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ES2563323T3 - Procedimiento para la preparación de un sólido cristalino a partir de derivados de ácido glicin-N,N-diacético - Google Patents

Procedimiento para la preparación de un sólido cristalino a partir de derivados de ácido glicin-N,N-diacético Download PDF

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Publication number
ES2563323T3
ES2563323T3 ES10747834.9T ES10747834T ES2563323T3 ES 2563323 T3 ES2563323 T3 ES 2563323T3 ES 10747834 T ES10747834 T ES 10747834T ES 2563323 T3 ES2563323 T3 ES 2563323T3
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Spain
Prior art keywords
formula
preparation
diacetic acid
crystalline solid
derivatives
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Active
Application number
ES10747834.9T
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English (en)
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ES2563323T5 (es
Inventor
Andreas Baranyai
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BASF SE
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BASF SE
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Application filed by BASF SE filed Critical BASF SE
Publication of ES2563323T3 publication Critical patent/ES2563323T3/es
Application granted granted Critical
Publication of ES2563323T5 publication Critical patent/ES2563323T5/es
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C07C229/16—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings to carbon atoms of hydrocarbon radicals substituted by amino or carboxyl groups, e.g. ethylenediamine-tetra-acetic acid, iminodiacetic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
    • C05D9/00—Other inorganic fertilisers
    • C05D9/02—Other inorganic fertilisers containing trace elements
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/33—Amino carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22—Organic compounds
    • C11D7/32—Organic compounds containing nitrogen
    • C11D7/3245—Aminoacids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2602/00—Systems containing two condensed rings
    • C07C2602/02—Systems containing two condensed rings the rings having only two atoms in common
    • C07C2602/04—One of the condensed rings being a six-membered aromatic ring
    • C07C2602/12—One of the condensed rings being a six-membered aromatic ring the other ring being at least seven-membered

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Detergent Compositions (AREA)

Abstract

Procedimiento para la preparación de un sólido cristalino que comprende, con respecto al contenido en sólido, del 70 % al 99,9 % en peso de derivados de ácido metilglicin-N,N-diacético de fórmula general I**Fórmula** en la que cada M significa independientemente entre sí hidrógeno, metal alcalino, amonio o amonio sustituido en las correspondientes cantidades estequiométricas, conservando el sólido durante el almacenamiento abierto a 25 ºC y una humedad del aire relativa del 76 % durante un período de tiempo de al menos un día su consistencia como granulado, caracterizado porque se dispone al menos un compuesto cristalino de fórmula I y se realiza una granulación por pulverización con al menos un compuesto de fórmula I.

Description

imagen1
imagen2
imagen3

Claims (1)

  1. imagen1
ES10747834T 2009-08-26 2010-08-25 Procedimiento para la preparación de un sólido cristalino a partir de derivados de ácido glicin-N,N-diacético Active ES2563323T5 (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102009038951 2009-08-26
DE102009038951A DE102009038951A1 (de) 2009-08-26 2009-08-26 Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
PCT/EP2010/005219 WO2011023382A2 (de) 2009-08-26 2010-08-25 Verfahren zur herstellung eines kristallinen feststoffes aus glycin-n, n-diessigsäure-derivaten mit hinreichend geringer hygroskopizität

Publications (2)

Publication Number Publication Date
ES2563323T3 true ES2563323T3 (es) 2016-03-14
ES2563323T5 ES2563323T5 (es) 2024-10-16

Family

ID=43500504

Family Applications (1)

Application Number Title Priority Date Filing Date
ES10747834T Active ES2563323T5 (es) 2009-08-26 2010-08-25 Procedimiento para la preparación de un sólido cristalino a partir de derivados de ácido glicin-N,N-diacético

Country Status (17)

Country Link
US (2) US9376649B2 (es)
EP (1) EP2470496B2 (es)
JP (1) JP5756107B2 (es)
KR (1) KR101755736B1 (es)
CN (1) CN102574775B (es)
AU (1) AU2010288872A1 (es)
BR (1) BR112012004179B1 (es)
CA (1) CA2771916C (es)
DE (1) DE102009038951A1 (es)
ES (1) ES2563323T5 (es)
MX (1) MX2012002244A (es)
MY (1) MY158464A (es)
PL (1) PL2470496T5 (es)
RU (1) RU2551851C2 (es)
SG (1) SG178352A1 (es)
WO (1) WO2011023382A2 (es)
ZA (1) ZA201202132B (es)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
MX2012004170A (es) * 2009-10-12 2012-05-08 Basf Se Metodo para producir un polvo que contiene una o mas sales de agente de complejacion.
DE102009060814A1 (de) 2009-12-30 2011-07-07 inprotec AG, 79423 Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält
CA2809749A1 (en) * 2010-09-27 2012-04-05 Basf Se Process for producing granules comprising one or more complexing agent salts
US9227915B2 (en) * 2011-05-03 2016-01-05 Basf Se Process for the preparation of a crystalline L-MGDA trialkali metal salt
GB2491619B (en) 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation
WO2014090943A1 (en) 2012-12-14 2014-06-19 Akzo Nobel Chemicals International B.V. Crystalline particles of salts of glutamic acid n,n-diacetic acid
US9815773B2 (en) 2012-12-14 2017-11-14 Akzo Nobel Chemicals International B.V. Crystalline particles of glutamic acid N,N-diacetic acid
WO2015173157A2 (en) 2014-05-13 2015-11-19 Akzo Nobel Chemicals International B.V. Process to crystallize chelating agents
BR112018011578A2 (pt) * 2015-12-11 2018-11-27 Basf Se processo para fabricação de grânulos
BR112018075476B1 (pt) * 2016-06-20 2022-10-04 Basf Se Processo para produção de um pó ou grânulo, pó ou grânulo, e, uso de grânulos e de pós
CN110312785B (zh) * 2017-02-24 2021-07-20 巴斯夫欧洲公司 制造固体甲基甘氨酸二乙酸(mgda)碱金属盐的方法和固体粒子
US10836709B2 (en) 2017-07-07 2020-11-17 Nouryon Chemicals International B.V. Process to prepare a solid composition of an amino acid diacetic acid
EP3802481A1 (en) 2018-05-30 2021-04-14 Basf Se Process for making solid methylglycine diacetate (mgda) alkali metal salt, and solid particles
WO2020006109A1 (en) 2018-06-26 2020-01-02 Juul Labs, Inc. Devices and methods for cessation of nicotine addiction
CN113382980B (zh) 2018-12-21 2024-06-21 诺力昂化学品国际有限公司 甲基甘氨酸n,n-二乙酸的易碎相组合物
KR102771094B1 (ko) 2019-11-21 2025-02-24 (주)아모레퍼시픽 고함량의 락테이트 금속염 및 실리콘계 오일의 혼합물을 포함하는 w/s형 화장료 조성물
WO2021255525A1 (en) 2020-06-19 2021-12-23 Nouryon Chemicals International B.V. Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3932316A (en) 1974-11-13 1976-01-13 The Procter & Gamble Company Free flowing detergent compositions containing benzoate salts
JPH0678225B2 (ja) * 1985-11-27 1994-10-05 株式会社林原生物化学研究所 脱水医薬品とその製造方法
DE4319935A1 (de) 1993-06-16 1994-12-22 Basf Ag Verwendung von Glycin-N,N-diessigsäure-Derivaten als Komplexbildner für Erdalkali- und Schwermetallionen
JP4711471B2 (ja) 1996-07-05 2011-06-29 三菱商事フードテック株式会社 結晶マルチトール及びそれを含有する含蜜結晶の製造方法
DE19649681A1 (de) * 1996-11-29 1998-06-04 Basf Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
US7182282B2 (en) * 2001-04-13 2007-02-27 Urea Casale S.A. Fluid bed granulation apparatus
DE102004032320A1 (de) * 2004-07-02 2006-01-19 Basf Ag Mischpulver oder Mischgranulat auf Basis von MGDA
MX2009013320A (es) * 2007-07-03 2010-01-20 Basf Se Proceso para producir un solido de flujo libre y estable al almacenamiento que comprende esencialmente acido a-alanina-n, n-diacetico y/o uno o mas derivados de acido a-alanina-n, n-diacetico.
US8183410B2 (en) 2008-04-01 2012-05-22 Conopco, Inc. Preparation of free flowing granules of methylglycine diacetic acid
FR2935383B1 (fr) 2008-08-26 2010-10-01 Pancosma Sa Pour L Ind Des Pro Procede et dispositif pour la fabrication de complexes organometalliques en poudre.
JP5745507B2 (ja) * 2009-05-20 2015-07-08 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ グリシン−ｎ，ｎ−二酢酸の１種以上の誘導体および／またはグルタミン−ｎ，ｎ−二酢酸の１種以上の誘導体を含む粉末ならびにメチルグリシン−ｎ，ｎ−二酢酸三ナトリウム塩粉末の調製方法
DE102009038951A1 (de) * 2009-08-26 2011-03-03 Inprotec Ag Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität
MX2012004170A (es) * 2009-10-12 2012-05-08 Basf Se Metodo para producir un polvo que contiene una o mas sales de agente de complejacion.
GB2491619B (en) * 2011-06-09 2014-10-01 Pq Silicas Bv Builder granules and process for their preparation

Also Published As

Publication number Publication date
US20120149936A1 (en) 2012-06-14
MX2012002244A (es) 2012-03-29
KR20120089470A (ko) 2012-08-10
DE102009038951A1 (de) 2011-03-03
CN102574775A (zh) 2012-07-11
CA2771916C (en) 2017-07-25
CN102574775B (zh) 2014-09-24
KR101755736B1 (ko) 2017-07-07
ES2563323T5 (es) 2024-10-16
CA2771916A1 (en) 2011-03-03
PL2470496T3 (pl) 2016-06-30
WO2011023382A3 (de) 2011-05-12
JP5756107B2 (ja) 2015-07-29
RU2551851C2 (ru) 2015-05-27
ZA201202132B (en) 2013-05-29
BR112012004179B1 (pt) 2018-09-11
BR112012004179A2 (pt) 2016-03-29
EP2470496B2 (de) 2024-03-27
JP2013503119A (ja) 2013-01-31
AU2010288872A1 (en) 2012-03-08
PL2470496T5 (pl) 2024-07-15
MY158464A (en) 2016-10-14
WO2011023382A2 (de) 2011-03-03
US9751829B2 (en) 2017-09-05
EP2470496B1 (de) 2016-01-06
US9376649B2 (en) 2016-06-28
RU2012111127A (ru) 2013-10-10
EP2470496A2 (de) 2012-07-04
SG178352A1 (en) 2012-03-29
US20160221930A1 (en) 2016-08-04

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