 9 has a low solution treatment temperature. Since 10 has a short solution treatment time, none of them can provide sufficient strength.
[0022]
【The invention's effect】
ADVANTAGE OF THE INVENTION According to this invention, the surface roughness is small and the Al-Mg-Si alloy extrusion material excellent in brilliancy is provided, and it is effective as a rotation component and a sliding component.

Claims (3)

Mg:0.4〜1.2%、Si:0.2〜0.8%を含有し、不純物としてのFeを0.5%以下に制限し、残部Alおよび不純物からなるアルミニウム合金鋳塊に対し、500〜600℃で1〜10時間加熱して、鋳塊温度が250℃になるまで50℃/h以下の冷却速度で徐冷する均質化処理を施したのち、300〜500℃の温度域で熱間押出を行うことによりRa:0.10μm以下の表面粗度を有する押出材とし、ついで500〜600℃で30分以上の溶体化処理後、焼入れを行い、150〜250℃で1〜12時間の人工時効処理を施し、205MPaを越える引張強さとすることを特徴とする表面粗度に優れた回転部品、摺動部品用Al−Mg−Si合金押出材の製造方法。An aluminum alloy ingot containing Mg: 0.4 to 1.2%, Si: 0.2 to 0.8%, limiting Fe as an impurity to 0.5% or less, and remaining Al and impurities. On the other hand, after heating at 500 to 600 ° C. for 1 to 10 hours and performing a homogenization treatment at a cooling rate of 50 ° C./h or less until the ingot temperature reaches 250 ° C., a temperature of 300 to 500 ° C. Ra: Extruded material having a surface roughness of 0.10 μm or less by hot extrusion in the region, then subjected to solution treatment at 500 to 600 ° C. for 30 minutes or more , followed by quenching, and 1 to 150 to 250 ° C. A method for producing an Al-Mg-Si alloy extruded material for rotating parts and sliding parts having excellent surface roughness, characterized by performing an artificial aging treatment for -12 hours to obtain a tensile strength exceeding 205 MPa . アルミニウム合金がさらにCr:0.5%以下(0%を除く、以下同じ)、Mn:0.5%以下のうちの1種または2種を含有することを特徴とする請求項記載の表面粗度に優れた回転部品、摺動部品用Al−Mg−Si合金押出材の製造方法。Aluminum alloy further Cr: 0.5% or less (excluding 0%, hereinafter the same), Mn: surface according to claim 1, characterized in that it contains one or two of 0.5% or less A method for producing an Al-Mg-Si alloy extruded material for rotating parts and sliding parts having excellent roughness. アルミニウム合金がさらにCr:0.5%以下、Mn:0.5%以下のうちの1種または2種、およびCu:0.5%以下を含有することを特徴とする請求項記載の表面粗度に優れた回転部品、摺動部品用Al−Mg−Si合金押出材の製造方法。Aluminum alloy further Cr: 0.5% or less, Mn: 1 one or two of 0.5% or less, and Cu: the surface according to claim 1, characterized in that it contains 0.5% or less A method for producing an Al-Mg-Si alloy extruded material for rotating parts and sliding parts having excellent roughness.
JP11618597A 1997-04-18 1997-04-18 Manufacturing method of Al-Mg-Si alloy extruded material for rotating parts and sliding parts with excellent surface roughness Expired - Fee Related JP3727041B2 (en)

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TWI550093B (en) * 2014-08-08 2016-09-21 中國鋼鐵股份有限公司 High surface quality aluminum alloy sheet and fabricating method thereof
CN113846239A (en) * 2021-08-12 2021-12-28 广东伟业铝厂集团有限公司 Aluminum alloy section for new energy battery pack and preparation method thereof
CN120119127A (en) * 2023-04-12 2025-06-10 中亿丰金益(苏州)科技有限公司 Aluminum alloy profile and processing method and application thereof
CN117230352A (en) * 2023-09-15 2023-12-15 昆山联滔电子有限公司 Regenerated 6063 aluminum alloy material and preparation method and application thereof
CN117737490A (en) * 2023-12-07 2024-03-22 安徽省金兰金盈铝业有限公司 A processing technology for high-strength aluminum alloy
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