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GB1589614A - Method of bottom teeming molten metal from a vessel provided with a valved outlet - Google Patents

Method of bottom teeming molten metal from a vessel provided with a valved outlet Download PDF

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Publication number
GB1589614A
GB1589614A GB4595976A GB4595976A GB1589614A GB 1589614 A GB1589614 A GB 1589614A GB 4595976 A GB4595976 A GB 4595976A GB 4595976 A GB4595976 A GB 4595976A GB 1589614 A GB1589614 A GB 1589614A
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GB
United Kingdom
Prior art keywords
melt
crust
granular
granular material
upper layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4595976A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stopinc AG
Original Assignee
Stopinc AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stopinc AG filed Critical Stopinc AG
Priority to GB4595976A priority Critical patent/GB1589614A/en
Publication of GB1589614A publication Critical patent/GB1589614A/en
Expired legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D41/00Casting melt-holding vessels, e.g. ladles, tundishes, cups or the like
    • B22D41/14Closures
    • B22D41/44Consumable closure means, i.e. closure means being used only once
    • B22D41/46Refractory plugging masses

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Casting Support Devices, Ladles, And Melt Control Thereby (AREA)

Description

(54) METHOD OF BOTTOM TEEMING MOLTEN METAL FROM A VESSEL PROVIDED WITH A VALVED OUTLET (71) We, STOPINC AKTIENGESELLSCHAFT, a Company organised under the laws of Switzerland of Zugerstrasse 76a, CH 6340 Baar, Switzerland do hereby declare the invention for which we pray that a patent may be granted to us, and the method by which it is to be performed, to be particularly described in and by the following statement: The invention relates to improvements in, and the operation of, slide gate nozzles including rotary and longitudinal sliding gate nozzles for metallurgical vessels in particular for the bottom teeming of steel or other metals from ladles and the like.
The closure plane of the slide gate nozzle is inevitably below the shell of the ladle, i.e.
at the lower end of the discharge duct in the nozzle brick. As this duct is of comparatively small diameter, e.g. 5 to 7 cm., the steel is liable to freeze in it and make the device inoperative during the waiting period between the filling of the ladle and the beginning of teeming.
One way of overcoming this problem is described in British Patent 1112368 (Paderwerk Gebr Benteler). According to this specification the said nozzle brick has a funnel shape which, before each charge of the ladle, is filled with highly refractory granular material, the free surface of the granular material in the funnel being at least 150 square centimetres with a following neck portion at least 30 mm long. A crust is formed at the interface of the refractory granular material with the molten steel, which prevents further penetration of steel into the dry granular material. On opening the slide gate valve the granular material below the crust flows out freely under its own weight, leaving the crust, which spans the funnels, unsupported. Under the weight of the liquid steel above it, the crust collapses thus allowing the steel to be teemed without difficulty.
It will be noted that the refractory material not only fills the narrow neck portion, but also the funnel. This is essential because according to the known method the crust only collapses if it has a sufficiently wide span. This in turn means that a substantial quantity of granular material has to be used which is undesirable as it increases the risk of contaminatig the molten steel. A further drawback is the fact that the technique does not work without a certain percentage of failures, in which the crust does not collapse and has to be destroyed by an oxygen lance.
The reasons for this were not understood.
It is the object of the present invention to at least reduce the severity of these drawbacks.
We now believe that the success of the above technique depends not so much on the diameter of the crust (its "span") but at least as much on the ratio of diameter to the thickness of the crust. The diameter of the crust, and hence the cross section of the part of the funnel in which it forms, may be smaller than the minimum of 150 square centimetres stipulated in the known technique, provided that the thickness of the crust is kept sufficiently small and does not materially increase with increasing waiting time prior to teeming.
The present invention is a method of bottom teeming molten metal from a vessel provided with a valved outlet having an outlet opening communicating with a nozzle brick located in the lining of the vessel, which comprises locating granular refractory material in the outlet passage of the nozzle brick so that the top surface of the said material is within the nozzle brick and selecting the composition or arrangement of the granular material in relation to the melt which is to be teemed to ensure that the interaction of the melt with the granular material is localised at the surface thereof.
The localisation of the formation of the crust is preferably achieved by using a two component granular material for the filling, the upper layer at the interface with the melt being a layer of refractory material which will sinter to a dense crust on contact with the melt thus inhibiting further penetration by the melt, the mass of granular material below the upper layer being of a different composition such as not to sinter in contact with the melt or at the temperatures to which it may be raised in use due to conduction from the melt. The material of the upper layer preferably has a sintering temperature close to the melting point of the melt, that is to say not far below the latter, e.g. not more than 200"C below the melting point of the melt.
The effect of this arrangement is threefold: (1) The surface layer of the granular material becomes rapidly impervious to the penetration of steel due to the sintering together of the grains forming the surface layer.
(2) The crust is only formed by the surface layer so that its depth remains small.
(3) The crust does not increase in depth even for a long waiting time, because the progressive increase in temperature of the principal mass of material below the crust can never reach the sintering temperature of the latter.
A suitable material for the principal mass of granular material is granular magnesite produced from sea water. There are many materials suitable for the surface layer. One such material is granular Transvaal chrome ore which tends to sinter between 1400 and 14500"C.
In applying the method according to this invention to a funnel shaped nozzle brick it is not advisable to fill only the neck portion of the nozzle brick if the latter is relatively short compared to the funnel portion. The danger in this case is not that the crust forms in a different manner, but that, due to the depth of the funnel, the lowermost layer of molten steel above the granular material freezes. If this occurred it would make the valve inoperative, or at least would necessitate burning a hole into the frozen steel layer with an oxygen lance.
It is preferred to use a nozzle brick of which the conical portion is shorter than the cylindrical portion and in which the outlet passage is almost filled with the granular material so that the crust is near the inside surface of the lining of the ladle. In this case the funnel shaped portion will have relatively small free opening which may be less than 150 square centimetres. In this case, the nozzle brick can be filled or almost filled without using a great amount of granular material. But as the crust would be near the bottom of the ladle, there would be little or no danger of the steel freezing above the granular material.
The upper or surface layer of granular material could be a mixture of such sinterable material and other refractory material which would not sinter with the melt involved, the mixture however being such as still to inhibit further penetration by the melt.
Preferably the mass of granular material below the upper layer material has a higher sintering temperature and melting point than the sinterable material of the upper layer.
The particle size of the sinterable material of the upper layer is preferably smaller than that of the non-sinterable material so as to form an effective barrier to penetration by the melt.
In order to facilitate the formation of a layer of sinterable material at the interface with the melt of correct thickness, the sinterable material may be supplied in disc shaped bags which may be of flat cylindrical shape or flat truncated cone shape. The bags are preferably of impermeable material which is imflammable and will be destroyed when the melt is placed in the vessel.
WHAT WE CLAIM IS: 1. A method of bottom teeming molten metal from a vessel provided with a valved outlet having an outlet opening communicating with a nozzle brick located in the lining of the vessel, which comprises locating granular refractory material in the outlet passage of the nozzle brick so that the top surface of the said material is within the nozzle brick and selecting the composition or arrangement of the granular material in relation to the melt which is to be teemed to ensure that the interaction of the melt with the granular material is localised at the surface thereof.
2. A method as claimed in Claim 1 in which the localization of the formation of the crust is achieved by using a two component granular material for the filling, the upper layer at the interface with the melt being a layer of refractory material which will sinter to a dense crust on contact with the melt thus inhibiting further penetration by the melt, the mass of granular material below the upper layer being of a different composition such as not to sinter in contact with the melt or at the temperatures to which it may be raised in use due to conduction from the melt.
3. A method as claimed in Claim 2 in which the material of the upper layer in contact with the melt has a sintering temperature the value of which is not more than 200"C below the melting point of the melt.
4. A method as claimed in claim 2 or claim 3 in which the particle size of the sinterable material of the upper layer is
**WARNING** end of DESC field may overlap start of CLMS **.

Claims (9)

**WARNING** start of CLMS field may overlap end of DESC **. crust is preferably achieved by using a two component granular material for the filling, the upper layer at the interface with the melt being a layer of refractory material which will sinter to a dense crust on contact with the melt thus inhibiting further penetration by the melt, the mass of granular material below the upper layer being of a different composition such as not to sinter in contact with the melt or at the temperatures to which it may be raised in use due to conduction from the melt. The material of the upper layer preferably has a sintering temperature close to the melting point of the melt, that is to say not far below the latter, e.g. not more than 200"C below the melting point of the melt. The effect of this arrangement is threefold: (1) The surface layer of the granular material becomes rapidly impervious to the penetration of steel due to the sintering together of the grains forming the surface layer. (2) The crust is only formed by the surface layer so that its depth remains small. (3) The crust does not increase in depth even for a long waiting time, because the progressive increase in temperature of the principal mass of material below the crust can never reach the sintering temperature of the latter. A suitable material for the principal mass of granular material is granular magnesite produced from sea water. There are many materials suitable for the surface layer. One such material is granular Transvaal chrome ore which tends to sinter between 1400 and 14500"C. In applying the method according to this invention to a funnel shaped nozzle brick it is not advisable to fill only the neck portion of the nozzle brick if the latter is relatively short compared to the funnel portion. The danger in this case is not that the crust forms in a different manner, but that, due to the depth of the funnel, the lowermost layer of molten steel above the granular material freezes. If this occurred it would make the valve inoperative, or at least would necessitate burning a hole into the frozen steel layer with an oxygen lance. It is preferred to use a nozzle brick of which the conical portion is shorter than the cylindrical portion and in which the outlet passage is almost filled with the granular material so that the crust is near the inside surface of the lining of the ladle. In this case the funnel shaped portion will have relatively small free opening which may be less than 150 square centimetres. In this case, the nozzle brick can be filled or almost filled without using a great amount of granular material. But as the crust would be near the bottom of the ladle, there would be little or no danger of the steel freezing above the granular material. The upper or surface layer of granular material could be a mixture of such sinterable material and other refractory material which would not sinter with the melt involved, the mixture however being such as still to inhibit further penetration by the melt. Preferably the mass of granular material below the upper layer material has a higher sintering temperature and melting point than the sinterable material of the upper layer. The particle size of the sinterable material of the upper layer is preferably smaller than that of the non-sinterable material so as to form an effective barrier to penetration by the melt. In order to facilitate the formation of a layer of sinterable material at the interface with the melt of correct thickness, the sinterable material may be supplied in disc shaped bags which may be of flat cylindrical shape or flat truncated cone shape. The bags are preferably of impermeable material which is imflammable and will be destroyed when the melt is placed in the vessel. WHAT WE CLAIM IS:
1. A method of bottom teeming molten metal from a vessel provided with a valved outlet having an outlet opening communicating with a nozzle brick located in the lining of the vessel, which comprises locating granular refractory material in the outlet passage of the nozzle brick so that the top surface of the said material is within the nozzle brick and selecting the composition or arrangement of the granular material in relation to the melt which is to be teemed to ensure that the interaction of the melt with the granular material is localised at the surface thereof.
2. A method as claimed in Claim 1 in which the localization of the formation of the crust is achieved by using a two component granular material for the filling, the upper layer at the interface with the melt being a layer of refractory material which will sinter to a dense crust on contact with the melt thus inhibiting further penetration by the melt, the mass of granular material below the upper layer being of a different composition such as not to sinter in contact with the melt or at the temperatures to which it may be raised in use due to conduction from the melt.
3. A method as claimed in Claim 2 in which the material of the upper layer in contact with the melt has a sintering temperature the value of which is not more than 200"C below the melting point of the melt.
4. A method as claimed in claim 2 or claim 3 in which the particle size of the sinterable material of the upper layer is
smaller than that of the non-sinterable material so as to form an effective barrier to penetration by the melt.
5. A method as claimed in Claim 2, 3 or 4 in which the material of the upper layer is granular Transvaal chrome ore which sinters between 1400 and 1450"C.
6. A method as claimed in any one of Claims 1 to 5 in which the principal mass of granular material is granular magnesite produced from sea water.
7. A method as claimed in any one of Claims 1 to 6 in which the outlet passage of the nozzle brick is funnel shaped, the conical portion of the funnel being shorter than the cylindrical portion of the funnel and in which the outlet passage is almost filled with the granular material so that the crust is near the inside surface of the lining of the ladle.
8. A method as claimed in any one of Claims 1 to 7 in which the sinterable material is supplied in disc shaped bags which are of flat cylindrical shape or flat truncated cone shape.
9. A method as claimed in Claim 8 in which the bags are of impermeable material which is inflammable and will be destroyed when the melt is placed in the vessel.
GB4595976A 1977-11-04 1977-11-04 Method of bottom teeming molten metal from a vessel provided with a valved outlet Expired GB1589614A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB4595976A GB1589614A (en) 1977-11-04 1977-11-04 Method of bottom teeming molten metal from a vessel provided with a valved outlet

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB4595976A GB1589614A (en) 1977-11-04 1977-11-04 Method of bottom teeming molten metal from a vessel provided with a valved outlet

Publications (1)

Publication Number Publication Date
GB1589614A true GB1589614A (en) 1981-05-13

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GB4595976A Expired GB1589614A (en) 1977-11-04 1977-11-04 Method of bottom teeming molten metal from a vessel provided with a valved outlet

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2120588A (en) * 1982-05-27 1983-12-07 British Steel Corp Introduction of refractory filler material into nozzle assemblies of molten metal-holding vessel
US4525463A (en) * 1982-04-17 1985-06-25 Heinz Dislich Spout-filling mass
GB2226262B (en) * 1988-12-21 1993-02-10 K S R International Limited Improvements in or relating to pouring of metals

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4525463A (en) * 1982-04-17 1985-06-25 Heinz Dislich Spout-filling mass
GB2120588A (en) * 1982-05-27 1983-12-07 British Steel Corp Introduction of refractory filler material into nozzle assemblies of molten metal-holding vessel
GB2226262B (en) * 1988-12-21 1993-02-10 K S R International Limited Improvements in or relating to pouring of metals

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PS Patent sealed
PCNP Patent ceased through non-payment of renewal fee