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GB526542A - Improvements in or relating to the absorption of bromine - Google Patents

Improvements in or relating to the absorption of bromine

Info

Publication number
GB526542A
GB526542A GB551239A GB551239A GB526542A GB 526542 A GB526542 A GB 526542A GB 551239 A GB551239 A GB 551239A GB 551239 A GB551239 A GB 551239A GB 526542 A GB526542 A GB 526542A
Authority
GB
United Kingdom
Prior art keywords
liquor
tower
volume
circulating
absorption
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB551239A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Priority to GB551239A priority Critical patent/GB526542A/en
Publication of GB526542A publication Critical patent/GB526542A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B7/00Halogens; Halogen acids
    • C01B7/09Bromine; Hydrogen bromide
    • C01B7/096Bromine

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Treating Waste Gases (AREA)

Abstract

526,542. Bromides and bromates. WILLIAMSON, A. T., and IMPERIAL CHEMICAL INDUSTRIES, Ltd. Feb. 18, 1939, No. 5512. [Class 1 (iii)] A process for absorbing bromine from gases containing it, e.g., from air blowing chlorinated brine, comprises treating the gas with an alkaline absorption liquor in a series of cyclically operated absorption towers, the flows of gas and liquor in the series as a whole being counter-current and in the towers either co- or counter-current, and reducing the back pressure of bromine exerted by the circulating liquor by employing in association with at least one tower such a volume of circulating liquor that the periodic time of circulation for that tower exceeds a time to move to = 5W/QL minutes (W being the total rate of absorption in kg. per minute and QL is the rate of liquor circulation in the tower in c. meters per min.) and/or by heating at least part of the circulating liquor associated with at least one tower, while the liquor is outside the tower, the liquor being cooled before it is again brought into contact with the gas. Preferably at least one tower at or near the end of the series has associated with it a volume of circulating liquor greater than the average volume per tower. The absorbing liquor may be a 3-12 per cent. aqueous solution of sodium carbonate, caustic soda or borax. In a typical example, illustrated by Fig. 1, the volume of liquid associated with each tower is 8 c.m., the liquor circulating rate being .278 c.m. per minute and the total rate of absorption is 0.164 kgs. per minute. The periodic time of circulation is 28.8 minutes, i.e., equal to 48.8 W/QL. Five towers only of a given efficiency are required compared with nine in the known process to absorb 97 per cent. bromine in the original gas and the total liquor volume is 40 c.m. In a further example (Fig. 2) each tower has 10 c.m. of liquor associated therewith and the liquor leaving tower No. 1 is heated to 60‹C. in the relay vessel and cooled to 20‹C. before its return to the tower. The periodic time of circulation in this case W is 36 mins., i.e., 61.4- and four towers only QL are necessary with a total liquor volume of 40 c.m.
GB551239A 1939-02-18 1939-02-18 Improvements in or relating to the absorption of bromine Expired GB526542A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB551239A GB526542A (en) 1939-02-18 1939-02-18 Improvements in or relating to the absorption of bromine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB551239A GB526542A (en) 1939-02-18 1939-02-18 Improvements in or relating to the absorption of bromine

Publications (1)

Publication Number Publication Date
GB526542A true GB526542A (en) 1940-09-20

Family

ID=9797598

Family Applications (1)

Application Number Title Priority Date Filing Date
GB551239A Expired GB526542A (en) 1939-02-18 1939-02-18 Improvements in or relating to the absorption of bromine

Country Status (1)

Country Link
GB (1) GB526542A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2481837A2 (en) 2011-01-26 2012-08-01 Superior Plus LP Process for producing chlorine with low bromine content
US8636893B2 (en) 2011-01-26 2014-01-28 Superior Plus Lp Process for producing chlorine with low bromine content
CN116161622A (en) * 2023-04-25 2023-05-26 天津长芦汉沽盐场有限责任公司 Method for preparing bromine by using carnallite mother liquor

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2481837A2 (en) 2011-01-26 2012-08-01 Superior Plus LP Process for producing chlorine with low bromine content
US8636893B2 (en) 2011-01-26 2014-01-28 Superior Plus Lp Process for producing chlorine with low bromine content
CN116161622A (en) * 2023-04-25 2023-05-26 天津长芦汉沽盐场有限责任公司 Method for preparing bromine by using carnallite mother liquor
CN116161622B (en) * 2023-04-25 2024-01-02 天津长芦汉沽盐场有限责任公司 Method for preparing bromine by using carnallite mother liquor

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