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GB989381A - Superconductors - Google Patents

Superconductors

Info

Publication number
GB989381A
GB989381A GB20299/62A GB2029962A GB989381A GB 989381 A GB989381 A GB 989381A GB 20299/62 A GB20299/62 A GB 20299/62A GB 2029962 A GB2029962 A GB 2029962A GB 989381 A GB989381 A GB 989381A
Authority
GB
United Kingdom
Prior art keywords
wire
chamber
heated
nb3sn
tube
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB20299/62A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
RCA Corp
Original Assignee
RCA Corp
Radio Corporation of America
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by RCA Corp, Radio Corporation of America filed Critical RCA Corp
Publication of GB989381A publication Critical patent/GB989381A/en
Expired legal-status Critical Current

Links

Classifications

    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N60/00—Superconducting devices
    • H10N60/01—Manufacture or treatment
    • H10N60/0184—Manufacture or treatment of devices comprising intermetallic compounds of type A-15, e.g. Nb3Sn
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/54—Apparatus specially adapted for continuous coating
    • C23C16/545—Apparatus specially adapted for continuous coating for coating elongated substrates
    • H—ELECTRICITY
    • H10—SEMICONDUCTOR DEVICES; ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N—ELECTRIC SOLID-STATE DEVICES NOT OTHERWISE PROVIDED FOR
    • H10N60/00—Superconducting devices
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S505/00—Superconductor technology: apparatus, material, process
    • Y10S505/80—Material per se process of making same
    • Y10S505/815—Process of making per se
    • Y10S505/818—Coating
    • Y10S505/819—Vapor deposition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Superconductors And Manufacturing Methods Therefor (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Chemical Vapour Deposition (AREA)
  • Superconductor Devices And Manufacturing Methods Thereof (AREA)

Abstract

In a process of coating a wire or tape with a superconducting material consisting of at least two elements, e.g. Nb3, Sn, the heated wire is passed continuously through mixed vapours of the chlorides of Nb and Sn and hydrogen, the temperature of the wire being such that the Nb3Sn is deposited on the wire. The wire may be W, Ta, Mo, Ni/Cr, W/Ta, Nb/Ta or Rh/Pd and as shown in the drawing the wire 11 is continuously fed into a reaction chamber 10, the wire being electrically heated to 800-1400 DEG C. via graphite plugs 16 and 18. Chlorine gas is passed over heated Nb3Sn in a double walled tube 19 via inlet 22 and enters reaction chamber 10 via outlet 27. Hydrogen with or without HCl is also introduced into chamber 10 via inlet 20 of tube 19 and outlet 27 and helium or argon are also introduced into chamber 10 via inlets 15 and 17. The whole assembly is heated by furnace 26 so that the temperature of the mixed chloride vapours in chamber 10 is maintained at 700-750 DEG C. Alternatively the mixed chloride vapours may be formed by reacting the chlorine gas with elemental Sn and Nb placed in the tube 19. <PICT:0989381/C1/1>ALSO:In a process of coating a wire or tape with a superconducting material consisting of at least two elements, e.g. Nb3Sn, the heated wire is passed continuously through mixed vapours of the chlorides of Nb and Sn and hydrogen, the temperature of the wire being such that the Nb3Sn is deposited on the wire. The wire may be W, Ta, Mo, Ni/Cr, W/Ta, Nb/Ta or Rh/Pd and as shown in the drawing the wire 11 is continuously fed into a reaction chamber 10 the wire being electrically heated to 800-1400 DEG C. via graphite plugs 16 and 18. Chlorine gas is passed over heated Nb3Sn in a double walled tube 19 via inlet 22 and enters reaction chamber 10 via outlet 27. Hydrogen with or without HCl is also introduced into chamber 10 via inlet 20 of tube 19 and outlet 27, and helium or argon are also introduced into chamber 10 via inlets 15 and 17. The whole assembly is heated by furnace 26 so that the temperature of the mixed chloride vapours in chamber 10 is maintained at 700-750 DEG C. Alternatively the mixed chloride vapours may be formed by reacting the chlorine gas with elemental Sn and Nb placed in the tube 19. <PICT:0989381/C6-C7/1>
GB20299/62A 1961-05-26 1962-05-25 Superconductors Expired GB989381A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US112853A US3268362A (en) 1961-05-26 1961-05-26 Deposition of crystalline niobium stannide

Publications (1)

Publication Number Publication Date
GB989381A true GB989381A (en) 1965-04-14

Family

ID=22346191

Family Applications (1)

Application Number Title Priority Date Filing Date
GB20299/62A Expired GB989381A (en) 1961-05-26 1962-05-25 Superconductors

Country Status (6)

Country Link
US (1) US3268362A (en)
JP (1) JPS3918215B1 (en)
DE (1) DE1446230B2 (en)
FR (1) FR1322777A (en)
GB (1) GB989381A (en)
NL (1) NL278934A (en)

Families Citing this family (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3472694A (en) * 1961-05-26 1969-10-14 Rca Corp Deposition of crystalline niobium stannide
FR1370673A (en) * 1963-06-24 1964-08-28 Csf Superconducting winding coil and method of making it
DE1458474A1 (en) * 1963-12-21 1968-12-19 Siemens Ag Process for the preparation of intermetallic superconducting compounds
DE1292465B (en) * 1964-04-30 1969-04-10 Siemens Ag Process for the production of superconducting layers from niobium-tin
US3420707A (en) * 1964-12-28 1969-01-07 Rca Corp Deposition of niobium stannide
US3400016A (en) * 1965-11-15 1968-09-03 Rca Corp Method of coating superconducting niobium tin with lattice defects
US3519481A (en) * 1966-10-14 1970-07-07 Gen Electric Method for forming thin films having superconductive contacts
US3847653A (en) * 1972-10-27 1974-11-12 Atomic Energy Commission Method and apparatus for fabricating composite ceramic members
US4044456A (en) * 1974-05-16 1977-08-30 Siemens Aktiengesellschaft Method for the manufacture of a superconductor with a superconductive intermetallic compound of at least two elements
FR2275032A1 (en) * 1974-06-14 1976-01-09 Siemens Ag PROCESS FOR MANUFACTURING A SUPRACONDUCTOR CONTAINING AN INTERMETAL COMPOUND, SUPRACONDUCTOR, CONSTITUTED BY AT LEAST TWO ELEMENTS
US4098920A (en) * 1976-12-27 1978-07-04 Texaco Inc. Method of continuous production of super conducting wire
US4138512A (en) * 1977-10-17 1979-02-06 The United States Of America As Represented By The Secretary Of The Army Process for chemical vapor deposition of a homogeneous alloy of refractory metals
US4367102A (en) * 1980-01-22 1983-01-04 Siemens Aktiengesellschaft Method for the manufacture of a superconductor containing an intermetallic compounds

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US553296A (en) * 1896-01-21 Jonas walter aylsworth
US1173012A (en) * 1914-04-29 1916-02-22 Friedrich Meyer Reduction of chlorids.
US1497417A (en) * 1919-03-31 1924-06-10 Henry C P Weber Process of coating metals
US1675120A (en) * 1922-12-09 1928-06-26 Westinghouse Lamp Co Deposition of thorium from its vaporizable compounds
US1987577A (en) * 1931-11-25 1935-01-08 Gen Electric Apparatus for the thermic treatment of metal wires, filaments, bands, or the like
US2430520A (en) * 1945-03-06 1947-11-11 Glass Science Inc Deposition of metal on glass from metal formates
US2552626A (en) * 1948-02-17 1951-05-15 Bell Telephone Labor Inc Silicon-germanium resistor and method of making it
US2711973A (en) * 1949-06-10 1955-06-28 Thompson Prod Inc Vapor phase coating of molybdenum articles
US2656284A (en) * 1949-09-07 1953-10-20 Ohio Commw Eng Co Method of plating rolled sheet metal
US2665475A (en) * 1950-03-18 1954-01-12 Fansteel Metallurgical Corp Highly refractory body
US2952904A (en) * 1957-01-15 1960-09-20 Westinghouse Electric Corp Applying protective metal coatings on molybdenum
NL229502A (en) * 1957-07-11
US3061462A (en) * 1959-03-26 1962-10-30 Chromalloy Corp Metallic diffusion processes
US3078554A (en) * 1960-06-08 1963-02-26 Gen Electric Columbium base alloy article
US3181936A (en) * 1960-12-30 1965-05-04 Gen Electric Superconductors and method for the preparation thereof

Also Published As

Publication number Publication date
DE1446230B2 (en) 1971-09-30
DE1446230A1 (en) 1968-11-14
FR1322777A (en) 1963-03-29
NL278934A (en)
US3268362A (en) 1966-08-23
JPS3918215B1 (en) 1964-08-28

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