FR2846965A1 - Procede de fabrication de 1,2-epoxy-3-chloropropane - Google Patents
Procede de fabrication de 1,2-epoxy-3-chloropropaneInfo
- Publication number
- FR2846965A1 FR2846965A1 FR0214207A FR0214207A FR2846965A1 FR 2846965 A1 FR2846965 A1 FR 2846965A1 FR 0214207 A FR0214207 A FR 0214207A FR 0214207 A FR0214207 A FR 0214207A FR 2846965 A1 FR2846965 A1 FR 2846965A1
- Authority
- FR
- France
- Prior art keywords
- epichlorohydrin
- production
- hydrogen peroxide
- allyl chloride
- comprises controlling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 title abstract 4
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 title abstract 3
- OSDWBNJEKMUWAV-UHFFFAOYSA-N Allyl chloride Chemical compound ClCC=C OSDWBNJEKMUWAV-UHFFFAOYSA-N 0.000 title abstract 2
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/02—Synthesis of the oxirane ring
- C07D301/03—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds
- C07D301/12—Synthesis of the oxirane ring by oxidation of unsaturated compounds, or of mixtures of unsaturated and saturated compounds with hydrogen peroxide or inorganic peroxides or peracids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Epoxy Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Procédé de fabrication de 1,2-époxy-3-chloropropane par réaction entre du chlorure d'allyle et du peroxyde d'hydrogène en présence d'un catalyseur et en présence éventuelle d'au moins un solvant dans un milieu d'époxydation comprenant au moins une phase liquide, dans lequel le pH de la phase liquide est contrôlé et maintenu à une valeur supérieure ou égale à 1,5 et inférieure à 4,8.
Priority Applications (13)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0214207A FR2846965B1 (fr) | 2002-11-12 | 2002-11-12 | Procede de fabrication de 1,2-epoxy-3-chloropropane |
| RU2005118075/04A RU2323213C2 (ru) | 2002-11-12 | 2003-11-10 | Способ получения 1,2-эпокси-3-хлорпропана |
| PCT/EP2003/012506 WO2004048353A1 (fr) | 2002-11-12 | 2003-11-10 | Procede d'obtention de 1,2-epoxy-3-chloropropane |
| AU2003302392A AU2003302392A1 (en) | 2002-11-12 | 2003-11-10 | Process for the manufacture of 1,2-epoxy-3-chloropropane |
| AT03811753T ATE399771T1 (de) | 2002-11-12 | 2003-11-10 | Verfahren zur herstellung von 1,2-epoxy-3- chlorpropan |
| JP2004554328A JP2006514930A (ja) | 2002-11-12 | 2003-11-10 | 1,2−エポキシ−3−クロロプロパンの製造方法 |
| DE60321948T DE60321948D1 (de) | 2002-11-12 | 2003-11-10 | Verfahren zur herstellung von 1,2-epoxy-3-chlorpropan |
| KR1020057008454A KR101081780B1 (ko) | 2002-11-12 | 2003-11-10 | 1,2-에폭시-3-클로로프로판의 제조 방법 |
| US10/534,502 US8058459B2 (en) | 2002-11-12 | 2003-11-10 | Process for the manufacture of 1,2-epoxy-3-chloropropane |
| EP03811753A EP1562926B1 (fr) | 2002-11-12 | 2003-11-10 | Procede d'obtention de 1,2-epoxy-3-chloropropane |
| ES03811753T ES2309395T3 (es) | 2002-11-12 | 2003-11-10 | Proceso para la fabricacion de 1,2-epoxi-3-cloropropano. |
| CNB2003801030150A CN100478334C (zh) | 2002-11-12 | 2003-11-10 | 生产1,2-环氧-3-氯丙烷的方法 |
| JP2011051477A JP2011132254A (ja) | 2002-11-12 | 2011-03-09 | 1,2−エポキシ−3−クロロプロパンの製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0214207A FR2846965B1 (fr) | 2002-11-12 | 2002-11-12 | Procede de fabrication de 1,2-epoxy-3-chloropropane |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2846965A1 true FR2846965A1 (fr) | 2004-05-14 |
| FR2846965B1 FR2846965B1 (fr) | 2006-10-13 |
Family
ID=32116603
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR0214207A Expired - Fee Related FR2846965B1 (fr) | 2002-11-12 | 2002-11-12 | Procede de fabrication de 1,2-epoxy-3-chloropropane |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8058459B2 (fr) |
| EP (1) | EP1562926B1 (fr) |
| JP (2) | JP2006514930A (fr) |
| KR (1) | KR101081780B1 (fr) |
| CN (1) | CN100478334C (fr) |
| AT (1) | ATE399771T1 (fr) |
| AU (1) | AU2003302392A1 (fr) |
| DE (1) | DE60321948D1 (fr) |
| ES (1) | ES2309395T3 (fr) |
| FR (1) | FR2846965B1 (fr) |
| RU (1) | RU2323213C2 (fr) |
| WO (1) | WO2004048353A1 (fr) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008122503A1 (fr) * | 2007-04-05 | 2008-10-16 | Solvay (Société Anonyme) | Solution aqueuse de peroxyde d'hydrogène, son procédé de préparation et son utilisation |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2846964B1 (fr) * | 2002-11-12 | 2006-07-21 | Procede de fabrication de 1,2-epoxy-3-chloropropane | |
| FR2846965B1 (fr) * | 2002-11-12 | 2006-10-13 | Procede de fabrication de 1,2-epoxy-3-chloropropane | |
| CN101279961B (zh) * | 2007-04-04 | 2013-05-08 | 中国石油化工股份有限公司 | 氯丙烯环氧化生产环氧氯丙烷的方法 |
| CN101279958B (zh) * | 2007-04-04 | 2011-01-19 | 中国石油化工股份有限公司上海石油化工研究院 | 氯丙烯环氧化制备环氧氯丙烷的方法 |
| EP2103604A1 (fr) | 2008-03-17 | 2009-09-23 | Evonik Degussa GmbH | Procédé de fabrication d'épichlorhydrine |
| EP2149569A1 (fr) | 2008-08-01 | 2010-02-03 | Hexion Specialty Chemicals Research Belgium S.A. | Procédé de fabrication d'un 1,2-epoxyde |
| EP2149570A1 (fr) | 2008-08-01 | 2010-02-03 | Hexion Specialty Chemicals Research Belgium S.A. | Procédé de fabrication d'épichlorhydrine avec peroxyde d'hydrogène et un complexe manganèse |
| WO2011062608A2 (fr) | 2009-11-19 | 2011-05-26 | Dow Global Technologies, Inc. | Epoxydation d'une oléfine |
| EP2343288A1 (fr) | 2009-11-27 | 2011-07-13 | Momentive Specialty Chemicals Research Belgium S.A. | Processus de fabrication d'oxyde de propylène |
| EP2354131A1 (fr) * | 2010-02-02 | 2011-08-10 | Momentive Specialty Chemicals Research Belgium | Procédé de fabrication de 1,2-époxyde et dispositif pour effectuer ce procédé |
| EP2354129A1 (fr) * | 2010-02-02 | 2011-08-10 | Momentive Specialty Chemicals Research Belgium S.A. | Procédé d'époxydation |
| EP2354130A1 (fr) | 2010-02-02 | 2011-08-10 | Momentive Specialty Chemicals Research Belgium | Fabrication de carboxylate époxyéhtyl ou carboxylate glycidylique |
| EP2357180A1 (fr) | 2010-02-02 | 2011-08-17 | Momentive Specialty Chemicals Research Belgium S.A. | Fabrication d'éthers d'époxyethyl ou esters glycidyliques |
| JP2011213716A (ja) * | 2010-03-15 | 2011-10-27 | Mitsubishi Chemicals Corp | ポリアリルオキシ化合物の製造方法及びポリグリシジルオキシ化合物の製造方法 |
| WO2012101176A1 (fr) | 2011-01-27 | 2012-08-02 | Solvay Sa | Procédé de fabrication du 1,2-époxy-3-chloropropane |
| WO2012101175A1 (fr) | 2011-01-27 | 2012-08-02 | Solvay Sa | Procédé de production de 1,2-époxy-3-chloropropane |
| EP2670742B1 (fr) * | 2011-02-04 | 2015-07-29 | Dow Global Technologies LLC | Un procédé pour l'élimination des ions de fer contenus dans un courant organique |
| EP2537836A1 (fr) * | 2011-06-22 | 2012-12-26 | Momentive Specialty Chemicals Research Belgium S.A. | Appareil et procédés permettant de préserver l'activité de catalyseur dans un procédé d'époxydation |
| CN115894400B (zh) * | 2022-12-01 | 2024-02-02 | 中国科学院大连化学物理研究所 | 一种应用液固循环流化床反应器直接氧化氯丙烯制环氧氯丙烷的工艺 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6288248B1 (en) * | 1997-11-27 | 2001-09-11 | Solvay (Société Anonyme) | Epichlorohydrin-based product and process for manufacturing this product |
| US6350888B1 (en) * | 1997-09-18 | 2002-02-26 | Solvay (Societe Anonyme) | Method for making an oxirane |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH04327582A (ja) * | 1991-04-24 | 1992-11-17 | Mitsui Toatsu Chem Inc | エピクロロヒドリンの製造方法 |
| TW372231B (en) | 1994-07-22 | 1999-10-21 | Shell Int Research | Purification of allyl chloride |
| US5646314A (en) * | 1994-11-16 | 1997-07-08 | Arco Chemical Technology, L.P. | Process for titanium silicalite-catalyzed epoxidation |
| JP3614548B2 (ja) * | 1994-12-26 | 2005-01-26 | 三菱化学株式会社 | 過酸化水素水の精製法 |
| BE1010717A3 (fr) * | 1996-10-25 | 1998-12-01 | Solvay | Procede de regeneration de catalyseurs. |
| JPH10291986A (ja) * | 1997-04-18 | 1998-11-04 | Mitsubishi Gas Chem Co Inc | オレフィン系炭化水素及びそのハロゲン化物のエポキシ化方法 |
| JP4016461B2 (ja) * | 1997-09-04 | 2007-12-05 | ダイソー株式会社 | オレフィンの選択的エポキシ化法 |
| GB2331071A (en) | 1997-11-11 | 1999-05-12 | Solvay | Manufacture of micro spherical zeolite containing catalyst particles |
| BE1011577A3 (fr) | 1997-11-27 | 1999-11-09 | Solvay | Catalyseur d'epoxydation, son utilisation et procede d'epoxydation en presence de catalyseur. |
| BE1011851A3 (fr) * | 1998-03-24 | 2000-02-01 | Solvay | Procede de fabrication d'un oxiranne. |
| IT1313572B1 (it) * | 1999-07-27 | 2002-09-09 | Enichem Spa | Procedimento per la preparazione di epossidi. |
| DE19936547A1 (de) * | 1999-08-04 | 2001-02-15 | Basf Ag | Verfahren zur Umsetzung einer organischen Verbindung mit einem Hydroperoxid |
| DE19944839A1 (de) * | 1999-09-18 | 2001-03-22 | Degussa | Verfahren zur Herstellung von Epoxiden aus Olefinen |
| JP4397084B2 (ja) * | 1999-12-27 | 2010-01-13 | 旭化成イーマテリアルズ株式会社 | 新規脂環基含有化合物及びその製造方法 |
| EP1122249A1 (fr) * | 2000-02-02 | 2001-08-08 | SOLVAY (Société Anonyme) | Procédé de fabrication d'un oxiranne |
| FR2806084A1 (fr) * | 2000-03-10 | 2001-09-14 | Solvay | Procede de fabrication d'un oxiranne |
| FR2846964B1 (fr) * | 2002-11-12 | 2006-07-21 | Procede de fabrication de 1,2-epoxy-3-chloropropane | |
| FR2846965B1 (fr) * | 2002-11-12 | 2006-10-13 | Procede de fabrication de 1,2-epoxy-3-chloropropane |
-
2002
- 2002-11-12 FR FR0214207A patent/FR2846965B1/fr not_active Expired - Fee Related
-
2003
- 2003-11-10 DE DE60321948T patent/DE60321948D1/de not_active Expired - Lifetime
- 2003-11-10 JP JP2004554328A patent/JP2006514930A/ja active Pending
- 2003-11-10 CN CNB2003801030150A patent/CN100478334C/zh not_active Expired - Fee Related
- 2003-11-10 KR KR1020057008454A patent/KR101081780B1/ko not_active Expired - Fee Related
- 2003-11-10 RU RU2005118075/04A patent/RU2323213C2/ru not_active IP Right Cessation
- 2003-11-10 US US10/534,502 patent/US8058459B2/en not_active Expired - Fee Related
- 2003-11-10 EP EP03811753A patent/EP1562926B1/fr not_active Revoked
- 2003-11-10 ES ES03811753T patent/ES2309395T3/es not_active Expired - Lifetime
- 2003-11-10 AU AU2003302392A patent/AU2003302392A1/en not_active Abandoned
- 2003-11-10 AT AT03811753T patent/ATE399771T1/de not_active IP Right Cessation
- 2003-11-10 WO PCT/EP2003/012506 patent/WO2004048353A1/fr not_active Ceased
-
2011
- 2011-03-09 JP JP2011051477A patent/JP2011132254A/ja active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6350888B1 (en) * | 1997-09-18 | 2002-02-26 | Solvay (Societe Anonyme) | Method for making an oxirane |
| US6288248B1 (en) * | 1997-11-27 | 2001-09-11 | Solvay (Société Anonyme) | Epichlorohydrin-based product and process for manufacturing this product |
Non-Patent Citations (2)
| Title |
|---|
| VENTURELLO C ET AL: "A NEW, EFFECTIVE CATALYTIC SYSTEM FOR EPOXIDATION OF OLEFINS BY HYDROGEN PEROXIDE UNDER PHASE-TRANSFER CONDITIONS", JOURNAL OF ORGANIC CHEMISTRY, AMERICAN CHEMICAL SOCIETY, WASHINGTON, DC, US, vol. 48, no. 21, 21 October 1983 (1983-10-21), pages 3831 - 3833, XP001012726, ISSN: 0022-3263 * |
| VENTURELLO, C. ET AL.: "Quaternary Ammonium Tetrakis(diperoxotungsto) phosphates(3-) as a New Class of Catalysts for Efficient Alkene Epoxidation with Hydrogen Peroxide", JOURNAL OF ORGANIC CHEMISTRY, vol. 53, no. 7, 1988, pages 1553 - 1557, XP002235620 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008122503A1 (fr) * | 2007-04-05 | 2008-10-16 | Solvay (Société Anonyme) | Solution aqueuse de peroxyde d'hydrogène, son procédé de préparation et son utilisation |
| US8558020B2 (en) | 2007-04-05 | 2013-10-15 | Solvay (Societe Anonyme) | Aqueous hydrogen peroxide solution, process for its preparation and use thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| RU2005118075A (ru) | 2006-01-20 |
| WO2004048353A1 (fr) | 2004-06-10 |
| DE60321948D1 (de) | 2008-08-14 |
| ATE399771T1 (de) | 2008-07-15 |
| KR101081780B1 (ko) | 2011-11-09 |
| KR20050074600A (ko) | 2005-07-18 |
| JP2006514930A (ja) | 2006-05-18 |
| CN1711253A (zh) | 2005-12-21 |
| EP1562926A1 (fr) | 2005-08-17 |
| AU2003302392A1 (en) | 2004-06-18 |
| FR2846965B1 (fr) | 2006-10-13 |
| US20060041150A1 (en) | 2006-02-23 |
| ES2309395T3 (es) | 2008-12-16 |
| JP2011132254A (ja) | 2011-07-07 |
| RU2323213C2 (ru) | 2008-04-27 |
| US8058459B2 (en) | 2011-11-15 |
| EP1562926B1 (fr) | 2008-07-02 |
| CN100478334C (zh) | 2009-04-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |
Effective date: 20160729 |