GB1388249A - Process for producing anhydrous disodium phosphate - Google Patents
Process for producing anhydrous disodium phosphateInfo
- Publication number
- GB1388249A GB1388249A GB3807073A GB3807073A GB1388249A GB 1388249 A GB1388249 A GB 1388249A GB 3807073 A GB3807073 A GB 3807073A GB 3807073 A GB3807073 A GB 3807073A GB 1388249 A GB1388249 A GB 1388249A
- Authority
- GB
- United Kingdom
- Prior art keywords
- disodium phosphate
- product
- anhydrous disodium
- saturated
- phosphonic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 title abstract 5
- 229910000397 disodium phosphate Inorganic materials 0.000 title abstract 4
- 235000019800 disodium phosphate Nutrition 0.000 title abstract 4
- 239000001488 sodium phosphate Substances 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 abstract 4
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 abstract 2
- 239000007791 liquid phase Substances 0.000 abstract 2
- 229910000029 sodium carbonate Inorganic materials 0.000 abstract 2
- 235000017550 sodium carbonate Nutrition 0.000 abstract 2
- 239000007790 solid phase Substances 0.000 abstract 2
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000012452 mother liquor Substances 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/30—Alkali metal phosphates
- C01B25/301—Preparation from liquid orthophosphoric acid or from an acid solution or suspension of orthophosphates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
1388249 Anhydrous disodium phosphate KAZAKHSKY FILIAL LENINGRADSKOGO GOSNDARSTVENUOGO I PROEKTNOGO INSTITUTA OSNOVNOI KHIMICHESKOI PROMYSHLENNOSTI and CHIMKENTSKY FOSFORNY ZAVOD IMEN1 10 Aug 1973 38070/73 Heading C1A A process for producing anhydrous disodium phosphate by reacting soda ash with phosphonic acid of 75-100% by wt. concentration in a solution of disodium phosphate saturated at 90-105‹ C. with the formation of a solid phase comprising the product and a liquid phase comprising a saturated disodium phosphate solution, followed by separating the phases. It is preferred to carry out the reaction using a columetric ratio of 1 : 3 between the solid and liquid phases. The process can be operated continuously by feeding the mother liquor, after separation of the product by, e.g. centrifuging, back to the reaction stage between soda ash and phosphonic acid at a temperature of 90-103‹ C. Figures are given for the particle size distribution of the product which are in the range 0À1-0À4 mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3807073A GB1388249A (en) | 1973-08-10 | 1973-08-10 | Process for producing anhydrous disodium phosphate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3807073A GB1388249A (en) | 1973-08-10 | 1973-08-10 | Process for producing anhydrous disodium phosphate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1388249A true GB1388249A (en) | 1975-03-26 |
Family
ID=10400961
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3807073A Expired GB1388249A (en) | 1973-08-10 | 1973-08-10 | Process for producing anhydrous disodium phosphate |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1388249A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4661331A (en) * | 1984-09-24 | 1987-04-28 | Monsanto Company | Continuous process for preparing sodium orthophosphate slurries from natural soda ash and orthophosphoric acid |
| US4853200A (en) * | 1984-09-24 | 1989-08-01 | Monsanto Company | Continuous process for preparing sodium orthophosphate slurries from natural soda ash orthophosphoric acid |
-
1973
- 1973-08-10 GB GB3807073A patent/GB1388249A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4661331A (en) * | 1984-09-24 | 1987-04-28 | Monsanto Company | Continuous process for preparing sodium orthophosphate slurries from natural soda ash and orthophosphoric acid |
| US4853200A (en) * | 1984-09-24 | 1989-08-01 | Monsanto Company | Continuous process for preparing sodium orthophosphate slurries from natural soda ash orthophosphoric acid |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |