ES8304572A2 - Process for recovering caffeine from activated carbon. - Google Patents
Process for recovering caffeine from activated carbon.Info
- Publication number
- ES8304572A2 ES8304572A2 ES512478A ES512478A ES8304572A2 ES 8304572 A2 ES8304572 A2 ES 8304572A2 ES 512478 A ES512478 A ES 512478A ES 512478 A ES512478 A ES 512478A ES 8304572 A2 ES8304572 A2 ES 8304572A2
- Authority
- ES
- Spain
- Prior art keywords
- caffeine
- activated carbon
- recovering caffeine
- recovering
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- RYYVLZVUVIJVGH-UHFFFAOYSA-N caffeine Chemical compound CN1C(=O)N(C)C(=O)C2=C1N=CN2C RYYVLZVUVIJVGH-UHFFFAOYSA-N 0.000 title abstract 10
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title abstract 5
- LPHGQDQBBGAPDZ-UHFFFAOYSA-N Isocaffeine Natural products CN1C(=O)N(C)C(=O)C2=C1N(C)C=N2 LPHGQDQBBGAPDZ-UHFFFAOYSA-N 0.000 title abstract 5
- 229960001948 caffeine Drugs 0.000 title abstract 5
- VJEONQKOZGKCAK-UHFFFAOYSA-N caffeine Natural products CN1C(=O)N(C)C(=O)C2=C1C=CN2C VJEONQKOZGKCAK-UHFFFAOYSA-N 0.000 title abstract 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 238000011084 recovery Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23F—COFFEE; TEA; THEIR SUBSTITUTES; MANUFACTURE, PREPARATION, OR INFUSION THEREOF
- A23F5/00—Coffee; Coffee substitutes; Preparations thereof
- A23F5/20—Reducing or removing alkaloid content; Preparations produced thereby; Extracts or infusions thereof
- A23F5/22—Reducing or removing alkaloid content from coffee extract
- A23F5/223—Reducing or removing alkaloid content from coffee extract using flocculating, precipitating, adsorbing or complex-forming agents, or ion-exchangers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D473/00—Heterocyclic compounds containing purine ring systems
- C07D473/02—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6
- C07D473/04—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms
- C07D473/06—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3
- C07D473/12—Heterocyclic compounds containing purine ring systems with oxygen, sulphur, or nitrogen atoms directly attached in positions 2 and 6 two oxygen atoms with radicals containing only hydrogen and carbon atoms, attached in position 1 or 3 with methyl radicals in positions 1, 3, and 7, e.g. caffeine
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Carbon And Carbon Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Saccharide Compounds (AREA)
- Tea And Coffee (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The recovery of caffeine from activated carbon is accomplished according to the present invention by employing an aqueous acetic acid solution, preferably having a concentration of between about 50 and 80% by weight, and which is capable of competing for the active sites on the carbon occupied by the caffeine to displace at least a portion of the caffeine which is then dissolved in the solvent. After the desired period of contact, preferably at a temperature above 100 DEG C, the caffeine is separated from the solution.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US30627681A | 1981-09-28 | 1981-09-28 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES8304572A2 true ES8304572A2 (en) | 1983-03-01 |
| ES512478A0 ES512478A0 (en) | 1983-03-01 |
Family
ID=23184580
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES512478A Granted ES512478A0 (en) | 1981-09-28 | 1982-05-24 | "IMPROVEMENTS INTRODUCED IN THE PURPOSE OF MAIN PATENT N 503.050, REQUESTED ON JUNE 15, 1981, BY: A PROCEDURE TO RECOVER CAFFEINE FROM ACTIVATED CARBON". |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP0076620B2 (en) |
| AT (1) | ATE15043T1 (en) |
| DE (1) | DE3265628D1 (en) |
| ES (1) | ES512478A0 (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ATE26981T1 (en) * | 1983-06-22 | 1987-05-15 | Hag Ag | RECOVERY OF CAFFEINE-LOADED CHARCOAL WITH HOT WATER. |
| ATE26718T1 (en) * | 1983-06-22 | 1987-05-15 | Hag Ag | RECOVERY OF CAFFEINE ADSORBED ON ACTIVATED CHARCOAL. |
| CA1301754C (en) * | 1986-05-30 | 1992-05-26 | Louris Kaper | Process for recovering caffeine absorbed in activated carbon, and a process for decaffeinating coffee |
| CA1318811C (en) * | 1986-05-30 | 1993-06-08 | Louris Kaper | Process for decaffeinating green coffee |
| NL8602012A (en) * | 1986-08-06 | 1988-03-01 | Douwe Egberts Tabaksfab | PROCESS FOR EXTRACTING CAFFEINE ADSORBED TO ACTIVE CARBON. |
| ATE180784T1 (en) * | 1992-08-18 | 1999-06-15 | Kraft Jacobs Suchard Ag | METHOD FOR RECOVERING CAFFEIN FROM ACTIVATED CHARCOAL |
| DE69322761T2 (en) * | 1993-02-24 | 1999-05-20 | Sara Lee/De N.V., Utrecht | Recovery of activated carbon loaded with caffeine using organic solvents |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD78586A (en) * | ||||
| US4298736A (en) * | 1980-06-16 | 1981-11-03 | General Foods Corporation | Carbon-caffeine separation |
-
1982
- 1982-05-24 ES ES512478A patent/ES512478A0/en active Granted
- 1982-09-28 EP EP82305113A patent/EP0076620B2/en not_active Expired - Lifetime
- 1982-09-28 AT AT82305113T patent/ATE15043T1/en not_active IP Right Cessation
- 1982-09-28 DE DE8282305113T patent/DE3265628D1/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| EP0076620A3 (en) | 1983-07-27 |
| EP0076620A2 (en) | 1983-04-13 |
| ES512478A0 (en) | 1983-03-01 |
| ATE15043T1 (en) | 1985-09-15 |
| EP0076620B1 (en) | 1985-08-21 |
| DE3265628D1 (en) | 1985-09-26 |
| EP0076620B2 (en) | 1990-10-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD2A | Announcement of lapse in spain |
Effective date: 20170710 |