GB1090975A - Improvements in or relating to volatilization of organic liquids - Google Patents
Improvements in or relating to volatilization of organic liquidsInfo
- Publication number
- GB1090975A GB1090975A GB579264A GB579264A GB1090975A GB 1090975 A GB1090975 A GB 1090975A GB 579264 A GB579264 A GB 579264A GB 579264 A GB579264 A GB 579264A GB 1090975 A GB1090975 A GB 1090975A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dispersion
- solution
- droplets
- polybutadiene
- rubbery
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 title abstract 5
- 239000006185 dispersion Substances 0.000 abstract 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 abstract 6
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 abstract 4
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 3
- 239000005062 Polybutadiene Substances 0.000 abstract 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 239000000463 material Substances 0.000 abstract 3
- 229920002857 polybutadiene Polymers 0.000 abstract 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 2
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 abstract 2
- -1 accelerators Substances 0.000 abstract 2
- MVPPADPHJFYWMZ-UHFFFAOYSA-N chlorobenzene Chemical compound ClC1=CC=CC=C1 MVPPADPHJFYWMZ-UHFFFAOYSA-N 0.000 abstract 2
- 229920001577 copolymer Polymers 0.000 abstract 2
- 239000004604 Blowing Agent Substances 0.000 abstract 1
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 abstract 1
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 239000006229 carbon black Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 238000013329 compounding Methods 0.000 abstract 1
- 239000004615 ingredient Substances 0.000 abstract 1
- 239000003999 initiator Substances 0.000 abstract 1
- 229920000126 latex Polymers 0.000 abstract 1
- 239000004816 latex Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229920003052 natural elastomer Polymers 0.000 abstract 1
- 229920001194 natural rubber Polymers 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 239000012763 reinforcing filler Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000004094 surface-active agent Substances 0.000 abstract 1
- 229920003051 synthetic elastomer Polymers 0.000 abstract 1
- 239000005061 synthetic rubber Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/14—Powdering or granulating by precipitation from solutions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/18—Evaporating by spraying to obtain dry solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0042—Degasification of liquids modifying the liquid flow
- B01D19/0047—Atomizing, spraying, trickling
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/06—Making microcapsules or microballoons by phase separation
- B01J13/12—Making microcapsules or microballoons by phase separation removing solvent from the wall-forming material solution
- B01J13/125—Making microcapsules or microballoons by phase separation removing solvent from the wall-forming material solution by evaporation of the solvent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
- C08C1/00—Treatment of rubber latex
- C08C1/02—Chemical or physical treatment of rubber latex before or during concentration
- C08C1/04—Purifying; Deproteinising
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08C—TREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
- C08C2/00—Treatment of rubber solutions
- C08C2/06—Winning of rubber from solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F36/00—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds
- C08F36/02—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds
- C08F36/04—Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, at least one having two or more carbon-to-carbon double bonds the radical having only two carbon-to-carbon double bonds conjugated
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
- C08G64/40—Post-polymerisation treatment
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
- C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
- C08J3/07—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media from polymer solutions
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/12—Powdering or granulating
- C08J3/122—Pulverisation by spraying
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2321/00—Characterised by the use of unspecified rubbers
- C08J2321/02—Latex
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
An aqueous dispersion of a rubbery polymeric material is prepared from a feedstock which contains the material in solution in a volatile organic liquid by sub-dividing the feestock into droplets, intimately mixing the droplets with steam in conditions in which steam condenses on the droplets and all of the organic liquid is volatilized from each droplet while that droplet is free of external contact with a solid or bulk liquid and collecting the remaining portions of the droplets as a dispersion in water, in the presence of a surface-active agent, the rubbery material being soft at the temperature of collection. Specified organic liquids are toluene, heptane, chloroform, carbon tetrachloride, chlorobenzene, trichlorethylene, ethyl acetate and acetone. The feedstock may be a solution of a natural or synthetic rubber or a dispersion of such a solution and may carry such compounding ingredients as reinforcing fillers, vulcanizing agents, accelerators, antioxidants, antiozonants, blowing agents, initiators and catalysts. Example are given of the preparation of (I) a dispersion of an ethylene/propylene copolymer from a solution of a rubbery ethylene/propylene copolymer in equal parts of carbon tetrachloride and hexane, (II) a dispersion of polybutadiene from a dispersion of a solution of polybutadiene in hexane, and (III) a latex of polybutadiene containing carbon black. Apparatus for carrying out the process is described.
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB579264A GB1090975A (en) | 1964-02-12 | 1964-02-12 | Improvements in or relating to volatilization of organic liquids |
| NL6501687A NL6501687A (en) | 1964-02-12 | 1965-02-11 | |
| NL6501691A NL6501691A (en) | 1964-02-12 | 1965-02-11 | |
| FR5296A FR1429499A (en) | 1964-02-12 | 1965-02-12 | Improvements to the volatilization of liquids |
| FR5297A FR1439898A (en) | 1964-02-12 | 1965-02-12 | Improvements to the volatilization of residual liquid monomers |
| DE19651570084 DE1570084A1 (en) | 1964-02-12 | 1965-02-12 | Process and device for volatilizing or evaporating organic liquids |
| DEP1268A DE1268395B (en) | 1964-02-12 | 1965-02-12 | Process for evaporating an unreacted liquid monomer from the aqueous dispersion of a synthetic polymer |
| GB9195/65A GB1126743A (en) | 1964-02-12 | 1965-03-04 | Preparation of solid polymeric compositions |
| FR52078A FR90414E (en) | 1964-02-12 | 1966-03-04 | Improvements to the volatilization of liquids |
| NL6602831A NL6602831A (en) | 1964-02-12 | 1966-03-04 | |
| DE19661595488 DE1595488A1 (en) | 1964-02-12 | 1966-03-04 | Production of solid polymer compositions |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB579264A GB1090975A (en) | 1964-02-12 | 1964-02-12 | Improvements in or relating to volatilization of organic liquids |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1090975A true GB1090975A (en) | 1967-11-15 |
Family
ID=9802709
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB579264A Expired GB1090975A (en) | 1964-02-12 | 1964-02-12 | Improvements in or relating to volatilization of organic liquids |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1090975A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5521230A (en) * | 1992-11-17 | 1996-05-28 | General Electric Company | Method of dispersing solid additives in polymers and products made therewith |
| US5583166A (en) * | 1991-02-20 | 1996-12-10 | Idemitsu Petrochemical Co., Ltd. | Process for production of polymer particles |
| US6005025A (en) * | 1992-11-17 | 1999-12-21 | General Electric Company | Method of dispersing solid additives in polymers and products made therewith |
| WO2002012374A1 (en) * | 2000-08-03 | 2002-02-14 | Prometic Biosciences Inc. | Apparatus and method for producing porous polymer particles |
-
1964
- 1964-02-12 GB GB579264A patent/GB1090975A/en not_active Expired
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5583166A (en) * | 1991-02-20 | 1996-12-10 | Idemitsu Petrochemical Co., Ltd. | Process for production of polymer particles |
| US5726223A (en) * | 1991-02-20 | 1998-03-10 | Idemitsu Petrochemical Co., Ltd. | Process for production of polymer particles |
| US5521230A (en) * | 1992-11-17 | 1996-05-28 | General Electric Company | Method of dispersing solid additives in polymers and products made therewith |
| US6005025A (en) * | 1992-11-17 | 1999-12-21 | General Electric Company | Method of dispersing solid additives in polymers and products made therewith |
| US6160038A (en) * | 1992-11-17 | 2000-12-12 | General Electric Company | Finely dispersed shell/core solid additives in polymers and products made therewith |
| US6469072B1 (en) | 1992-11-17 | 2002-10-22 | General Electric Company | Finely dispersed shell/core solid additives in polymers and products made therewith |
| WO2002012374A1 (en) * | 2000-08-03 | 2002-02-14 | Prometic Biosciences Inc. | Apparatus and method for producing porous polymer particles |
| AU2001281619B2 (en) * | 2000-08-03 | 2004-06-03 | Prometic Biosciences Inc. | Apparatus and method for producing porous polymer particles |
| US7207499B2 (en) | 2000-08-03 | 2007-04-24 | Prometic Biosciences Ltd | Apparatus and method for producing porous polymer particles |
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