FR3120629B1 - Procédé de purification de vanilline ou d’un dérivé de vanilline obtenus par un procédé biotechnologique - Google Patents
Procédé de purification de vanilline ou d’un dérivé de vanilline obtenus par un procédé biotechnologique Download PDFInfo
- Publication number
- FR3120629B1 FR3120629B1 FR2102534A FR2102534A FR3120629B1 FR 3120629 B1 FR3120629 B1 FR 3120629B1 FR 2102534 A FR2102534 A FR 2102534A FR 2102534 A FR2102534 A FR 2102534A FR 3120629 B1 FR3120629 B1 FR 3120629B1
- Authority
- FR
- France
- Prior art keywords
- vanillin
- purifying
- biotechnological
- derivative obtained
- derivatives
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- MWOOGOJBHIARFG-UHFFFAOYSA-N vanillin Chemical compound COC1=CC(C=O)=CC=C1O MWOOGOJBHIARFG-UHFFFAOYSA-N 0.000 title abstract 5
- FGQOOHJZONJGDT-UHFFFAOYSA-N vanillin Natural products COC1=CC(O)=CC(C=O)=C1 FGQOOHJZONJGDT-UHFFFAOYSA-N 0.000 title abstract 4
- 235000012141 vanillin Nutrition 0.000 title abstract 4
- 238000011138 biotechnological process Methods 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- ZENOXNGFMSCLLL-UHFFFAOYSA-N vanillyl alcohol Chemical compound COC1=CC(CO)=CC=C1O ZENOXNGFMSCLLL-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/81—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/79—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/78—Separation; Purification; Stabilisation; Use of additives
- C07C45/80—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P7/00—Preparation of oxygen-containing organic compounds
- C12P7/24—Preparation of oxygen-containing organic compounds containing a carbonyl group
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biotechnology (AREA)
- Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
Titre : Procédé de purification de vanilline ou ses dérivés obtenus par un procédé biotechnologique La présente invention concerne un procédé de purification de vanilline ou ses dérivés, obtenus par un procédé biotechnologique, comprenant au moins une étape dans laquelle la vanilline ou ses dérivés sont séparés de l’alcool vanillique ou ses dérivés par cristallisation. Pas de figure pour l’abrégé
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR2102534A FR3120629B1 (fr) | 2021-03-15 | 2021-03-15 | Procédé de purification de vanilline ou d’un dérivé de vanilline obtenus par un procédé biotechnologique |
| EP22714200.7A EP4308534A1 (fr) | 2021-03-15 | 2022-03-14 | Procede de purification de vanilline ou d'un derive de vanilline obtenus par un procede biotechnologique |
| CN202280021151.8A CN117098747A (zh) | 2021-03-15 | 2022-03-14 | 通过生物技术方法获得的香草醛或香草醛衍生物的纯化方法 |
| BR112023018030A BR112023018030A2 (pt) | 2021-03-15 | 2022-03-14 | Processo para purificação de vanilina ou derivado de vanilina obtido por um processo biotecnológico |
| US18/550,801 US20240190801A1 (en) | 2021-03-15 | 2022-03-14 | Process for the purification of vanillin or a vanillin derivative obtained by a biotechnological process |
| PCT/EP2022/056527 WO2022194771A1 (fr) | 2021-03-15 | 2022-03-14 | Procede de purification de vanilline ou d'un derive de vanilline obtenus par un procede biotechnologique |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR2102534A FR3120629B1 (fr) | 2021-03-15 | 2021-03-15 | Procédé de purification de vanilline ou d’un dérivé de vanilline obtenus par un procédé biotechnologique |
| FR2102534 | 2021-03-15 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR3120629A1 FR3120629A1 (fr) | 2022-09-16 |
| FR3120629B1 true FR3120629B1 (fr) | 2024-01-19 |
Family
ID=75690513
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR2102534A Active FR3120629B1 (fr) | 2021-03-15 | 2021-03-15 | Procédé de purification de vanilline ou d’un dérivé de vanilline obtenus par un procédé biotechnologique |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20240190801A1 (fr) |
| EP (1) | EP4308534A1 (fr) |
| CN (1) | CN117098747A (fr) |
| BR (1) | BR112023018030A2 (fr) |
| FR (1) | FR3120629B1 (fr) |
| WO (1) | WO2022194771A1 (fr) |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2745796A (en) | 1953-10-21 | 1956-05-15 | Aschaffenburger Zellstoffwerke | Method of recovering vanillin |
| DE1132113B (de) | 1959-07-09 | 1962-06-28 | Aschaffenburger Zellstoffwerke | Verfahren zur Reinigung von Vanillin |
| DE3920039A1 (de) | 1989-06-20 | 1991-01-03 | Haarmann & Reimer Gmbh | Verfahren zur herstellung von natuerlichem vanillin |
| CA2238215A1 (fr) | 1997-06-19 | 1998-12-19 | Markus Wetli | Methode d'obtention de vanilline |
| CN101386570B (zh) * | 2007-09-10 | 2010-09-29 | 中国石油天然气集团公司 | 二氧化碳超临界萃取香兰素或乙基香兰素粗制品的方法 |
| EP3514226B1 (fr) | 2011-08-08 | 2023-03-29 | International Flavors & Fragrances Inc. | Compositions et procédés pour la biosynthèse de vanilline ou de la bêta-d-glucoside de vanilline |
| FR2984314B1 (fr) * | 2011-12-15 | 2014-01-17 | Rhodia Operations | Procede de purification de la vanilline par extraction liquide-liquide |
| EP2948424B1 (fr) | 2013-01-24 | 2022-06-01 | Rhodia Operations | Procédé de purification de la vanilline naturelle |
| CN104119213B (zh) * | 2014-06-30 | 2016-04-27 | 上海应用技术学院 | 一种香兰素的制备方法 |
| FR3062652B1 (fr) * | 2017-02-08 | 2020-10-16 | Rhodia Operations | Procede de purification de la vanilline naturelle |
| FR3099477B1 (fr) * | 2019-07-30 | 2023-01-13 | Rhodia Operations | Compositions de vanilline naturelle |
-
2021
- 2021-03-15 FR FR2102534A patent/FR3120629B1/fr active Active
-
2022
- 2022-03-14 US US18/550,801 patent/US20240190801A1/en active Pending
- 2022-03-14 WO PCT/EP2022/056527 patent/WO2022194771A1/fr not_active Ceased
- 2022-03-14 EP EP22714200.7A patent/EP4308534A1/fr active Pending
- 2022-03-14 BR BR112023018030A patent/BR112023018030A2/pt unknown
- 2022-03-14 CN CN202280021151.8A patent/CN117098747A/zh active Pending
Also Published As
| Publication number | Publication date |
|---|---|
| FR3120629A1 (fr) | 2022-09-16 |
| BR112023018030A2 (pt) | 2023-10-03 |
| EP4308534A1 (fr) | 2024-01-24 |
| US20240190801A1 (en) | 2024-06-13 |
| WO2022194771A1 (fr) | 2022-09-22 |
| CN117098747A (zh) | 2023-11-21 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PLFP | Fee payment |
Year of fee payment: 2 |
|
| PLSC | Publication of the preliminary search report |
Effective date: 20220916 |
|
| CA | Change of address |
Effective date: 20221102 |
|
| PLFP | Fee payment |
Year of fee payment: 3 |
|
| PLFP | Fee payment |
Year of fee payment: 4 |
|
| TP | Transmission of property |
Owner name: SPECIALTY OPERATIONS FRANCE, FR Effective date: 20240613 |
|
| PLFP | Fee payment |
Year of fee payment: 5 |