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FR3138523B1 - gas phase physicochemical analysis process - Google Patents

gas phase physicochemical analysis process Download PDF

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Publication number
FR3138523B1
FR3138523B1 FR2207857A FR2207857A FR3138523B1 FR 3138523 B1 FR3138523 B1 FR 3138523B1 FR 2207857 A FR2207857 A FR 2207857A FR 2207857 A FR2207857 A FR 2207857A FR 3138523 B1 FR3138523 B1 FR 3138523B1
Authority
FR
France
Prior art keywords
physicochemical analysis
gas sample
gas phase
analysis process
dichlorine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR2207857A
Other languages
French (fr)
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FR3138523A1 (en
Inventor
Rachid Mouflih
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hemera
Original Assignee
Hemera
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hemera filed Critical Hemera
Priority to FR2207857A priority Critical patent/FR3138523B1/en
Priority to PCT/EP2023/071042 priority patent/WO2024023320A1/en
Priority to EP23745581.1A priority patent/EP4562404A1/en
Publication of FR3138523A1 publication Critical patent/FR3138523A1/en
Application granted granted Critical
Publication of FR3138523B1 publication Critical patent/FR3138523B1/en
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Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/33Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using ultraviolet light
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/005Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods investigating the presence of an element by oxidation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/22Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using chemical indicators
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/0004Gaseous mixtures, e.g. polluted air
    • G01N33/0009General constructional details of gas analysers, e.g. portable test equipment
    • G01N33/0027General constructional details of gas analysers, e.g. portable test equipment concerning the detector
    • G01N33/0036General constructional details of gas analysers, e.g. portable test equipment concerning the detector specially adapted to detect a particular component

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Immunology (AREA)
  • Molecular Biology (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Biophysics (AREA)
  • Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

La présente invention concerne un procédé d’analyse physico-chimique d’un échantillon gazeux comprenant un gaz porteur dans lequel est dilué du dichlore gazeux, le procédé d’analyse physico-chimique comprenant : a) une étape de conversion du dichlore de l’échantillon gazeux en dioxyde de chlore dans une ampoule de conversion ; b) une étape d’acquisition d’un spectre d’absorption de l’échantillon gazeux après exécution de l’étape a) dans une cellule de mesure reliée fluidiquement à l’ampoule de conversion ; c) une étape de traitement mathématique du spectre d’absorption en vue d’en déduire la concentration de dioxyde de chlore dans l’échantillon gazeux. Figure 1The present invention relates to a method for the physicochemical analysis of a gas sample comprising a carrier gas in which gaseous dichlorine is diluted, the physicochemical analysis method comprising: a) a step of converting the dichlorine of the gas sample into chlorine dioxide in a conversion bulb; b) a step of acquiring an absorption spectrum of the gas sample after performing step a) in a measuring cell fluidically connected to the conversion bulb; c) a step of mathematically processing the absorption spectrum in order to deduce therefrom the concentration of chlorine dioxide in the gas sample. Figure 1

FR2207857A 2022-07-29 2022-07-29 gas phase physicochemical analysis process Active FR3138523B1 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
FR2207857A FR3138523B1 (en) 2022-07-29 2022-07-29 gas phase physicochemical analysis process
PCT/EP2023/071042 WO2024023320A1 (en) 2022-07-29 2023-07-28 Gas-phase physico-chemical analysis method
EP23745581.1A EP4562404A1 (en) 2022-07-29 2023-07-28 Gas-phase physico-chemical analysis method

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2207857 2022-07-29
FR2207857A FR3138523B1 (en) 2022-07-29 2022-07-29 gas phase physicochemical analysis process

Publications (2)

Publication Number Publication Date
FR3138523A1 FR3138523A1 (en) 2024-02-02
FR3138523B1 true FR3138523B1 (en) 2024-10-04

Family

ID=83505719

Family Applications (1)

Application Number Title Priority Date Filing Date
FR2207857A Active FR3138523B1 (en) 2022-07-29 2022-07-29 gas phase physicochemical analysis process

Country Status (3)

Country Link
EP (1) EP4562404A1 (en)
FR (1) FR3138523B1 (en)
WO (1) WO2024023320A1 (en)

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4311485A (en) * 1980-12-23 1982-01-19 E. I. Du Pont De Nemours And Company Method and apparatus for photometrically monitoring the concentrations of both chlorine and chlorine dioxide
JPS57113350A (en) * 1981-01-06 1982-07-14 Toyota Motor Corp Determination of chlorine dioxide by ultraviolet spectrophotometery
JP3432571B2 (en) * 1994-02-17 2003-08-04 東亜ディーケーケー株式会社 Method for measuring chlorite ion in solution
US10414651B2 (en) * 2010-08-23 2019-09-17 The Trustees Of Princeton University Iron porphyrazines as efficient, catalytic and scalable method to produce chlorine dioxide
KR101208659B1 (en) * 2011-08-30 2012-12-05 한국기계연구원 Detection method using colorimetric analysis
JP5798230B1 (en) * 2014-11-25 2015-10-21 滝本技研工業株式会社 Chlorine dioxide gas concentration measuring device

Also Published As

Publication number Publication date
EP4562404A1 (en) 2025-06-04
WO2024023320A1 (en) 2024-02-01
FR3138523A1 (en) 2024-02-02

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