ES8104137A1 - Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado - Google Patents
Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificadoInfo
- Publication number
- ES8104137A1 ES8104137A1 ES492362A ES492362A ES8104137A1 ES 8104137 A1 ES8104137 A1 ES 8104137A1 ES 492362 A ES492362 A ES 492362A ES 492362 A ES492362 A ES 492362A ES 8104137 A1 ES8104137 A1 ES 8104137A1
- Authority
- ES
- Spain
- Prior art keywords
- sulphuric acid
- regenerating
- oxidising agent
- regenerating sulphuric
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 230000001172 regenerating effect Effects 0.000 title abstract 2
- 235000011149 sulphuric acid Nutrition 0.000 title abstract 2
- 239000001117 sulphuric acid Substances 0.000 title abstract 2
- 239000007800 oxidant agent Substances 0.000 abstract 2
- 229910003556 H2 SO4 Inorganic materials 0.000 abstract 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- VQTGUFBGYOIUFS-UHFFFAOYSA-N nitrosylsulfuric acid Chemical compound OS(=O)(=O)ON=O VQTGUFBGYOIUFS-UHFFFAOYSA-N 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/0094—Evaporating with forced circulation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/02—Evaporators with heating coils
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/06—Evaporators with vertical tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/88—Concentration of sulfuric acid
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B17/00—Sulfur; Compounds thereof
- C01B17/69—Sulfur trioxide; Sulfuric acid
- C01B17/90—Separation; Purification
- C01B17/905—Removal of organic impurities
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
PROCEDIMIENTO Y DISPOSITIVO PARA LA REGENERACION DE ACIDO SULFURICO IMPURIFICADO MEDIANTE CALENTAMIENTO INDIRECTO. CONSISTE EN INTRODUCIR EN UNA UNIDAD DE PURIFICACION EL ACIDO SULFURICO IMPURIFICADO CON UNA CONCENTRACION DEL 90 AL 98,3 POR 100 EN PESO DE H2SO4 Y SOMETERLO EN LA ZONA DE CALENTAMIENTO (A) A UNA TEMPERATURA COMPRENDIDA ENTRE 140 Y 330 GRADOS, DESPUES SE LE PASA A LA ZONA DE REACCION (C), DONDE SE LE SOMETE A UNA PRESION COMPRENDIDA ENTRE 100 TORR Y LA ATMOSFERA, Y, POR ULTIMO, SE LE PASA A LA ZONA DE REACCION ULTERIOR, DONDE SE LA MANTIENE A UNA TEMPERATURA DE 330 GRADOS Y A UNA PRESION NORMAL O INFERIOR, CONSIGUIENDOSE LA PURIFICACION DEL ACIDO, CUYA CONCENTRACION EN LA ZONA DE SALIDA DEL REFRIGERADOR MEZCLADO (D) ES, COMO MINIMO, DEL 96 POR 100 EN PESO DE H2SO4. EL DISPOSITIVO CONSTA EN ESENCIA DE UNA UNIDAD DE PURIFICACION FORMADA POR UN TUBO DE CRISTAL DE CUARZO CALENTADO POR RADIACION, ESTANDO DICHO TUBO RODEADO POR UNA ENVOLTURA CONCENTRICA Y ESTA A SU VEZ POR UNA RESISTENCIA DE CALEFACCION ELECTRICA. EL SISTEMA OFRECE VARIANTES. A
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH551379A CH641126A5 (en) | 1979-06-13 | 1979-06-13 | Process and system for regenerating sulphuric acid |
| DE19803018664 DE3018664A1 (de) | 1979-06-13 | 1980-05-16 | Verfahren und vorrichtung zum regenerieren von schwefelsaeure |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES8104137A1 true ES8104137A1 (es) | 1981-04-16 |
| ES492362A0 ES492362A0 (es) | 1981-04-16 |
Family
ID=25697890
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES492362A Granted ES492362A0 (es) | 1979-06-13 | 1980-06-12 | Procedimiento y dispositivo para la regeneracion de acido sulfurico impurificado |
Country Status (4)
| Country | Link |
|---|---|
| EP (1) | EP0022473B1 (es) |
| CA (1) | CA1158836A (es) |
| ES (1) | ES492362A0 (es) |
| FI (1) | FI67354C (es) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH654282A5 (de) * | 1983-02-09 | 1986-02-14 | Bertrams Ag | Verfahren und einrichtung zum konzentrieren und reinigen von organische verunreinigungen enthaltender schwefelsaeure. |
| DE4230099C2 (de) * | 1992-09-09 | 1998-09-24 | Bayer Ag | Verfahren zum Regenerieren gebrauchter Schwefelsäure |
| DE19807632A1 (de) * | 1998-02-23 | 1999-09-02 | Bayer Ag | Vorrichtung zum Konzentrieren und Reinigen von Schwefelsäure |
| US12297106B2 (en) | 2023-06-12 | 2025-05-13 | Applied Technology Limited Partnership | Methods and systems for producing sulfur-containing products |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE688010C (es) * | 1936-10-18 | 1940-10-24 | E H Harry Pauling Dipl Ing Dr | |
| GB1280624A (en) * | 1970-02-16 | 1972-07-05 | Imp Smelting Corp Ltd | Improvements in or relating to the purification of sulphuric acid |
| DE2242055C3 (de) * | 1972-08-26 | 1979-05-31 | Industrie Chemie Thoma Gmbh, 6000 Frankfurt | Verfahren zur Konzentration und Reinigung von durch organische Substanzen verunreinigter Schwefelsäure |
| DE2360706C3 (de) * | 1973-12-06 | 1980-10-16 | Hoechst Ag, 6000 Frankfurt | Verfahren zur Regeneration von Schwefelsäure |
-
1980
- 1980-06-09 EP EP80103185A patent/EP0022473B1/de not_active Expired
- 1980-06-11 FI FI801879A patent/FI67354C/fi not_active IP Right Cessation
- 1980-06-11 CA CA000353804A patent/CA1158836A/en not_active Expired
- 1980-06-12 ES ES492362A patent/ES492362A0/es active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| ES492362A0 (es) | 1981-04-16 |
| CA1158836A (en) | 1983-12-20 |
| EP0022473A1 (de) | 1981-01-21 |
| FI801879A7 (fi) | 1980-12-14 |
| FI67354B (fi) | 1984-11-30 |
| EP0022473B1 (de) | 1983-10-19 |
| FI67354C (fi) | 1985-03-11 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 19970519 |