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FR2993882B1 - Procede de preparation d'alkoxyhydroxybenzaldehyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldehyde - Google Patents

Procede de preparation d'alkoxyhydroxybenzaldehyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldehyde

Info

Publication number
FR2993882B1
FR2993882B1 FR1257280A FR1257280A FR2993882B1 FR 2993882 B1 FR2993882 B1 FR 2993882B1 FR 1257280 A FR1257280 A FR 1257280A FR 1257280 A FR1257280 A FR 1257280A FR 2993882 B1 FR2993882 B1 FR 2993882B1
Authority
FR
France
Prior art keywords
alkoxyhydroxybenzaldehyde
alkyl
preparation
substantially free
free
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
FR1257280A
Other languages
English (en)
Other versions
FR2993882A1 (fr
Inventor
Laurent Garel
Hubert Gayet
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Operations SAS
Original Assignee
Rhodia Operations SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1257280A priority Critical patent/FR2993882B1/fr
Application filed by Rhodia Operations SAS filed Critical Rhodia Operations SAS
Priority to BR112015001565A priority patent/BR112015001565A2/pt
Priority to ES13735354.6T priority patent/ES2505475T1/es
Priority to PCT/EP2013/064859 priority patent/WO2014016145A1/fr
Priority to RU2015106362A priority patent/RU2648044C2/ru
Priority to CN201380012015.3A priority patent/CN104203891B/zh
Priority to EP13735354.6A priority patent/EP2760815B1/fr
Priority to US14/417,010 priority patent/US9284247B2/en
Priority to IN10925DEN2014 priority patent/IN2014DN10925A/en
Priority to DE13735354.6T priority patent/DE13735354T1/de
Publication of FR2993882A1 publication Critical patent/FR2993882A1/fr
Application granted granted Critical
Publication of FR2993882B1 publication Critical patent/FR2993882B1/fr
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
    • C07C45/38—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a primary hydroxyl group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/37—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups
    • C07C45/39—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of >C—O—functional groups to >C=O groups being a secondary hydroxyl group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/09—Preparation of ethers by dehydration of compounds containing hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/34—Separation; Purification; Stabilisation; Use of additives
    • C07C41/40—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation
    • C07C41/42—Separation; Purification; Stabilisation; Use of additives by change of physical state, e.g. by crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/54—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of compounds containing doubly bound oxygen atoms, e.g. esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/353—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by isomerisation; by change of size of the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/367—Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of functional groups containing oxygen only in singly bound form
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FR1257280A 2012-07-26 2012-07-26 Procede de preparation d'alkoxyhydroxybenzaldehyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldehyde Expired - Fee Related FR2993882B1 (fr)

Priority Applications (10)

Application Number Priority Date Filing Date Title
FR1257280A FR2993882B1 (fr) 2012-07-26 2012-07-26 Procede de preparation d'alkoxyhydroxybenzaldehyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldehyde
IN10925DEN2014 IN2014DN10925A (fr) 2012-07-26 2013-07-12
PCT/EP2013/064859 WO2014016145A1 (fr) 2012-07-26 2013-07-12 Procédé de préparation d'alkoxyhydroxybenzaldéhyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldéhyde
RU2015106362A RU2648044C2 (ru) 2012-07-26 2013-07-12 Способ получения алкоксигидроксибензальдегида, в существенной степени свободного от алкилалкоксигидроксибензальдегида
CN201380012015.3A CN104203891B (zh) 2012-07-26 2013-07-12 用于生产基本上不含烷基-烷氧基-羟基苯甲醛的烷氧基-羟基苯甲醛的方法
EP13735354.6A EP2760815B1 (fr) 2012-07-26 2013-07-12 Procédé de préparation d'alkoxyhydroxybenzaldéhyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldéhyde
BR112015001565A BR112015001565A2 (pt) 2012-07-26 2013-07-12 processos para preparar pelo menos um alcoxihidroxibenzaldeído, para separar guaiacol e para sintetizar pelo menos um alcoxifenol.
ES13735354.6T ES2505475T1 (es) 2012-07-26 2013-07-12 Procedimiento de preparación de alcoxi-hidroxibenzaldehído sensiblemente exento de alquil-alcoxi-hidroxibenzaldehído
DE13735354.6T DE13735354T1 (de) 2012-07-26 2013-07-12 Verfahren zur herstellung von alkoxy-hydroxybenzaldehyd weitgehend frei von alkyl-alkoxy-hydroxybenzaldehyd
US14/417,010 US9284247B2 (en) 2012-07-26 2013-07-12 Method for producing alkoxy-hydroxybenzaldehyde that is substantially free of alkyl-alkoxy-hydroxybenzaldehyde

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR1257280A FR2993882B1 (fr) 2012-07-26 2012-07-26 Procede de preparation d'alkoxyhydroxybenzaldehyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldehyde

Publications (2)

Publication Number Publication Date
FR2993882A1 FR2993882A1 (fr) 2014-01-31
FR2993882B1 true FR2993882B1 (fr) 2014-08-15

Family

ID=46889297

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1257280A Expired - Fee Related FR2993882B1 (fr) 2012-07-26 2012-07-26 Procede de preparation d'alkoxyhydroxybenzaldehyde sensiblement exempte d'alkyl-alkoxyhydroxybenzaldehyde

Country Status (10)

Country Link
US (1) US9284247B2 (fr)
EP (1) EP2760815B1 (fr)
CN (1) CN104203891B (fr)
BR (1) BR112015001565A2 (fr)
DE (1) DE13735354T1 (fr)
ES (1) ES2505475T1 (fr)
FR (1) FR2993882B1 (fr)
IN (1) IN2014DN10925A (fr)
RU (1) RU2648044C2 (fr)
WO (1) WO2014016145A1 (fr)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9650322B2 (en) 2012-07-26 2017-05-16 Rhodia Operations Method for producing alkoxyhydroxybenzaldehyde
FR2993881B1 (fr) 2012-07-26 2014-08-15 Rhodia Operations Procede de preparation d'alkoxyphenol et d'alkoxyhydroxybenzaldehyde
US11484052B2 (en) 2017-07-28 2022-11-01 Rhodia Operations Vanillin and/or ethylvanillin, process for their preparations and use thereof
US20190031588A1 (en) * 2017-07-28 2019-01-31 Rhodia Operations New vanillin and or ethylvanillin, process for their preparations and use thereof
CN110483253B (zh) * 2019-07-25 2022-05-06 中国林业科学研究院林产化学工业研究所 一种蒸汽辅助固定床热解木质素制备愈创木酚类产物的方法
CN112608221B (zh) * 2020-12-11 2022-11-08 万华化学集团股份有限公司 一种藜芦醚的制备方法
CN113173906B (zh) * 2021-04-16 2022-11-04 兄弟科技股份有限公司 一种胡椒醛的合成方法
CN114736118B (zh) * 2022-04-26 2023-05-09 重庆欣欣向荣精细化工有限公司 一种3-甲氧基-4-羟基扁桃酸分离及其高纯度产物制备方法
CN115974662B (zh) * 2022-12-01 2024-09-03 兄弟科技股份有限公司 一种生物基香兰素或乙基香兰素的合成方法

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU55779A1 (ru) * 1938-11-07 1938-11-30 М.А. Яхилевич Способ получени ванилина
US4165341A (en) 1977-02-04 1979-08-21 Ube Industries, Ltd. Process for preparing protocatechualdehyde and its derivatives
SU1181260A1 (ru) * 1983-08-12 1995-05-27 Калужский филиал Всесоюзного научно-исследовательского института синтетических и натуральных душистых веществ Способ получения метилового и этилового моноэфиров пирокатехина
JPH0463110A (ja) * 1990-07-03 1992-02-28 Ube Ind Ltd アルコール含有反応液の分離精製法
US5248835A (en) 1991-04-19 1993-09-28 Ube Industries, Ltd. Method of producing a monoalkylether of a dihydric phenol compound
FR2693458B1 (fr) 1992-07-10 1994-12-09 Rhone Poulenc Chimie Procédé de para-hydroxyalkylation de composés aromatiques hydroxylés.
US5977416A (en) 1997-04-15 1999-11-02 Ube Industries, Ltd. Dehydration catalyst and process for producing a monoalkylether of a dihydric phenolic compound using same
EP0914854B1 (fr) 1997-10-28 2004-01-14 Ube Industries, Ltd. Appareil et procédé pour générer des vapeurs constitués d'un mélange de plusieurs composants
EP0933107B1 (fr) 1998-01-30 2005-10-26 Ube Industries, Ltd. Procédé pour la séparation d'un composé thermosensible d'une mélange liquide a multiples composants par destillation
FR2779718B1 (fr) 1998-06-16 2000-12-29 Rhodia Chimie Sa Procede de preparation de composes p-hydroxymandeliques eventuellement substitues et derives
FR2917085B1 (fr) 2007-06-06 2009-07-17 Rhodia Recherches & Tech Procede de preparation d'un aldehyde hydroxyaromatique.
FR2925047B1 (fr) 2007-12-18 2010-01-01 Rhodia Operations Procede de preparation de composes p-hydroxymandeliques eventuellement substitues et derives.
FR2931476B1 (fr) 2008-05-22 2012-12-28 Rhodia Operations Procede de separation d'un compose phenolique sous forme solifiee
FR2933974B1 (fr) 2008-07-18 2010-09-17 Rhodia Operations Procede de separation d'un aldehyde aromatique
CN101492353A (zh) * 2009-03-13 2009-07-29 北京化工大学 一种甲醇法制备愈创木酚的方法
FR2950886B1 (fr) 2009-10-02 2011-10-28 Rhodia Operations Procede de separation de composes phenoliques sous forme salifiee
CN102010310B (zh) 2010-10-21 2013-04-10 宁波王龙科技股份有限公司 一种香兰素的乙醛酸法生产工艺
FR2993881B1 (fr) 2012-07-26 2014-08-15 Rhodia Operations Procede de preparation d'alkoxyphenol et d'alkoxyhydroxybenzaldehyde

Also Published As

Publication number Publication date
US9284247B2 (en) 2016-03-15
RU2015106362A (ru) 2016-09-20
FR2993882A1 (fr) 2014-01-31
EP2760815A1 (fr) 2014-08-06
ES2505475T1 (es) 2014-10-10
EP2760815B1 (fr) 2016-08-24
BR112015001565A2 (pt) 2017-07-04
WO2014016145A1 (fr) 2014-01-30
DE13735354T1 (de) 2014-09-11
US20150203428A1 (en) 2015-07-23
CN104203891B (zh) 2019-03-15
CN104203891A (zh) 2014-12-10
RU2648044C2 (ru) 2018-03-22
IN2014DN10925A (fr) 2015-09-18

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