GB200816A - Improvements in and relating to a process of preparing alkali celluloses, and in the preparation of cellulose ethers therefrom - Google Patents
Improvements in and relating to a process of preparing alkali celluloses, and in the preparation of cellulose ethers therefromInfo
- Publication number
- GB200816A GB200816A GB17765/23A GB1776523A GB200816A GB 200816 A GB200816 A GB 200816A GB 17765/23 A GB17765/23 A GB 17765/23A GB 1776523 A GB1776523 A GB 1776523A GB 200816 A GB200816 A GB 200816A
- Authority
- GB
- United Kingdom
- Prior art keywords
- alkali
- drying
- cellulose
- celluloses
- cellulose ethers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003513 alkali Substances 0.000 title abstract 7
- 229920002678 cellulose Polymers 0.000 title abstract 7
- 238000000034 method Methods 0.000 title abstract 3
- 229920003086 cellulose ether Polymers 0.000 title abstract 2
- 235000010980 cellulose Nutrition 0.000 title 1
- 238000001035 drying Methods 0.000 abstract 5
- 239000000463 material Substances 0.000 abstract 4
- 239000003518 caustics Substances 0.000 abstract 3
- 239000001913 cellulose Substances 0.000 abstract 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000012084 conversion product Substances 0.000 abstract 1
- 238000001816 cooling Methods 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 229910052757 nitrogen Inorganic materials 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
- C08B1/08—Alkali cellulose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Alkali-celluloses of low water-content are prepared from watery alkali-celluloses by drying at temperatures below 18 DEG C., preferably below 10 DEG C. It is preferred to carry out the drying in vacuum apparatus provided with cooling means, the material being spread in thin layers or continuously stirred or kneaded; but the drying may also be carried out in the presence of air, for example, in hydrogen or nitrogen. To hasten drying, a dessicating agent may be employed. The initial material may be cellulose or a conversion product in which the cellulose has not been degraded too far. The material may be soaked in a solution containing the correct amount of caustic alkali but an excess of water, and the whole mass subsequently dried; or an excess of alkali solution may be employed, and the mass pressed, centrifuged, &c. before drying, until it contains the correct amount of alkali; or the material may be impregnated with alkali solution, pressed if necessary, and solid caustic alkali added. The alkali-celluloses obtained are particularly adapted for the manufacture of cellulose ethers, either by a single stage or multi-stage process, the procedure depending on the character of the desired product and on the amount of caustic alkali incorporated with the cellulose.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AT200816X | 1922-07-13 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB200816A true GB200816A (en) | 1924-11-10 |
Family
ID=3669086
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB17765/23A Expired GB200816A (en) | 1922-07-13 | 1923-07-09 | Improvements in and relating to a process of preparing alkali celluloses, and in the preparation of cellulose ethers therefrom |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB200816A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0023292A1 (en) * | 1979-07-18 | 1981-02-04 | Henkel Kommanditgesellschaft auf Aktien | Process for preparing cellulose derivatives with highly reactive alkali cellulose |
| US4339574A (en) * | 1979-07-18 | 1982-07-13 | Henkel Kommanditgesellschaft Auf Aktien | Preparation of alkyl cellulose |
-
1923
- 1923-07-09 GB GB17765/23A patent/GB200816A/en not_active Expired
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0023292A1 (en) * | 1979-07-18 | 1981-02-04 | Henkel Kommanditgesellschaft auf Aktien | Process for preparing cellulose derivatives with highly reactive alkali cellulose |
| US4339574A (en) * | 1979-07-18 | 1982-07-13 | Henkel Kommanditgesellschaft Auf Aktien | Preparation of alkyl cellulose |
| US4339573A (en) * | 1979-07-18 | 1982-07-13 | Henkel Kommanditgesellschaft Auf Aktien | Preparation of cellulose derivatives using highly reactive alkali cellulose |
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