GB698636A - Improvements in the manufacture of condensation products - Google Patents
Improvements in the manufacture of condensation productsInfo
- Publication number
- GB698636A GB698636A GB1269/51A GB126951A GB698636A GB 698636 A GB698636 A GB 698636A GB 1269/51 A GB1269/51 A GB 1269/51A GB 126951 A GB126951 A GB 126951A GB 698636 A GB698636 A GB 698636A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- group
- reacted
- amino
- dodecyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007859 condensation product Substances 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 7
- 239000000047 product Substances 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 125000003277 amino group Chemical group 0.000 abstract 3
- ONJQDTZCDSESIW-UHFFFAOYSA-N polidocanol Chemical compound CCCCCCCCCCCCOCCOCCOCCOCCOCCOCCOCCOCCOCCO ONJQDTZCDSESIW-UHFFFAOYSA-N 0.000 abstract 3
- ALYNCZNDIQEVRV-UHFFFAOYSA-N 4-aminobenzoic acid Chemical compound NC1=CC=C(C(O)=O)C=C1 ALYNCZNDIQEVRV-UHFFFAOYSA-N 0.000 abstract 2
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 abstract 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- -1 benzal group Chemical group 0.000 abstract 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 abstract 2
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 abstract 2
- 229920000151 polyglycol Polymers 0.000 abstract 2
- 239000010695 polyglycol Substances 0.000 abstract 2
- 239000011734 sodium Substances 0.000 abstract 2
- 229910052708 sodium Inorganic materials 0.000 abstract 2
- SKDHHIUENRGTHK-UHFFFAOYSA-N 4-nitrobenzoyl chloride Chemical compound [O-][N+](=O)C1=CC=C(C(Cl)=O)C=C1 SKDHHIUENRGTHK-UHFFFAOYSA-N 0.000 abstract 1
- PHSPJQZRQAJPPF-UHFFFAOYSA-N N-alpha-Methylhistamine Chemical compound CNCCC1=CN=CN1 PHSPJQZRQAJPPF-UHFFFAOYSA-N 0.000 abstract 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 1
- 239000005864 Sulphur Substances 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 230000002421 anti-septic effect Effects 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000000249 desinfective effect Effects 0.000 abstract 1
- 238000005187 foaming Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 238000005984 hydrogenation reaction Methods 0.000 abstract 1
- 150000007522 mineralic acids Chemical class 0.000 abstract 1
- SBOJXQVPLKSXOG-UHFFFAOYSA-N o-amino-hydroxylamine Chemical class NON SBOJXQVPLKSXOG-UHFFFAOYSA-N 0.000 abstract 1
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 abstract 1
- 230000000361 pesticidal effect Effects 0.000 abstract 1
- DHRLEVQXOMLTIM-UHFFFAOYSA-N phosphoric acid;trioxomolybdenum Chemical compound O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.OP(O)(O)=O DHRLEVQXOMLTIM-UHFFFAOYSA-N 0.000 abstract 1
- IYDGMDWEHDFVQI-UHFFFAOYSA-N phosphoric acid;trioxotungsten Chemical compound O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.O=[W](=O)=O.OP(O)(O)=O IYDGMDWEHDFVQI-UHFFFAOYSA-N 0.000 abstract 1
- XAEFZNCEHLXOMS-UHFFFAOYSA-M potassium benzoate Chemical compound [K+].[O-]C(=O)C1=CC=CC=C1 XAEFZNCEHLXOMS-UHFFFAOYSA-M 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 239000001648 tannin Substances 0.000 abstract 1
- 235000018553 tannin Nutrition 0.000 abstract 1
- 229920001864 tannin Polymers 0.000 abstract 1
- 238000009736 wetting Methods 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/16—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing nitrogen, e.g. nitro-, nitroso-, azo-compounds, nitriles, cyanates
- A61K47/18—Amines; Amides; Ureas; Quaternary ammonium compounds; Amino acids; Oligopeptides having up to five amino acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/45—Derivatives containing from 2 to 10 oxyalkylene groups
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Epidemiology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Dermatology (AREA)
- Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
Abstract
Condensation products, apparently amino-esters and amino-ethers, are prepared by heating a polyglycol ether product of the formula A.(OC2H4)n.B (in which A is an aliphatic hydrocarbon chain with at least four carbon atoms, B is -OH, -ONa, -OK, or the radical of an inorganic acid, and n is an integer) with an aromatic acid or phenol or a functional derivative thereof containing in its molecule as a substituent at least one amino group or a nitro group, and converting any nitro groups present in the product into amino groups. The polyglycolether chain may be interrupted by a divalent group or sulphur, and the amino group of the aromatic acid or phenol may be protected, e.g. by a benzal group. The products are soluble and may be made more so by introduction of sulphuric acid radicals or polyglycol ether radicals or by peralkylation. They form difficultly soluble products with tannin, synthetic or natural tanning agents, phosphotungstic acid, phosphomolybdic acid, phosphotungstomolybdic acid, or silicolungstic acid. They have disinfecting, preserving, pesticidal, antiseptic, foaming, wetting, and dispersing properties. In examples: (1) dodecyl nonaglycol ether is reacted in toluene with phosphorus tribromide to give dodecyl nonaglycol bromide, which is reacted with the potassium salt of para-aminobenzoic acid; (2) cetyl decaglycol bromide is reacted with sodium p-benzolaminophenate, the benzal group being split off; (3) dodecyl nonaglycol ether is reacted with sodium in benzene and then with p-nitrobenzoyl chloride, followed by hydrogenation.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE698636X | 1950-01-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB698636A true GB698636A (en) | 1953-10-21 |
Family
ID=6608212
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1269/51A Expired GB698636A (en) | 1950-01-26 | 1951-01-17 | Improvements in the manufacture of condensation products |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB698636A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE974320C (en) * | 1954-05-14 | 1960-11-24 | Ciba Geigy | Process for the preparation of a p-amino-benzoic acid-polyglycol ester which can be used as a local anesthetic |
| EP0675939A4 (en) * | 1993-10-28 | 1996-03-20 | Chevron Chem Co | Fuel compositions containing poly(oxyalkylene) aromatic ethers. |
-
1951
- 1951-01-17 GB GB1269/51A patent/GB698636A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE974320C (en) * | 1954-05-14 | 1960-11-24 | Ciba Geigy | Process for the preparation of a p-amino-benzoic acid-polyglycol ester which can be used as a local anesthetic |
| EP0675939A4 (en) * | 1993-10-28 | 1996-03-20 | Chevron Chem Co | Fuel compositions containing poly(oxyalkylene) aromatic ethers. |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| GB698636A (en) | Improvements in the manufacture of condensation products | |
| GB224376A (en) | Improvements in the manufacture of triarylguanidines | |
| GB972972A (en) | Novel 2-amino-benzophenones and the preparation thereof | |
| ES192667A1 (en) | IMPROVEMENTS MADE IN THE PREPARATION OF DETERGENT COMPOSITIONS | |
| GB717863A (en) | Improvements relating to rubber antioxidants | |
| GB1429458A (en) | Tetrisocyanate composition and process therefor | |
| GB367494A (en) | Improvements in methods of preserving rubber and products obtained thereby | |
| GB423504A (en) | Improved insecticides | |
| GB355425A (en) | Improvements in or relating to the manufacture of vulcanised rubber and the like | |
| GB300716A (en) | Manufacture of arsenobenzenes | |
| GB450323A (en) | Improvements in or relating to the preservation of rubber | |
| GB426243A (en) | Manufacture of mixed carbonyl salicylic etheranhydride of salicylocarbonic acid and homologues thereof | |
| GB498302A (en) | Improvements in and relating to synthetic rubber-like materials | |
| GB403915A (en) | Manufacture of symmetrical di-(arylamino)-hydroxybenzenes | |
| GB1041560A (en) | Improvements in or relating to the bleaching of clays | |
| GB305229A (en) | New antiseptics and disinfectants | |
| GB705692A (en) | Improvements in the production of n-gamma-oxoalkyl derivatives of amino phenols or naphthols | |
| GB632848A (en) | Improvements in or relating to pesticidal compositions | |
| GB633885A (en) | Improvements in or relating to emulsions for combating noxious organisms | |
| FR992068A (en) | Coating strip for shoe sole or other similar articles, as well as soles and shoes conforming to those obtained | |
| GB311930A (en) | Improvements in or relating to the manufacture of rubber compositions | |
| ES270914A2 (en) | PROCEDURE FOR THE PREPARATION OF ALKIL- (ARIL) -MERCAPTO-METHYLENAMIDES OF 0,0-DIAKYL-THIO- (DITIO) -PHOSPHORYL-ACEUTICS ACIDS, WITH PESTICIDAL ACTIVITY | |
| GB689430A (en) | Improvements in or relating to the preparation of 2:4:5-trichlorbenzylchloride | |
| GB1182366A (en) | Preparation of Aromatic Dithiols | |
| GB413012A (en) | Improvements in and relating to the preservation of rubber |