GB1215561A - Process for producing dialkyl sulphosuccinic acid salts - Google Patents
Process for producing dialkyl sulphosuccinic acid saltsInfo
- Publication number
- GB1215561A GB1215561A GB1284669A GB1284669A GB1215561A GB 1215561 A GB1215561 A GB 1215561A GB 1284669 A GB1284669 A GB 1284669A GB 1284669 A GB1284669 A GB 1284669A GB 1215561 A GB1215561 A GB 1215561A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dialkyl
- prepared
- acid salts
- maleate
- aqueous solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ULUAUXLGCMPNKK-UHFFFAOYSA-N Sulfobutanedioic acid Chemical class OC(=O)CC(C(O)=O)S(O)(=O)=O ULUAUXLGCMPNKK-UHFFFAOYSA-N 0.000 title abstract 4
- 239000007864 aqueous solution Substances 0.000 abstract 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical class OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 abstract 2
- 239000003795 chemical substances by application Substances 0.000 abstract 2
- WBZKQQHYRPRKNJ-UHFFFAOYSA-L disulfite Chemical class [O-]S(=O)S([O-])(=O)=O WBZKQQHYRPRKNJ-UHFFFAOYSA-L 0.000 abstract 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 abstract 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- -1 amine salt Chemical class 0.000 abstract 1
- ROPXFXOUUANXRR-YPKPFQOOSA-N bis(2-ethylhexyl) (z)-but-2-enedioate Chemical compound CCCCC(CC)COC(=O)\C=C/C(=O)OCC(CC)CCCC ROPXFXOUUANXRR-YPKPFQOOSA-N 0.000 abstract 1
- 238000009833 condensation Methods 0.000 abstract 1
- 230000005494 condensation Effects 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- JMGZBMRVDHKMKB-UHFFFAOYSA-L disodium;2-sulfobutanedioate Chemical compound [Na+].[Na+].OS(=O)(=O)C(C([O-])=O)CC([O-])=O JMGZBMRVDHKMKB-UHFFFAOYSA-L 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 239000012429 reaction media Substances 0.000 abstract 1
- 239000011541 reaction mixture Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/32—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of salts of sulfonic acids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1,215,561. Dialkyl sulphosuccinic acid salts. MELLE BEZONS. 11 March, 1969 [25 March, 1968], No. 12846/69. Heading C2C. Dialkyl sulpho-succinic acid salts are prepared by gradually introducing an aqueous solution of a hydrogen sulphite salt or a metabisulphite salt into the corresponding dialkyl maleate, under stirring, in the presence of a homogenizing agent which maintains the reaction medium in homogeneous form. Preferably a concentrated, freshly prepared aqueous solution of Na, K, ammonium or amine salt of the hydrogen sulphite or metabisulphite is used. The homogenizing agent may be an alcohol or a dialkyl sulphosuccinate identical to the one to be prepared, and is advantageously present in 5-20% by weight with respect to the maleate. An organic diluent such as an alcohol, ether, ester or hydrocarbon may also be present. Amongst the examples di-(2-ethyl hexyl) sodium sulphosuccinate is prepared by gradually adding an aqueous solution of NaHSO 3 over a period of 5 hours to di-(2-ethyl hexyl) maleate with a portion of the final reaction mixture from a previous identical condensation as homogenizer.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR79000482 | 1968-03-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1215561A true GB1215561A (en) | 1970-12-09 |
Family
ID=9696338
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1284669A Expired GB1215561A (en) | 1968-03-25 | 1969-03-11 | Process for producing dialkyl sulphosuccinic acid salts |
Country Status (2)
| Country | Link |
|---|---|
| FR (1) | FR1573080A (en) |
| GB (1) | GB1215561A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0130818A2 (en) | 1983-07-01 | 1985-01-09 | Unilever N.V. | Process for the handling of dialkyl sulphosuccinates |
| EP0140710A3 (en) * | 1983-11-01 | 1985-11-27 | Unilever N.V. | Dialkyl sulphosuccinate composition and process for its preparation |
| WO1992008695A1 (en) * | 1990-11-12 | 1992-05-29 | Henkel Kommanditgesellschaft Auf Aktien | METHOD OF PREPARING CONCENTRATED AQUEOUS DISPERSIONS OF THE MONO AND/OR DI SALTS OF α-SULPHONIC ACIDS |
| CN1045592C (en) * | 1996-03-25 | 1999-10-13 | 南京理工大学 | Preparation process of diisooctyl sodium sulfosuccinate |
| WO2016196555A1 (en) | 2015-06-02 | 2016-12-08 | Stepan Company | Cold-water cleaning method |
| WO2017100051A2 (en) | 2015-12-07 | 2017-06-15 | Stepan Comapny | Cold-water cleaning compositions and methods |
| CN114249673A (en) * | 2021-11-29 | 2022-03-29 | 四川科宏达集团有限责任公司 | Method for catalytically synthesizing succinate sulfonate |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4325923A1 (en) * | 1993-08-02 | 1995-02-09 | Henkel Kgaa | Liquid formulations containing sulfosuccinic acid diesters |
-
1968
- 1968-03-25 FR FR1573080D patent/FR1573080A/fr not_active Expired
-
1969
- 1969-03-11 GB GB1284669A patent/GB1215561A/en not_active Expired
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0130818A2 (en) | 1983-07-01 | 1985-01-09 | Unilever N.V. | Process for the handling of dialkyl sulphosuccinates |
| EP0140710A3 (en) * | 1983-11-01 | 1985-11-27 | Unilever N.V. | Dialkyl sulphosuccinate composition and process for its preparation |
| WO1992008695A1 (en) * | 1990-11-12 | 1992-05-29 | Henkel Kommanditgesellschaft Auf Aktien | METHOD OF PREPARING CONCENTRATED AQUEOUS DISPERSIONS OF THE MONO AND/OR DI SALTS OF α-SULPHONIC ACIDS |
| US5329030A (en) * | 1990-11-12 | 1994-07-12 | Henkel Kommanditgesellschaft Auf Aktien | Process for the production of concentrated aqueous dispersions of α-sulfofatty acide mono- and/or disalt |
| CN1045592C (en) * | 1996-03-25 | 1999-10-13 | 南京理工大学 | Preparation process of diisooctyl sodium sulfosuccinate |
| WO2016196555A1 (en) | 2015-06-02 | 2016-12-08 | Stepan Company | Cold-water cleaning method |
| WO2017100051A2 (en) | 2015-12-07 | 2017-06-15 | Stepan Comapny | Cold-water cleaning compositions and methods |
| CN114249673A (en) * | 2021-11-29 | 2022-03-29 | 四川科宏达集团有限责任公司 | Method for catalytically synthesizing succinate sulfonate |
| CN114249673B (en) * | 2021-11-29 | 2023-03-14 | 四川科宏达集团有限责任公司 | Method for catalytically synthesizing succinate sulfonate |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1912531A1 (en) | 1970-04-09 |
| FR1573080A (en) | 1969-07-04 |
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