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GB1066938A - Process for drying heat-sensitive materials as well as drying apparatus for the performance of the afore-mentioned process - Google Patents

Process for drying heat-sensitive materials as well as drying apparatus for the performance of the afore-mentioned process

Info

Publication number
GB1066938A
GB1066938A GB16598/65A GB1659865A GB1066938A GB 1066938 A GB1066938 A GB 1066938A GB 16598/65 A GB16598/65 A GB 16598/65A GB 1659865 A GB1659865 A GB 1659865A GB 1066938 A GB1066938 A GB 1066938A
Authority
GB
United Kingdom
Prior art keywords
particles
compartment
wall
vapours
drying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB16598/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of GB1066938A publication Critical patent/GB1066938A/en
Expired legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F5/00—Coffee; Coffee substitutes; Preparations thereof
    • A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
    • A23F5/28—Drying or concentrating coffee extract
    • A23F5/34—Drying or concentrating coffee extract by spraying into a gas stream
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
    • A23B2/00—Preservation of foods or foodstuffs, in general
    • A23B2/90—Preservation of foods or foodstuffs, in general by drying or kilning; Subsequent reconstitution
    • A23B2/92—Freeze drying
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
    • A23B2/00—Preservation of foods or foodstuffs, in general
    • A23B2/90—Preservation of foods or foodstuffs, in general by drying or kilning; Subsequent reconstitution
    • A23B2/93—Spray drying
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C1/00—Concentration, evaporation or drying
    • A23C1/04—Concentration, evaporation or drying by spraying into a gas stream
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C1/00—Concentration, evaporation or drying
    • A23C1/06—Concentration by freezing out the water
    • A23C1/08—Freeze-drying
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
    • A23F5/00—Coffee; Coffee substitutes; Preparations thereof
    • A23F5/24—Extraction of coffee; Coffee extracts; Making instant coffee
    • A23F5/28—Drying or concentrating coffee extract
    • A23F5/32—Drying or concentrating coffee extract by lyophilisation
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof containing fruit or vegetable juices
    • A23L2/08—Concentrating or drying of juices
    • A23L2/12—Concentrating or drying of juices by freezing
    • A23L2/14—Concentrating or drying of juices by freezing and sublimation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/16—Evaporating by spraying
    • B01D1/18—Evaporating by spraying to obtain dry solids
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B17/00—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement
    • F26B17/10—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by fluid currents, e.g. issuing from a nozzle, e.g. pneumatic, flash, vortex or entrainment dryers
    • F26B17/101—Machines or apparatus for drying materials in loose, plastic, or fluidised form, e.g. granules, staple fibres, with progressive movement with movement performed by fluid currents, e.g. issuing from a nozzle, e.g. pneumatic, flash, vortex or entrainment dryers the drying enclosure having the shape of one or a plurality of shafts or ducts, e.g. with substantially straight and vertical axis
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00—Drying solid materials or objects by processes involving the application of heat
    • F26B3/02—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
    • F26B3/10—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it
    • F26B3/12—Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour carrying the materials or objects to be dried with it in the form of a spray, i.e. sprayed or dispersed emulsions or suspensions
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/048—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum in combination with heat developed by electro-magnetic means, e.g. microwave energy
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B5/00—Drying solid materials or objects by processes not involving the application of heat
    • F26B5/04—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum
    • F26B5/06—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing
    • F26B5/065—Drying solid materials or objects by processes not involving the application of heat by evaporation or sublimation of moisture under reduced pressure, e.g. in a vacuum the process involving freezing the product to be freeze-dried being sprayed, dispersed or pulverised
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S159/00—Concentrating evaporators
    • Y10S159/06—Infrared

Landscapes

  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • General Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Microbiology (AREA)
  • Nutrition Science (AREA)
  • Freezing, Cooling And Drying Of Foods (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Drying Of Solid Materials (AREA)

Abstract

1,066,938. Drying foods &c. F. ANDERWERT. April 20, 1965 [April 24, 1964], No. 16598/65. Heading A2D. [Also in Divisions B2 and F4] In apparatus for drying heat-sensitive, atomizable materials, e.g. milk, fruit juices, aroma-rich extracts, in particle form produced either by pre-freezing liquid material in apparatus described with reference to Fig. 4 (not shown), or by delivery through atomizer or sprayer means 18 into a compartment 1 evacuated by a pump 9 and having a heat radiating wall 2, the particles fall by gravity through the chamber and are prevented from contacting the wall 2 by a mesh cylinder 10 coaxially mounted within the compartment. A vortex is formed within the compart ment by an agitator 14 with vanes 14<SP>1</SP> so that the vapours sublimed or evaporated from the particles are caused to flow through a vapour conduit leading to the pump 9 and the dried particles separated therefrom are removed through a valved base 5. A temperature sensing device41 may control the quantity of radiant energy and/or the speed of delivery of the particles to the apparatus as a function of the temperature of the vapour stream. A portion of the vapours from the conduit or condenser 8 therein is delivered by a blower 12 to the annular compartment lb formed between the wall 2 and cylinder 10 and into the compartment 1 to prevent particles contacting the wall 2. In a modification, Fig. 2 (not shown) the agitator 14 is replaced by tangentially introducing the vapours from the blower 12 and the radiant walls in the embodiments of Figs. 2 and 3 may have areas at different temperatures.
GB16598/65A 1964-04-24 1965-04-20 Process for drying heat-sensitive materials as well as drying apparatus for the performance of the afore-mentioned process Expired GB1066938A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CH534764A CH408781A (en) 1964-04-24 1964-04-24 Process for drying atomizable material by sublimation and drying device for carrying out the process

Publications (1)

Publication Number Publication Date
GB1066938A true GB1066938A (en) 1967-04-26

Family

ID=4292049

Family Applications (1)

Application Number Title Priority Date Filing Date
GB16598/65A Expired GB1066938A (en) 1964-04-24 1965-04-20 Process for drying heat-sensitive materials as well as drying apparatus for the performance of the afore-mentioned process

Country Status (6)

Country Link
US (1) US3300868A (en)
CH (1) CH408781A (en)
DE (1) DE1604768A1 (en)
ES (1) ES312609A1 (en)
GB (1) GB1066938A (en)
NL (1) NL6505303A (en)

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2338983C1 (en) * 2007-06-22 2008-11-20 Олег Савельевич Кочетов Boiling bed flash dryer with inert nozzle
RU2340852C1 (en) * 2007-07-26 2008-12-10 Олег Савельевич Кочетов Dryer for suspension bed with impulse-6 type passive nozzle
RU2340851C1 (en) * 2007-07-26 2008-12-10 Олег Савельевич Кочетов Plant for drying in pseudo-liquid bed with passive nozzle
RU2340847C1 (en) * 2007-07-03 2008-12-10 Олег Савельевич Кочетов Suspension bed dryer with passive nozzle
RU2343382C1 (en) * 2007-07-03 2009-01-10 Олег Савельевич Кочетов Device for spray drying and granulating particulates
RU2343384C1 (en) * 2007-07-26 2009-01-10 Олег Савельевич Кочетов Device for spray drying and granulating particulates
RU2343385C1 (en) * 2007-07-26 2009-01-10 Олег Савельевич Кочетов Device for spray drying and granulating pulse-6 type particulates
RU2343383C1 (en) * 2007-07-26 2009-01-10 Олег Савельевич Кочетов Apparatus for drying solutions and suspensions
RU2343378C1 (en) * 2007-06-05 2009-01-10 Общество с ограниченной ответственностью "Производственно-технологический центр "ПРОМИН" Method of drying capillary-porous materials and device to this realisation
EP2270409A4 (en) * 2008-03-19 2012-08-08 Morimoto Pharma Co Ltd METHOD OF FREEZING AND APPARATUS FOR LYOPHILIZATION
RU2646998C1 (en) * 2017-06-26 2018-03-13 Олег Савельевич Кочетов Suspended layer dryer with inert attachment
RU2647001C1 (en) * 2017-06-29 2018-03-13 Олег Савельевич Кочетов Suspended layer dryer with inert attachment

Families Citing this family (30)

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US3620776A (en) * 1968-06-28 1971-11-16 Nestle Sa Spray drying process
GB1288766A (en) * 1969-01-30 1972-09-13
US3731392A (en) * 1971-02-25 1973-05-08 H Gottfried Continuous freeze dryer
US3880668A (en) * 1972-04-05 1975-04-29 Western Consumers Ind Inc Apparatus for producing molasses food product
US3847714A (en) * 1972-06-15 1974-11-12 Dasi Industries Method and apparatus for heat treating liqueform materials
US3837491A (en) * 1972-11-03 1974-09-24 Pollution Control Inc Liquid purification apparatus and process
US4284495A (en) * 1979-12-10 1981-08-18 Newton William A Coating apparatus and method
BR8600564A (en) * 1985-02-11 1986-10-21 Falvourtech Pty Ltd CONTRA-CURRENT CONTACT DEVICE OR DISTILLATION COLUMN, SYSTEM TO REDUCE THE ALCOHOLIC CONTENT OF A DRINK CONTAINING ALCOHOL, SYSTEM TO REDUCE THE ALCOHOLIC CONTENT OF WINE, SYSTEM FOR REMOVING AROMA AND / OR TASTE OF FRUIT JUICE, DE-DESULFURIZING A LIQUID AND PROCESS TO DISTILL, DISTILL BY FRACTIONATION OR REMOVE A SELECTED VOLATILE COMPONENT, OR COMPONENTS OF A LIQUID
FR2635273B1 (en) * 1988-07-21 1990-11-30 Faddi Etienne PROCESS AND PLANT FOR SEPARATING COMPONENTS OF PLANT OR ANIMAL MATERIAL
DE3829013A1 (en) * 1988-08-26 1990-03-08 Heraeus Schott Quarzschmelze Thickening apparatus for jelly-like material
JP2571890B2 (en) * 1992-06-09 1997-01-16 株式会社 佐藤鉄工所 Vacuum drying method and apparatus for neat soap
US5744008A (en) * 1996-01-02 1998-04-28 Oceanit Laboratories, Inc. Hurricane tower water desalination device
US6168141B1 (en) * 1999-03-22 2001-01-02 Artur G. Zimmer Apparatus for treatment of fluent materials
WO2001063191A1 (en) * 2000-02-25 2001-08-30 Glatt Gmbh Method for producing particulate goods
US7575761B2 (en) * 2000-06-30 2009-08-18 Novartis Pharma Ag Spray drying process control of drying kinetics
DE10112167C2 (en) * 2001-03-12 2003-02-13 Bionorica Ag Process for the gentle extraction of dry extracts
JP3824891B2 (en) * 2001-07-06 2006-09-20 共和真空技術株式会社 Dry bulk crushing equipment in freeze-drying equipment for foods and pharmaceuticals
DE102005022154A1 (en) * 2005-05-13 2006-11-16 Degussa Ag Reactor and method for gentle product drying
GB2434195B (en) * 2006-01-12 2010-11-24 Dyson Technology Ltd Drying apparatus
EP2101131A1 (en) * 2007-12-31 2009-09-16 Terruzzi Fercalx S.p.A. Lyophilization method and system therefor
US9945611B2 (en) 2010-08-04 2018-04-17 Ima Life North America Inc. Bulk freeze drying using spray freezing and agitated drying
WO2012018320A1 (en) 2010-08-04 2012-02-09 Ima Life North America Inc. Bulk freeze drying using spray freezing and stirred drying
SE1100493A1 (en) * 2011-06-23 2012-12-24 Dragoljub Perunicic Cyclone distillery / refinery which has steam duct connected impeller / turbine
JP5837670B2 (en) * 2014-10-24 2015-12-24 アイエムエー ライフ ノース アメリカ インコーポレーテッド Bulk freeze drying using spray freezing and stirring drying
US10465985B2 (en) 2015-06-01 2019-11-05 Ima Life North America Inc. Bulk freeze drying using spray freezing and agitated drying with dielectric heating
EP4509208A3 (en) * 2019-12-09 2025-04-16 Grant Prideco, Inc. Apparatus for continuous thermal separation of a multi-component substance
KR20220108173A (en) * 2019-12-09 2022-08-02 헬레네스 홀딩 에이에스 Continuous thermal separation method for multi-component materials
CN112197550A (en) * 2020-10-09 2021-01-08 马鞍山健鼎化工有限公司 Efficient drying device for producing polyaluminium chloride and working method
CN112268432B (en) * 2020-10-22 2021-06-01 盐城市科瑞达科技咨询服务有限公司 An industrial dust dryer
WO2024178110A1 (en) 2023-02-22 2024-08-29 Ima Life North America, Inc. Direct contact spray freezing system

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US996832A (en) * 1907-10-02 1911-07-04 Charles H Campbell Desiccating milk.
US1104920A (en) * 1911-09-27 1914-07-28 Osborne Patented Machinery Co Inc Art of making ice.
US1976204A (en) * 1932-01-08 1934-10-09 Standard Oil Co Process of making ice
US2020719A (en) * 1934-06-12 1935-11-12 Girdler Corp Process and apparatus for solidifying material in finely subdivided form
US2471035A (en) * 1943-10-02 1949-05-24 Frank E Hurd Apparatus for the desiccation of organic substances
US2515098A (en) * 1945-08-01 1950-07-11 Chain Belt Co Continuous low-temperature dehydration
US2533125A (en) * 1946-02-16 1950-12-05 Michael Reese Res Foundation Apparatus for desiccation by ice sublimation
US2751687A (en) * 1952-05-21 1956-06-26 Proctor Drying And Freezing Co Process and apparatus for producing stabilized products
US2800463A (en) * 1953-05-14 1957-07-23 Shawinigan Resins Corp Polyvinyl acetate powder and process of making the same
US2813350A (en) * 1954-03-12 1957-11-19 Commw Eugineering Company Of O Process for concentration of solutions by sublimation
US3024117A (en) * 1958-11-17 1962-03-06 Bar Rup Corp Method of freezing citrus fruit juices

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2343378C1 (en) * 2007-06-05 2009-01-10 Общество с ограниченной ответственностью "Производственно-технологический центр "ПРОМИН" Method of drying capillary-porous materials and device to this realisation
RU2338983C1 (en) * 2007-06-22 2008-11-20 Олег Савельевич Кочетов Boiling bed flash dryer with inert nozzle
RU2340847C1 (en) * 2007-07-03 2008-12-10 Олег Савельевич Кочетов Suspension bed dryer with passive nozzle
RU2343382C1 (en) * 2007-07-03 2009-01-10 Олег Савельевич Кочетов Device for spray drying and granulating particulates
RU2340852C1 (en) * 2007-07-26 2008-12-10 Олег Савельевич Кочетов Dryer for suspension bed with impulse-6 type passive nozzle
RU2340851C1 (en) * 2007-07-26 2008-12-10 Олег Савельевич Кочетов Plant for drying in pseudo-liquid bed with passive nozzle
RU2343384C1 (en) * 2007-07-26 2009-01-10 Олег Савельевич Кочетов Device for spray drying and granulating particulates
RU2343385C1 (en) * 2007-07-26 2009-01-10 Олег Савельевич Кочетов Device for spray drying and granulating pulse-6 type particulates
RU2343383C1 (en) * 2007-07-26 2009-01-10 Олег Савельевич Кочетов Apparatus for drying solutions and suspensions
EP2270409A4 (en) * 2008-03-19 2012-08-08 Morimoto Pharma Co Ltd METHOD OF FREEZING AND APPARATUS FOR LYOPHILIZATION
RU2646998C1 (en) * 2017-06-26 2018-03-13 Олег Савельевич Кочетов Suspended layer dryer with inert attachment
RU2647001C1 (en) * 2017-06-29 2018-03-13 Олег Савельевич Кочетов Suspended layer dryer with inert attachment

Also Published As

Publication number Publication date
US3300868A (en) 1967-01-31
DE1604768A1 (en) 1970-01-29
CH408781A (en) 1966-02-28
NL6505303A (en) 1965-10-25
ES312609A1 (en) 1966-01-01

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