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FR2394512A1 - Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle - Google Patents

Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle

Info

Publication number
FR2394512A1
FR2394512A1 FR7718136A FR7718136A FR2394512A1 FR 2394512 A1 FR2394512 A1 FR 2394512A1 FR 7718136 A FR7718136 A FR 7718136A FR 7718136 A FR7718136 A FR 7718136A FR 2394512 A1 FR2394512 A1 FR 2394512A1
Authority
FR
France
Prior art keywords
tri
acrylic acid
butyl phosphate
separation
solutions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7718136A
Other languages
English (en)
Other versions
FR2394512B1 (fr
Inventor
Georges Biola
Yves Komorn
Gerard Schneider
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhone Poulenc Industries SA
Original Assignee
Rhone Poulenc Industries SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhone Poulenc Industries SA filed Critical Rhone Poulenc Industries SA
Priority to FR7718136A priority Critical patent/FR2394512A1/fr
Priority to DE7878400011T priority patent/DE2862438D1/de
Priority to EP78400011A priority patent/EP0000110B1/fr
Priority to US05/914,923 priority patent/US4219389A/en
Priority to BR787803779A priority patent/BR7803779A/pt
Priority to MX10108678U priority patent/MX5447E/es
Priority to CA305,325A priority patent/CA1103196A/fr
Priority to IT49856/78A priority patent/IT1105727B/it
Priority to JP7045478A priority patent/JPS5416421A/ja
Priority to ES470776A priority patent/ES470776A1/es
Priority to SU782627502A priority patent/SU963461A3/ru
Publication of FR2394512A1 publication Critical patent/FR2394512A1/fr
Application granted granted Critical
Publication of FR2394512B1 publication Critical patent/FR2394512B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention se rapporte à la séparation d'acide acrylique à partir de ses solutions dans le phosphate de tri-n-butyle. Le procédé consiste : a. à constituer une phase vapeur comprenant tout l'acide acrylique et une partie du phosphate de tri-n-butyle par chauffage de la solution de départ dans des conditions qui évitent la dégradation du phosphate de tri-n-butyle, b. puis, après condensation partielle ou totale de la phase vapeur, à effectuer, à partir de cette phase, une distillation d'acide acrylique en maintenant dans le pied de la colonne une teneur en acide acrylique suffisante pour éviter la dégradation du phosphate de tri-n-butyle dans les conditions opératoires, c. éventuellement à recycler à l'alimentation du stade a le résidu de distillation du stade b.
FR7718136A 1977-06-14 1977-06-14 Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle Granted FR2394512A1 (fr)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FR7718136A FR2394512A1 (fr) 1977-06-14 1977-06-14 Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle
DE7878400011T DE2862438D1 (en) 1977-06-14 1978-06-05 Process for obtaining acrylic acid from its solutions in tri-n-butyl phosphate
EP78400011A EP0000110B1 (fr) 1977-06-14 1978-06-05 Procédé d'obtention d'acide acrylique à partir de ses solutions dans le phosphate de tri-n-butyle.
US05/914,923 US4219389A (en) 1977-06-14 1978-06-12 Separation of acrylic acid from solutions thereof in tri-n-butyl phosphate
MX10108678U MX5447E (es) 1977-06-14 1978-06-13 Procedimiento de separacion de acido acrilico a partir de sus soluciones en fosfato de tri-n-butilo
CA305,325A CA1103196A (fr) 1977-06-14 1978-06-13 Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle
BR787803779A BR7803779A (pt) 1977-06-14 1978-06-13 Processo de preparacao de acido acrilico a partir de suas solucoes em fosfato de tri-n-butila
IT49856/78A IT1105727B (it) 1977-06-14 1978-06-13 Procedimento di separazione di acido acrilico a partire dalle sue soluzioni nel fosfato di tri-n-butile
JP7045478A JPS5416421A (en) 1977-06-14 1978-06-13 Method of separating acrylic acid from triinnbutylphosphate solution
ES470776A ES470776A1 (es) 1977-06-14 1978-06-14 Procedimiento para la separacion de acido acrilico a partir de sus soluciones en fosfato de tri-n-butilo
SU782627502A SU963461A3 (ru) 1977-06-14 1978-06-14 Способ выделени акриловой кислоты

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7718136A FR2394512A1 (fr) 1977-06-14 1977-06-14 Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle

Publications (2)

Publication Number Publication Date
FR2394512A1 true FR2394512A1 (fr) 1979-01-12
FR2394512B1 FR2394512B1 (fr) 1980-01-18

Family

ID=9192057

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7718136A Granted FR2394512A1 (fr) 1977-06-14 1977-06-14 Procede de separation d'acide acrylique a partir de ses solutions dans le phosphate de tri-n-butyle

Country Status (10)

Country Link
US (1) US4219389A (fr)
EP (1) EP0000110B1 (fr)
JP (1) JPS5416421A (fr)
BR (1) BR7803779A (fr)
CA (1) CA1103196A (fr)
DE (1) DE2862438D1 (fr)
ES (1) ES470776A1 (fr)
FR (1) FR2394512A1 (fr)
IT (1) IT1105727B (fr)
SU (1) SU963461A3 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010064250A1 (de) 2010-12-28 2012-06-28 Evonik Degussa Gmbh Verfahren zur Herstellung von Methylmercaptopropionaldehyd

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6098794A (ja) * 1983-11-04 1985-06-01 Matsushita Electric Ind Co Ltd 圧電型電気音響変換器
JPS61159899A (ja) * 1985-01-08 1986-07-19 Kimio Takahashi 圧電スピ−カ
JPS61159900A (ja) * 1985-01-08 1986-07-19 Kimio Takahashi 圧電スピ−カ
JPS61161100A (ja) * 1985-01-09 1986-07-21 Kimio Takahashi 圧電スピ−カ
DE3629093A1 (de) * 1986-08-27 1988-03-10 Stettner & Co Piezokeramischer schallwandler
JPH01176200A (ja) * 1987-12-29 1989-07-12 Nec Corp 圧電振動板
JPH04105795U (ja) * 1991-02-23 1992-09-11 太陽誘電株式会社 圧電音響装置
FR2735989B1 (fr) * 1995-06-29 1997-08-14 Rhone Poulenc Nutrition Animal Procede et installation de purification d'un flux gazeux contenant de l'acroleine
DE19740252A1 (de) * 1997-09-12 1999-03-18 Basf Ag Verfahren zur Herstellung von Acrylsäure und Methacrylsäure
DE19833049A1 (de) * 1998-07-22 2000-01-27 Basf Ag Verfahren zur Herstellung von Acrylsäure
DE19838783A1 (de) * 1998-08-26 2000-03-02 Basf Ag Verfahren zur kontinuierlichen Gewinnung von (Meth)acrylsäure
NL1013682C2 (nl) * 1999-11-26 2001-05-30 Purac Biochem Bv Werkwijze en inrichting voor het zuiveren van een waterige oplossing van melkzuur.
US20030150705A1 (en) * 2002-01-08 2003-08-14 Deshpande Sanjeev D. Acrylic acid recovery utilizing ethyl acrylate and selected co-solvents
DE10220494A1 (de) * 2002-05-07 2003-11-20 Basf Ag Verfahren zur Herstellung einer wässrigen Alkaliacrylat-Lösung
DE10347664A1 (de) 2003-10-09 2004-12-02 Basf Ag Verfahren der rektifikativen Auftrennung einer Acrylsäure enthaltenden Flüssigkeit
TWI337996B (en) * 2003-10-09 2011-03-01 Basf Ag Rectificative separation of an acrylic acid-containing liquid

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3092587A (en) * 1959-07-22 1963-06-04 Bergwerksgesellschaft Hibernia Process for the production of high percentage solutions of organic peroxides
FR1359885A (fr) * 1963-03-21 1964-04-30 Electrochimie Soc Procédé de fabrication d'acide acrylique glacial
US3555082A (en) * 1966-12-15 1971-01-12 Knapsack Ag Process for isolating acrylic acid from the reaction gases obtained by oxidation of propylene or acrolein
AT274743B (de) * 1967-09-28 1969-09-25 Krems Chemie Gmbh Verfahren und Vorrichtung zur kontinuierlichen Fraktionierung von Tallöl oder andern organischen Mehrstoffgemischen
US3697387A (en) * 1968-05-16 1972-10-10 Buss Ag Process and device for the purification of a mixture of organic substances of high molecular weight
NL180579C (nl) * 1972-05-24 1987-03-16 Sumitomo Chemical Co Werkwijze voor het scheiden van een mengsel bestaande uit acrylzuur, azijnzuur en water.
US4043873A (en) * 1973-06-15 1977-08-23 Societa' Italiana Resine S.I.R. S.P.A. Plural stage recovery of trioxane in a process having a molecular distillation step

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102010064250A1 (de) 2010-12-28 2012-06-28 Evonik Degussa Gmbh Verfahren zur Herstellung von Methylmercaptopropionaldehyd

Also Published As

Publication number Publication date
FR2394512B1 (fr) 1980-01-18
DE2862438D1 (en) 1984-10-04
ES470776A1 (es) 1979-02-01
IT7849856A0 (it) 1978-06-13
BR7803779A (pt) 1979-02-20
IT1105727B (it) 1985-11-04
US4219389A (en) 1980-08-26
EP0000110B1 (fr) 1984-08-29
CA1103196A (fr) 1981-06-16
JPS5711896B2 (fr) 1982-03-08
SU963461A3 (ru) 1982-09-30
EP0000110A1 (fr) 1978-12-20
JPS5416421A (en) 1979-02-07

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