GB1265550A - - Google Patents
Info
- Publication number
- GB1265550A GB1265550A GB1265550DA GB1265550A GB 1265550 A GB1265550 A GB 1265550A GB 1265550D A GB1265550D A GB 1265550DA GB 1265550 A GB1265550 A GB 1265550A
- Authority
- GB
- United Kingdom
- Prior art keywords
- sol
- aging
- mins
- july
- alumina
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 abstract 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 230000032683 aging Effects 0.000 abstract 3
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 abstract 2
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 abstract 2
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 2
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 abstract 2
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 abstract 1
- 229910018626 Al(OH) Inorganic materials 0.000 abstract 1
- 229910019440 Mg(OH) Inorganic materials 0.000 abstract 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical class 0.000 abstract 1
- 239000004411 aluminium Substances 0.000 abstract 1
- 229910052782 aluminium Inorganic materials 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 239000008119 colloidal silica Substances 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 150000007530 organic bases Chemical class 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- XREXPQGDOPQPAH-QKUPJAQQSA-K trisodium;[(z)-18-[1,3-bis[[(z)-12-sulfonatooxyoctadec-9-enoyl]oxy]propan-2-yloxy]-18-oxooctadec-9-en-7-yl] sulfate Chemical compound [Na+].[Na+].[Na+].CCCCCCC(OS([O-])(=O)=O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CC(CCCCCC)OS([O-])(=O)=O)COC(=O)CCCCCCC\C=C/CC(CCCCCC)OS([O-])(=O)=O XREXPQGDOPQPAH-QKUPJAQQSA-K 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
- C01B33/146—After-treatment of sols
- C01B33/149—Coating
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Colloid Chemistry (AREA)
Abstract
1,265,550. Alumina-coated silica sol. E.I. DU PONT DE NEMOURS & CO. 16 July, 1969 [18 July, 1968; 9 June, 1969], No. 35918/69. Heading C1A. A positively charged alumina-coated silica sol is made by mixing a negatively-charged aquasol of colloidal silica particles (e.g. 7-30 mÁ. in size) with an aqueous solution of a basic aluminium chloride, aging the sol and then raising the pH of the aged sol to 4À5-6À5 by adding NH 4 OH, an alkali or alkaline earth metal base, e.g. NaOH, KOH, LiOH, Ca(OH) 2 or Mg(OH) 2 , or a water soluble organic base, e.g. methylamine or monoethanolamine or two or more of these. When the aged sol contains 10% or less by wt. of solids, the pH may be raised to 4À5- 7À0. The molar ratio of aluminium to surface SiO a in the product may be 1 : 2 to 2 : 1. The basic aluminium chloride may be of the formula Al(OH) 2 Cl to Al 3 (OH) 8 Cl, e.g. Al 2 (OH) 5 Cl. Aging may be carried out by allowing the mixture to stand at room temperature, or by heating it at temperatures up to 100‹ C. or, under pressure, above 100‹ C., and is preferably continued till the lowered pH remains constant, generally at 4 or less. Specified aging conditions are about 2 hrs. at 60‹ C., about 30 mins. at 80‹ C. and about 15 mins. at 90‹ C.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US74571468A | 1968-07-18 | 1968-07-18 | |
| US83174869A | 1969-06-09 | 1969-06-09 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1265550A true GB1265550A (en) | 1972-03-01 |
Family
ID=27114509
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1265550D Expired GB1265550A (en) | 1968-07-18 | 1969-07-16 |
Country Status (7)
| Country | Link |
|---|---|
| BE (1) | BE736238A (en) |
| DE (1) | DE1935666A1 (en) |
| ES (1) | ES369370A1 (en) |
| FR (1) | FR2016805A1 (en) |
| GB (1) | GB1265550A (en) |
| LU (1) | LU59112A1 (en) |
| NL (1) | NL6910696A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1999020564A1 (en) * | 1997-10-16 | 1999-04-29 | Ab Carl Munters | Method for treating silica gel |
| US6224944B1 (en) | 1991-09-20 | 2001-05-01 | Eka Nobel Ab | Method of protecting a surface |
| US6379500B2 (en) | 1999-12-20 | 2002-04-30 | Akzo Nobel Nv | Silica-based sols |
| EP1010666A4 (en) * | 1998-06-12 | 2003-01-02 | Asahi Glass Co Ltd | SILICON DIOXIDE ALUMINUM OXIDE COMPOUND SOL, METHOD FOR THE PRODUCTION THEREOF, AND RECORDING MEDIUM |
| US7862868B2 (en) | 2005-01-19 | 2011-01-04 | Ferrania Technologies, S.P.A. | Ink-jet recording material |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3544727A1 (en) * | 1985-12-18 | 1987-06-19 | Schock & Co Gmbh | Sink unit having a moulding in the shape of a work surface |
-
1969
- 1969-07-10 ES ES369370A patent/ES369370A1/en not_active Expired
- 1969-07-11 NL NL6910696A patent/NL6910696A/xx unknown
- 1969-07-14 DE DE19691935666 patent/DE1935666A1/en active Pending
- 1969-07-16 LU LU59112D patent/LU59112A1/xx unknown
- 1969-07-16 GB GB1265550D patent/GB1265550A/en not_active Expired
- 1969-07-17 BE BE736238D patent/BE736238A/xx unknown
- 1969-07-17 FR FR6924371A patent/FR2016805A1/fr not_active Withdrawn
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6224944B1 (en) | 1991-09-20 | 2001-05-01 | Eka Nobel Ab | Method of protecting a surface |
| WO1999020564A1 (en) * | 1997-10-16 | 1999-04-29 | Ab Carl Munters | Method for treating silica gel |
| GB2344583A (en) * | 1997-10-16 | 2000-06-14 | Munters Ab Carl | Method for treating silica gel |
| GB2344583B (en) * | 1997-10-16 | 2001-05-16 | Munters Ab Carl | Method for treating silica gel |
| US6375914B1 (en) | 1997-10-16 | 2002-04-23 | Ab Carl Munters | Method for treating silica gel |
| EP1010666A4 (en) * | 1998-06-12 | 2003-01-02 | Asahi Glass Co Ltd | SILICON DIOXIDE ALUMINUM OXIDE COMPOUND SOL, METHOD FOR THE PRODUCTION THEREOF, AND RECORDING MEDIUM |
| US6623820B1 (en) | 1998-06-12 | 2003-09-23 | Asahi Glass Company Ltd. | Silica-alumina composite sol, processes for producing the same, and recording medium |
| US6379500B2 (en) | 1999-12-20 | 2002-04-30 | Akzo Nobel Nv | Silica-based sols |
| US6893538B2 (en) | 1999-12-20 | 2005-05-17 | Akzo Nobel N.V. | Process for the production of paper using silica-based sols |
| US7862868B2 (en) | 2005-01-19 | 2011-01-04 | Ferrania Technologies, S.P.A. | Ink-jet recording material |
Also Published As
| Publication number | Publication date |
|---|---|
| LU59112A1 (en) | 1969-11-25 |
| NL6910696A (en) | 1970-01-20 |
| FR2016805A1 (en) | 1970-05-15 |
| DE1935666A1 (en) | 1970-02-26 |
| ES369370A1 (en) | 1971-06-16 |
| BE736238A (en) | 1969-12-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |