ES2607477T3 - Determinación de la corrosividad de azufre en aceites aislantes con una banda de cobre con calentamiento y agitación - Google Patents
Determinación de la corrosividad de azufre en aceites aislantes con una banda de cobre con calentamiento y agitación Download PDFInfo
- Publication number
- ES2607477T3 ES2607477T3 ES09805861.3T ES09805861T ES2607477T3 ES 2607477 T3 ES2607477 T3 ES 2607477T3 ES 09805861 T ES09805861 T ES 09805861T ES 2607477 T3 ES2607477 T3 ES 2607477T3
- Authority
- ES
- Spain
- Prior art keywords
- vials
- corrosivity
- oil
- determination
- methods
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
- G01N33/2835—Specific substances contained in the oils or fuels
- G01N33/287—Sulfur content
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
- G01N33/2835—Specific substances contained in the oils or fuels
- G01N33/2876—Total acid number
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/18—Sulfur containing
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Sampling And Sample Adjustment (AREA)
- Detergent Compositions (AREA)
- Organic Insulating Materials (AREA)
Abstract
Métodos integrados para la determinación del envejecimiento, corrosividad, huella y/o contaminantes así como el diagnóstico funcional, la descontaminación, la despolarización y la detoxificación de aceites y fluidos técnicos como aceites minerales aislantes, ésteres naturales y/o sintéticos, lubricantes, fluidos hidráulicos, diatérmicos y técnicos en general, utilizados en transformadores eléctricos, reactores, aisladores, interruptores y turbinas, para la generación, transmisión, distribución y uso de electricidad, dichos métodos se basan en una o más de las siguientes opciones: I - prueba de corrosividad acelerada para el aceite, preferiblemente a 150°C por 12 horas, en la presencia de cobre con calor específico y aparato de agitación, y II - envejecimiento acelerado del aceite, preferiblemente a 120°C por 24 horas, en la presencia de cobre con calor específico y aparato de agitación, dichos métodos se caracterizan por componerse de los pasos para preparar viales con volumen desde 10 hasta 100ml en una mesa giratoria especializada que tiene espacio para 1 a 100 viales. Se purgan gases en sobrepresión con respecto al ambiente para la saturación de los viales, donde estos gases son argón y nitrógeno, se introduce el aceite en los viales y se sellan los viales con tapas para mantener una atmósfera controlada.
Description
Claims (1)
-
imagen1 imagen2
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ITTO2008A000936A IT1394617B1 (it) | 2008-12-16 | 2008-12-16 | Metodi integrati per la determinazione della corrosivita', dell'invecchiamento, del fingerprint, nonchè la diagnosi, la decontaminazione, la depolarizzazione e la detossificazione di oli |
| ITTO20080936 | 2008-12-16 | ||
| PCT/IB2009/055778 WO2010070590A1 (en) | 2008-12-16 | 2009-12-16 | The corrosity of sulfur in insulating oils is determined with a copper strip under heated and stirred conditions |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2607477T3 true ES2607477T3 (es) | 2017-03-31 |
Family
ID=41172350
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES09805861.3T Active ES2607477T3 (es) | 2008-12-16 | 2009-12-16 | Determinación de la corrosividad de azufre en aceites aislantes con una banda de cobre con calentamiento y agitación |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US9075038B2 (es) |
| EP (1) | EP2373994B1 (es) |
| ES (1) | ES2607477T3 (es) |
| IT (1) | IT1394617B1 (es) |
| WO (1) | WO2010070590A1 (es) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP5718822B2 (ja) * | 2009-11-25 | 2015-05-13 | 出光興産株式会社 | 潤滑油の劣化状態判断方法及びその判断装置、並びに機械・装置における潤滑油監視システム |
| CN102062734B (zh) * | 2010-12-13 | 2012-04-11 | 西南铝业(集团)有限责任公司 | 一种覆盖剂中钠含量和钾含量的分析检测方法 |
| US9140679B2 (en) * | 2010-12-28 | 2015-09-22 | Chevron U.S.A. Inc. | Process for characterizing corrosivity of refinery feedstocks |
| CA2818679A1 (en) * | 2010-12-28 | 2012-07-05 | Chevron U.S.A. Inc. | Processes and systems for characterizing and blending refinery feedstocks |
| US9103813B2 (en) * | 2010-12-28 | 2015-08-11 | Chevron U.S.A. Inc. | Processes and systems for characterizing and blending refinery feedstocks |
| US8474324B2 (en) * | 2011-11-30 | 2013-07-02 | King Fahd University Of Petroleum And Minerals | Stress corrosion cracking testing device |
| US8932863B2 (en) | 2011-12-15 | 2015-01-13 | Uop Llc | Methods for evaluating fuel compositions |
| US20150192559A1 (en) * | 2012-11-20 | 2015-07-09 | Mitsubishi Electric Corporation | Diagnosis method and maintenance method for oil-filled electrical equipment |
| US9310288B2 (en) * | 2013-01-28 | 2016-04-12 | Fisher-Rosemount Systems, Inc. | Systems and methods to monitor operating processes |
| CN103604877B (zh) * | 2013-10-29 | 2015-09-30 | 安徽农业大学 | 一种石斛生物碱类成分的高效液相色谱指纹图谱构建方法及应用 |
| CN103681239B (zh) * | 2013-10-29 | 2016-09-28 | 宁夏银星能源股份有限公司 | 一种清洗单晶硅片表面的方法 |
| CN103868784B (zh) * | 2014-03-03 | 2016-05-04 | 北京航空航天大学 | 一种基于接触应力的橡胶密封件性能退化监测方法 |
| CN103969246A (zh) * | 2014-05-21 | 2014-08-06 | 国家电网公司 | 一种定量检测矿物绝缘油中腐蚀性硫含量的方法 |
| CN104807902B (zh) * | 2015-04-27 | 2016-06-08 | 广东电网有限责任公司电力科学研究院 | 绝缘油中二苄基二硫醚和抗氧化剂的检测方法 |
| KR20160143140A (ko) * | 2015-06-04 | 2016-12-14 | 엘에스산전 주식회사 | 전력설비 건전성 평가시스템 |
| CN106483237B (zh) * | 2015-08-26 | 2017-10-13 | 菏泽天鸿果蔬有限公司 | 一种污水中多氯联苯含量的检测方法 |
| CN105388227A (zh) * | 2015-10-29 | 2016-03-09 | 山东中实易通集团有限公司 | 充油电气设备油中二苄基二硫的定量检测方法 |
| CN105645704A (zh) * | 2015-12-29 | 2016-06-08 | 安徽理工大学 | 一种采煤塌陷区底泥中有机氯农药的处理、提取与净化方法 |
| CN106291172B (zh) * | 2016-07-28 | 2019-04-30 | 国网河北省电力公司电力科学研究院 | 一种复合绝缘子老化状态评估方法 |
| CN108535104A (zh) * | 2018-03-20 | 2018-09-14 | 苏州市信测标准技术服务有限公司 | 一种橡胶综合老化试验方法 |
| CN108519546A (zh) * | 2018-06-27 | 2018-09-11 | 广东电网有限责任公司 | 一种检测高压设备局部放电的方法和系统 |
| CN110174364B (zh) * | 2019-05-20 | 2021-08-20 | 国网陕西省电力公司电力科学研究院 | 一种基于朗伯比尔定律的复合绝缘子无损检测装置及方法 |
| US11118427B2 (en) | 2019-09-30 | 2021-09-14 | Saudi Arabian Oil Company | Managing corrosion and scale buildup in a wellbore |
| CN110646422B (zh) * | 2019-11-14 | 2022-03-08 | 徐州飞梦电子科技有限公司 | 一种空气中硫含量检测采样的无人机设备及其使用方法 |
| CN112924651B (zh) * | 2020-12-30 | 2022-07-29 | 广东电网有限责任公司电力科学研究院 | 一种变压器油老化程度检测方法、装置及设备 |
| EP4591045A1 (en) * | 2022-09-22 | 2025-07-30 | Shell Internationale Research Maatschappij B.V. | Copper corrosion test method |
| RS20230532A1 (sr) * | 2023-07-12 | 2025-01-31 | Elektrotehnicki Inst Nikola Tesla Akcionarsko Drustvo Beograd | Postupak za desulfurizaciju |
Family Cites Families (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1769463A (en) * | 1928-07-23 | 1930-07-01 | Rice Cyrus William | Detector |
| US2679752A (en) * | 1949-11-25 | 1954-06-01 | Socony Vacuum Oil Co Inc | Method for measuring corrosivity of fluids |
| GB1358291A (en) * | 1971-01-18 | 1974-07-03 | British Petroleum Co | Antioxidant composition |
| US3791803A (en) * | 1971-07-15 | 1974-02-12 | Mobil Oil Corp | Organic compositions containing n-acyl benzotriazoles |
| US3788993A (en) * | 1972-04-24 | 1974-01-29 | Mobil Oil Corp | Lubricating compositions |
| US3969237A (en) * | 1973-03-22 | 1976-07-13 | Mobil Oil Corporation | Lubricant compositions containing benzotriazole derivatives as copper passivators |
| DE2818251C2 (de) * | 1978-04-26 | 1981-10-08 | Bodenseewerk Perkin-Elmer & Co GmbH, 7770 Überlingen | Probengeber für Gaschromatographen |
| DE3130245A1 (de) * | 1981-07-31 | 1983-02-17 | Bodenseewerk Perkin-Elmer & Co GmbH, 7770 Überlingen | Probengeber zum aufgeben von proben bei der gaschromatographie |
| US4450424A (en) * | 1982-05-10 | 1984-05-22 | Mcgraw-Edison Company | Electrical insulating system |
| JPS5995463A (ja) | 1982-11-25 | 1984-06-01 | Seiko Instr & Electronics Ltd | ケミカルマニピユレ−タ |
| SE8401581L (sv) * | 1984-03-21 | 1985-09-22 | Foersvarets Forskningsanstalt | Metod och anordning for metning av vetskors korrosivitet eller reaktivitet mot fremst metaller |
| JPS63180832A (ja) * | 1987-01-22 | 1988-07-25 | Power Reactor & Nuclear Fuel Dev Corp | 自動重量サンプリング装置 |
| US5012845A (en) * | 1988-08-18 | 1991-05-07 | Dynatech Precision Sampling Corporation | Fluid injector |
| CA2076370A1 (en) * | 1990-03-02 | 1991-09-03 | Thomas B. Green | Analyzer transport device |
| US5157963A (en) * | 1990-05-22 | 1992-10-27 | Eaton Corporation | Procedure for qualifying synthetic base gear lubricant |
| ITMI922961A1 (it) | 1992-12-24 | 1994-06-24 | Sea Marconi Technologies Sas | Procedimento per la dealogenazione chimica di composti organici alogenati. |
| US5332900A (en) * | 1993-02-16 | 1994-07-26 | Exxon Research & Engineering Co. | On-line corrosivity monitor for petroleum products |
| US5516969A (en) * | 1995-01-23 | 1996-05-14 | Ontario Hydro | Waste oil decontamination process |
| US6096695A (en) * | 1996-06-03 | 2000-08-01 | Ethyl Corporation | Sulfurized phenolic antioxidant composition, method of preparing same, and petroleum products containing same |
| US5874309A (en) * | 1996-10-16 | 1999-02-23 | Taiwan Semiconductor Manufacturing Company, Ltd. | Method for monitoring metal corrosion on integrated circuit wafers |
| US6074610A (en) * | 1997-05-22 | 2000-06-13 | Exxonmobil Upstream Research Company | Multi-sample reactor |
| US6436713B1 (en) * | 1997-07-28 | 2002-08-20 | 3M Innovative Properties Company | Methods and devices for measuring total polar compounds in degrading oils |
| US6365413B1 (en) * | 1998-02-27 | 2002-04-02 | Savant, Inc. | Thin film thermal oxidative oil deposit testing device and method |
| US6759014B2 (en) * | 2001-01-26 | 2004-07-06 | Symyx Technologies, Inc. | Apparatus and methods for parallel processing of multiple reaction mixtures |
| CA2340737C (en) * | 1998-08-20 | 2009-04-07 | Shell Internationale Research Maatschappij B.V. | Lubricating oil composition useful in hydraulic fluids |
| US6294387B1 (en) * | 1999-03-24 | 2001-09-25 | Intevep, S.A. | Method of determining the corrosiveness of naphthenic acid in crude oil refinery streams |
| US6132686A (en) * | 1999-05-28 | 2000-10-17 | Mettler-Toledo Bohdan, Inc. | Pressurized reaction block |
| US7025138B2 (en) * | 2000-12-08 | 2006-04-11 | Schlumberger Technology Corporation | Method and apparatus for hydrogen sulfide monitoring |
| JP2004217797A (ja) * | 2003-01-15 | 2004-08-05 | Ethyl Japan Kk | 長寿命で熱安定性に優れたギア油組成物 |
| US20050095717A1 (en) * | 2003-10-31 | 2005-05-05 | Wollenberg Robert H. | High throughput screening methods for lubricating oil compositions |
| US7306948B2 (en) * | 2004-02-13 | 2007-12-11 | Chevron Oronite Company Llc | High throughput screening methods for lubricating oil compositions |
| US7553449B2 (en) * | 2004-09-21 | 2009-06-30 | Exxonmobil Research & Engineering Company | Method of determination of corrosion rate |
| EP2214184A4 (en) * | 2007-10-26 | 2014-03-12 | Mitsubishi Electric Corp | METHOD FOR EXAMINING AN OIL-FILLED ELECTRICAL DEVICE |
-
2008
- 2008-12-16 IT ITTO2008A000936A patent/IT1394617B1/it active
-
2009
- 2009-12-16 ES ES09805861.3T patent/ES2607477T3/es active Active
- 2009-12-16 WO PCT/IB2009/055778 patent/WO2010070590A1/en not_active Ceased
- 2009-12-16 EP EP09805861.3A patent/EP2373994B1/en not_active Not-in-force
- 2009-12-16 US US13/130,156 patent/US9075038B2/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| ITTO20080936A1 (it) | 2010-06-17 |
| WO2010070590A8 (en) | 2010-10-28 |
| EP2373994B1 (en) | 2016-09-21 |
| WO2010070590A1 (en) | 2010-06-24 |
| US9075038B2 (en) | 2015-07-07 |
| US20110223672A1 (en) | 2011-09-15 |
| IT1394617B1 (it) | 2012-07-05 |
| EP2373994A1 (en) | 2011-10-12 |
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