IN2014DN06601A - - Google Patents
Info
- Publication number
- IN2014DN06601A IN2014DN06601A IN6601DEN2014A IN2014DN06601A IN 2014DN06601 A IN2014DN06601 A IN 2014DN06601A IN 6601DEN2014 A IN6601DEN2014 A IN 6601DEN2014A IN 2014DN06601 A IN2014DN06601 A IN 2014DN06601A
- Authority
- IN
- India
- Prior art keywords
- reactor
- hcc
- hcl
- recovered
- distillation column
- Prior art date
Links
- 238000004821 distillation Methods 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- FFTOUVYEKNGDCM-OWOJBTEDSA-N (e)-1,3,3-trifluoroprop-1-ene Chemical compound F\C=C\C(F)F FFTOUVYEKNGDCM-OWOJBTEDSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000006227 byproduct Substances 0.000 abstract 1
- 125000001309 chloro group Chemical group Cl* 0.000 abstract 1
- 239000013065 commercial product Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000005191 phase separation Methods 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 230000003068 static effect Effects 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/23—Preparation of halogenated hydrocarbons by dehalogenation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/206—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being HX
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/38—Separation; Purification; Stabilisation; Use of additives
- C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
A process for the manufacture of 1 chloro 3 3 3 trifluoropropene (HCFC 1233zd) at commercial scale from the reaction of HCC 240 and HF is disclosed. In one embodiment HCC 240fa and HF are fed to a reactor operating at high pressure. Several different reactor designs useful in this process include; a stirred tank reactor (batch and/or continuous flow); a plug flow reactor; a static mixer used as a reactor; at least one of the above reactors operating at high pressure; optionally combined with a distillation column running at a lower pressure; and combinations of the above; and/or with a distillation column. The resulting product stream consisting of 1233zd HCl HF and other byproducts is partially condensed to recover HF by phase separation. The recovered HF phase is recycled to the reactor. The HCl is scrubbed from the vapor stream and recovered as an aqueous solution. The remaining organic components including the desired HCFC 1233zd are scrubbed dried and distilled to meet commercial product specifications.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261598938P | 2012-02-15 | 2012-02-15 | |
| US13/757,963 US8921621B2 (en) | 2012-02-15 | 2013-02-04 | Process for the production of HCFC-1233zd |
| PCT/US2013/025523 WO2013122860A1 (en) | 2012-02-15 | 2013-02-11 | PROCESS FOR THE PRODUCTION OF HCFC-1233zd |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IN2014DN06601A true IN2014DN06601A (en) | 2015-05-22 |
Family
ID=48946152
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IN6601DEN2014 IN2014DN06601A (en) | 2012-02-15 | 2013-02-11 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8921621B2 (en) |
| EP (3) | EP2814795B1 (en) |
| JP (1) | JP6220352B2 (en) |
| KR (1) | KR102050520B1 (en) |
| CN (2) | CN104105682A (en) |
| CA (1) | CA2863860C (en) |
| ES (1) | ES2869223T3 (en) |
| IN (1) | IN2014DN06601A (en) |
| MX (1) | MX337640B (en) |
| PL (1) | PL2814795T3 (en) |
| WO (1) | WO2013122860A1 (en) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9926244B2 (en) | 2008-10-28 | 2018-03-27 | Honeywell International Inc. | Process for drying HCFO-1233zd |
| US9540296B2 (en) | 2015-03-19 | 2017-01-10 | Honeywell International Inc. | Process for drying HCFO-1233zd |
| US9000240B2 (en) | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
| US9272969B2 (en) * | 2013-03-13 | 2016-03-01 | Honeywell International Inc. | Azeotropic compositions of 1,3,3-trichloro-1,1-difluoropropane and hydrogen fluoride |
| US9272968B2 (en) * | 2013-03-14 | 2016-03-01 | Honeywell International Inc. | Process to suppress the formation of 3,3,3-trifluoropropyne in fluorocarbon manufacture |
| US9255045B2 (en) | 2014-01-13 | 2016-02-09 | Arkema France | E-1-chloro-3,3,3-trifluoropropene production process from 1,1,3,3-tetrachloropropene |
| ES2891855T3 (en) | 2014-01-13 | 2022-01-31 | Arkema France | Production process of E-1-chloro-3,3,3-trifluoropropene from 1,1,3,3-tetrachloropropene |
| US9764998B2 (en) * | 2015-05-12 | 2017-09-19 | Honeywell International Inc. | Process for making HCFO-1233zd |
| FR3036398B1 (en) | 2015-05-22 | 2019-05-03 | Arkema France | COMPOSITIONS BASED ON 1,1,3,3-TETRACHLOROPROPENE |
| JP6826280B2 (en) * | 2016-01-15 | 2021-02-03 | セントラル硝子株式会社 | Method for producing trans-1-chloro-3,3,3-trifluoropropene |
| MX2019006410A (en) | 2016-12-02 | 2019-09-04 | Honeywell Int Inc | Process for drying hcfo-1233zd. |
| BR112019008414A2 (en) * | 2016-12-21 | 2019-07-09 | Arkema Inc | Processes and systems for recovering r1233zd in purified form |
| US9994502B1 (en) | 2018-01-30 | 2018-06-12 | Honeywell International Inc. | Process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) |
| US10000431B1 (en) | 2018-01-30 | 2018-06-19 | Honeywell International Inc. | Process for the production of 1-chloro-3,3,3-trifluoropropene (HCFO-1233zd) |
| US10717662B2 (en) | 2018-02-07 | 2020-07-21 | Honeywell International Inc. | Process for the removal of iron and phosphate ions from a chlorinated hydrocarbon waste stream |
| FR3081158B1 (en) | 2018-05-16 | 2020-07-31 | Arkema France | PROCESS FOR THE PRODUCTION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE. |
| FR3083232B1 (en) | 2018-06-27 | 2021-11-12 | Arkema France | 1-CHLORO-3,3,3-TRIFLUOROPROPENE PRODUCTION PROCESS |
| FR3086287B1 (en) | 2018-09-26 | 2020-09-18 | Arkema France | STABILIZATION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE |
Family Cites Families (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3818398B2 (en) | 1995-12-29 | 2006-09-06 | ダイキン工業株式会社 | Process for producing 1,1,1,3,3-pentafluoropropane |
| US6111150A (en) | 1996-06-20 | 2000-08-29 | Central Glass Company, Limited | Method for producing 1,1,1,3,3,-pentafluoropropane |
| US6023004A (en) | 1996-11-12 | 2000-02-08 | Alliedsignal, Inc. | Liquid phase catalytic fluorination of hydrochlorocarbon and hydrochlorofluorocarbon |
| BE1011765A3 (en) | 1998-02-26 | 2000-01-11 | Solvay | HYDROCARBONS hydrofluorination process. |
| ES2296420T3 (en) | 1998-11-13 | 2008-04-16 | Daikin Industries, Ltd. | AZEOTROPIC COMPOSITION CONSISTING OF 1,1,1,3,3-PENTAFLUOROPROPANO AND 1,1,1, -TRIFLUORO-3-CHLORO-2-PROPENE, ITS SEPARATION AND PURIFICATION PROCEDURE, AND 1,1,1 PRODUCTION PROCEDURE , 3,3-PENTAFLUOROPROPANO AND 1,1,1, -TRIFLUORO-3-CHLORINE-2-PROPENE. |
| US6844475B1 (en) * | 2003-08-08 | 2005-01-18 | Honeywell International Business Machines | Low temperature production of 1-chloro-3,3,3-trifluoropropene (HCFC-1233zd) |
| US8067650B2 (en) * | 2006-08-24 | 2011-11-29 | Honeywell International Inc. | Process for the production of HFO trans-1234ze from HFC-245fa |
| JP5416587B2 (en) * | 2006-10-03 | 2014-02-12 | メキシケム、アマンコ、ホールディング、ソシエダッド、アノニマ、デ、カピタル、バリアブレ | process |
| JP5416087B2 (en) | 2007-03-29 | 2014-02-12 | アーケマ・インコーポレイテッド | Hydrofluoropropene and hydrochlorofluoroolefin blowing agent composition |
| CN101687731B (en) | 2007-06-27 | 2013-09-04 | 阿科玛股份有限公司 | Process for the manufacture of hydrofluoroolefins |
| JP5599706B2 (en) | 2007-06-27 | 2014-10-01 | アーケマ・インコーポレイテッド | Stabilized hydrochlorofluoroolefins and hydrofluoroolefins |
| US20090018377A1 (en) * | 2007-07-09 | 2009-01-15 | Boyce C Bradford | Catalytic process for the preparation of fluorinated halocarbons |
| US8513473B2 (en) | 2007-10-10 | 2013-08-20 | Central Glass Company, Limited | Method for producing trans-1,3,3,3-tetrafluoropropene |
| US20110232306A1 (en) | 2008-04-30 | 2011-09-29 | Honeywell International Inc. | Absorption refrigeration cycles using a lgwp refrigerant |
| JP5515555B2 (en) * | 2008-09-25 | 2014-06-11 | セントラル硝子株式会社 | Method for producing 1,3,3,3-tetrafluoropropene |
| EP2341040B1 (en) * | 2008-09-25 | 2017-09-06 | Central Glass Company, Limited | Process for producing 1,3,3,3-tetrafluoropropene |
| EP2349962B1 (en) | 2008-11-19 | 2020-02-26 | Arkema Inc. | Process for the manufacture of hydrochlorofluoroolefins |
| CN102216245B (en) * | 2008-11-19 | 2014-04-23 | 阿科玛股份有限公司 | Process for the manufacture of hydrofluoroolefins |
| KR101684333B1 (en) * | 2009-03-24 | 2016-12-08 | 알케마 인코포레이티드 | Separation of r-1233 from hydrogen fluoride |
| US9045386B2 (en) | 2010-02-18 | 2015-06-02 | Honeywell International Inc. | Integrated process and methods of producing (E)-1-chloro-3,3,3-trifluoropropene |
| US8426656B2 (en) * | 2010-04-05 | 2013-04-23 | Honeywell International Inc. | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropropene and trans-1,3,3,3-tetrafluoropropene |
| US20110269999A1 (en) | 2010-04-29 | 2011-11-03 | Honeywell International Inc. | Process for dehydrohalogenation of halogenated alkanes |
| US9156752B2 (en) * | 2011-01-04 | 2015-10-13 | Honeywell International Inc. | High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same |
| US9000240B2 (en) * | 2011-05-19 | 2015-04-07 | Honeywell International Inc. | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene |
-
2013
- 2013-02-04 US US13/757,963 patent/US8921621B2/en not_active Expired - Fee Related
- 2013-02-11 CN CN201380009478.4A patent/CN104105682A/en active Pending
- 2013-02-11 IN IN6601DEN2014 patent/IN2014DN06601A/en unknown
- 2013-02-11 MX MX2014009815A patent/MX337640B/en active IP Right Grant
- 2013-02-11 EP EP13748643.7A patent/EP2814795B1/en active Active
- 2013-02-11 EP EP21160560.5A patent/EP3858808A1/en active Pending
- 2013-02-11 CN CN201711224589.3A patent/CN107827702A/en active Pending
- 2013-02-11 KR KR1020147025558A patent/KR102050520B1/en active Active
- 2013-02-11 PL PL13748643T patent/PL2814795T3/en unknown
- 2013-02-11 CA CA2863860A patent/CA2863860C/en active Active
- 2013-02-11 ES ES13748643T patent/ES2869223T3/en active Active
- 2013-02-11 EP EP24201575.8A patent/EP4461716A3/en active Pending
- 2013-02-11 WO PCT/US2013/025523 patent/WO2013122860A1/en not_active Ceased
- 2013-02-11 JP JP2014557705A patent/JP6220352B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| WO2013122860A1 (en) | 2013-08-22 |
| CA2863860C (en) | 2020-09-22 |
| CN107827702A (en) | 2018-03-23 |
| CN104105682A (en) | 2014-10-15 |
| KR20140129165A (en) | 2014-11-06 |
| PL2814795T3 (en) | 2021-09-13 |
| CA2863860A1 (en) | 2013-08-22 |
| MX337640B (en) | 2016-03-14 |
| ES2869223T3 (en) | 2021-10-25 |
| EP3858808A1 (en) | 2021-08-04 |
| US8921621B2 (en) | 2014-12-30 |
| EP2814795A1 (en) | 2014-12-24 |
| JP6220352B2 (en) | 2017-10-25 |
| KR102050520B1 (en) | 2019-11-29 |
| MX2014009815A (en) | 2014-09-25 |
| JP2015511946A (en) | 2015-04-23 |
| EP2814795B1 (en) | 2021-04-07 |
| US20130211154A1 (en) | 2013-08-15 |
| EP2814795A4 (en) | 2015-09-30 |
| EP4461716A2 (en) | 2024-11-13 |
| EP4461716A3 (en) | 2025-02-26 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| IN2014DN06601A (en) | ||
| US9556091B2 (en) | Integrated process for the production of 1-chloro-3,3,3-trifluoropropene | |
| JP6926173B2 (en) | Method for producing 1,1,3,3-tetrachloropropene | |
| MX2012011450A (en) | Integrated process to co-produce trans-1-chloro-3,3,3-trifluoropr opene and trans-1,3,3,3-tetrafluoropropene. | |
| TW201612152A (en) | Process for preparing terephthalic diesters with return alcohol enrichment | |
| MX2015010873A (en) | An improved integrated process to produce 2,3,3,3-tetrafluoroprop ene. | |
| US10836692B2 (en) | Method for isolating HFC-245cb and (E)-HFO-1234ze from composition containing both compounds | |
| IN2014DN07599A (en) | ||
| MX2017014314A (en) | PROCESS FOR MAKING HCFO-1233zd. | |
| MX343642B (en) | Synthesis of 1,1,3-trichloro-1-propene. | |
| MY183713A (en) | Process for the production of dialkyl succinate | |
| MY179084A (en) | Process for producing acetic acid | |
| IN2014CN00791A (en) | ||
| TH148345A (en) | Separation of 5-hydroxymethylfurfural (HMF) from reaction solution by steam distillation. |