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ES2255332A1 - Manufacturing method for plastic panels, involves co-extruding intermediate, external, and internal layers each containing high percentage by weight of recycled polyolefins - Google Patents

Manufacturing method for plastic panels, involves co-extruding intermediate, external, and internal layers each containing high percentage by weight of recycled polyolefins

Info

Publication number
ES2255332A1
ES2255332A1 ES200200126A ES200200126A ES2255332A1 ES 2255332 A1 ES2255332 A1 ES 2255332A1 ES 200200126 A ES200200126 A ES 200200126A ES 200200126 A ES200200126 A ES 200200126A ES 2255332 A1 ES2255332 A1 ES 2255332A1
Authority
ES
Spain
Prior art keywords
weight
panels
manufacture
coextrusion
organic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
ES200200126A
Other languages
Spanish (es)
Other versions
ES2255332B1 (en
Inventor
Juan Luis Ripolles Romeu
Pere Palau Gudiol
Miguel Sannicolas Martinez
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nature Pack S A
NATURE PACK SA
Original Assignee
Nature Pack S A
NATURE PACK SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nature Pack S A, NATURE PACK SA filed Critical Nature Pack S A
Priority to ES200200126A priority Critical patent/ES2255332B1/en
Publication of ES2255332A1 publication Critical patent/ES2255332A1/en
Application granted granted Critical
Publication of ES2255332B1 publication Critical patent/ES2255332B1/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C48/00Extrusion moulding, i.e. expressing the moulding material through a die or nozzle which imparts the desired form; Apparatus therefor
    • B29C48/16Articles comprising two or more components, e.g. co-extruded layers
    • B29C48/18Articles comprising two or more components, e.g. co-extruded layers the components being layers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29BPREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
    • B29B17/00Recovery of plastics or other constituents of waste material containing plastics
    • B29C47/06
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/62Plastics recycling; Rubber recycling

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Environmental & Geological Engineering (AREA)
  • Laminated Bodies (AREA)
  • Extrusion Moulding Of Plastics Or The Like (AREA)

Abstract

The intermediate, external, and internal layers, each containing high percentage e.g. 95 %, by weight of recycled polyolefins, are co-extruded together and applied extrusion lubricant. An independent claim is also included for a plastic panel.

Description

Procedimiento para la fabricación de paneles de materiales plásticos, estratificados, con cargas orgánicas o inorgánicas, por coextrusión y paneles fabricados mediante el mismo.Procedure for the manufacture of panels plastic materials, laminated, with organic fillers or inorganic, by coextrusion and panels manufactured by means of same.

La presente invención se refiere a un procedimiento para la fabricación de paneles realizados en materiales plásticos de tipo estratificado, con cargas orgánicas e inorgánicas, utilizando procedimientos de coextrusión y como mínimo tres estratos en cada panel.The present invention relates to a procedure for manufacturing panels made in plastic materials of stratified type, with organic loads and inorganic, using coextrusion procedures and at least Three layers in each panel.

Dichos paneles tienen diferentes aplicaciones industriales, en especial en el sector de fabricación de envases y embalajes.These panels have different applications industrial, especially in the sector of packaging manufacturing and packaging

En la actualidad son conocidos paneles realizados por coextrusión en los que dos capas exteriores están realizadas mediante poliolefinas y cargas inorgánicas y una capa intermedia queda conformada a base de poliolefinas y cargas de tipo orgánico.Nowadays panels are known made by coextrusion in which two outer layers are made using polyolefins and inorganic fillers and a layer intermediate is made up of polyolefins and type charges organic.

En la fabricación de dichos paneles y en la fabricación posterior de elementos para cajas de envase y embalaje fabricadas a partir de los mismos se producen desperdicios en importantes cantidades, que hasta el momento no se han aprovechado industrialmente y que representan un aumento de costes sensible en los paneles fabricados.In the manufacture of said panels and in the subsequent manufacture of elements for container and packaging boxes manufactured from them waste is produced in significant amounts, which so far have not been taken advantage of industrially and that represent a sensible increase in costs in the manufactured panels.

La presente invención está destinada precisamente a conseguir la posibilidad de utilización de materiales reciclados y/o recuperados sobre todo para la capa intermedia o central del panel, que es la que habitualmente tiene una proporción más elevada de masa del panel en su conjunto, permitiendo conseguir importantes ahorros en los costes de las materias primas.The present invention is intended precisely to achieve the possibility of using recycled and / or recovered materials especially for the layer intermediate or central panel, which is the one that usually has a higher proportion of mass of the panel as a whole, allowing to achieve significant savings in the costs of raw Materials.

En este sentido, se debe tener en cuenta que, en una fabricación típica de dicho tipo de paneles, el 70% de la masa de los mismos corresponde a la masa de la capa intermedia y el 30% restante se distribuye de forma habitualmente irregular, por ejemplo 20% y 10% respectivamente en una y otra de las dos capas externas que recubren la capa intermedia.In this regard, it should be borne in mind that, in a typical manufacture of such panels, 70% of the mass of these corresponds to the mass of the intermediate layer and 30% remaining is usually distributed irregularly, by example 20% and 10% respectively in both layers external covering the intermediate layer.

La realización de diferentes experimentos y pruebas por parte de los inventores ha permitido conseguir el procedimiento objeto de la presente invención, que permite utilizar materiales reciclados y/o recuperados en porcentajes que pueden llegar hasta el 95% en la capa intermedia del panel.The performance of different experiments and evidence by the inventors has allowed to get the procedure object of the present invention, which allows to use recycled and / or recovered materials in percentages that may reach up to 95% in the middle layer of the panel.

Por materiales reciclados, se comprenden tanto los paneles defectuosos por una u otra razón y que resultan rechazados durante su fabricación o al final de la misma, como asimismo los recortes de fabricación de piezas troqueladas a partir de dichos paneles cuyas piezas están destinadas a ser utilizadas posteriormente en la fabricación de envases y embalajes, entendiéndose por materiales de recuperación los existentes en el comercio procedentes del aprovechamiento de otros restos y residuos de materias primas similares.Recycled materials include both defective panels for one reason or another and that result rejected during its manufacture or at the end of it, as also the cuts of manufacture of pieces cut from of said panels whose parts are intended to be used subsequently in the manufacture of containers and packaging, understood by recovery materials those existing in the trade from the use of other remains and waste  of similar raw materials.

De acuerdo con la presente invención, se procede a la fabricación del panel por coextrusión mediante una capa intermedia que está compuesta en una proporción variable, que puede llegar al 95%, por material de poliolefinas con cargas orgánicas e inorgánicas, procedente de reciclado o recuperación tal como se ha mencionado, debidamente triturado para posibilitar su utilización en una extrusionadora, mezclando previamente al material a extrusionar una proporción comprendida entre 0,25% y 3% en peso de una materia lubrificante del tipo utilizado para la extrusión de materiales plásticos, por ejemplo, estearato de zinc, estearato cálcico u otros.In accordance with the present invention, we proceed to the manufacture of the panel by coextrusion by means of a layer intermediate that is composed in a variable proportion, which can reach 95%, by polyolefins material with organic fillers and inorganic, from recycling or recovery as it has been mentioned, properly crushed to enable its use in an extruder, previously mixing the material to extrude a proportion between 0.25% and 3% by weight of a lubricating material of the type used for extrusion of plastic materials, for example, zinc stearate, stearate Calcium or others.

Los inventores han observado que los mejores resultados se consiguen cuando se utiliza una proporción de lubrificantes similar a la que se ha indicado, es decir, comprendida aproximadamente entre 0,25% y 3% en peso para las capas externas, si bien no se pueden excluir otras proporciones en determinados casos.The inventors have observed that the best results are achieved when a proportion of lubricants similar to the one indicated, that is, between approximately 0.25% and 3% by weight for the layers external, although other proportions cannot be excluded in certain cases

Con la aplicación del presente procedimiento los paneles estratificados tienen espesores comprendidos preferentemente entre 0,5 mm y 5 mm preferentemente y las capas externas tienen una composición a base de una poliolefina y una carga inorgánica, preferentemente constituida por talco en polvo o carbonato cálcico y un lubrificante en la proporción indicada, por lo que su composición final resulta ser aproximadamente:With the application of this procedure the stratified panels have thicknesses included preferably between 0.5 mm and 5 mm preferably and the layers external have a composition based on a polyolefin and a inorganic filler, preferably consisting of talcum powder or calcium carbonate and a lubricant in the proportion indicated, by what its final composition turns out to be approximately:

poliolefinas: 25% a 75%polyolefins: 25% to 75%

cargas minerales: 25% a 75%mineral loads: 25% to 75%

lubrificante: 0,25% a 3%lubricant: 0.25% to 3%

La capa intermedia queda realizada en una importante proporción por materiales de poliolefinas y cargas orgánicas e inorgánicas de reciclado y/o recuperación, que pueden llegar hasta 95% en peso, complementados por un lubrificante comprendido entre 0,25% y 3% en peso y carga orgánica comprendida entre 4% y 60%.The intermediate layer is made in a significant proportion of polyolefin materials and fillers organic and inorganic recycling and / or recovery, which can reach up to 95% by weight, complemented by a lubricant between 0.25% and 3% by weight and organic load included between 4% and 60%.

Mediante la aplicación del presente procedimiento se consigue la reutilización de gran cantidad de productos reciclados de la misma fabricación de los paneles utilizados como materia prima y asimismo se posibilita la utilización de materiales de desecho de la fabricación de los paneles troquelados para obtener las piezas de envases y embalajes, lo cual representa una importante reducción del coste de las materias primas. Dadas las características del procedimiento objeto de la presente invención, éste permite no solamente utilizar productos reciclados procedentes de la misma fabricación de los paneles o del troquelado de los mismos, sino también poliolefinas de recuperación comerciales, es decir, poliolefinas recicladas procedentes de otras aplicaciones.By applying this procedure you get the reuse of lots of recycled products of the same panel manufacturing used as raw material and also the use of waste materials in the manufacture of stamped panels to obtain the pieces of containers and packagings, which represents a significant reduction in the cost of raw Materials. Given the characteristics of the object procedure of the present invention, this allows not only to use recycled products from the same manufacturing of or die cut panels thereof, but also polyolefins of commercial recovery, that is, recycled polyolefins from other applications.

Los paneles obtenidos mediante la presente invención se caracterizan por su baja densidad real e inapreciable absorción de agua, con excelentes características mecánicas, tal como es de ver en la tabla adjunta que corresponde a las características de paneles realizados, a título de ejemplo, de acuerdo con la presente invención con una tolerancia de espesores de láminas de \pm 0,5 mm.The panels obtained herein invention are characterized by their low real and invaluable density water absorption, with excellent mechanical characteristics, such as you can see in the attached table that corresponds to the characteristics of panels made, by way of example, of according to the present invention with a thickness tolerance of sheets of ± 0.5 mm.

En la tabla adjunta se muestran los resultados de diferentes características mecánicas para cinco ejemplos de paneles realizados de acuerdo con la invención, con espesores respectivos de: 0,85, 1, 1,6, 2 y 3 mm.The attached table shows the results. of different mechanical characteristics for five examples of panels made in accordance with the invention, with thicknesses respective of: 0.85, 1, 1.6, 2 and 3 mm.

       \vskip1.000000\baselineskip\ vskip1.000000 \ baselineskip
    

Resultados de pruebas realizadas con paneles según la invenciónResults of tests performed with panels according to invention

Espesor de láminasThickness of sheets CaracterísticaCharacteristic NormaRule Dirección deDirection from ValorValue (mm)( mm ) probetatest tube 0,850.85 Temperatura deTemperature from No detectadoDo not detected 1one flexión bajo cargalow flex load No detectadoDo not detected 1,61.6 (Para una extensión(For one extension UNE EN ISO 75(1-2)UNE IN ISO 75 (1-2) LONGITUDINALLONGITUDINAL 33,25ºC; Ext: 0,36 mm33.25 ° C; Ext: 0.36 mm 22 de 0.36 mm)from 0.36 mm) 36,02ºC; Ext: 0,36 mm36.02 ° C; Ext: 0.36 mm 33 46,65ºC; Est: 0,36 mm46.65 ° C; Est: 0.36 mm 0,850.85 89,23N; Ext: 2,43 mm89.23N; Ext: 2.43 mm 1one Resistencia a laResistance to UNE EN ISO 527-2UNE EN ISO 527-2 106,11N; Est: 2,83 mm106.11N; Est: 2.83 mm 1,61.6 traccióntraction Probetas Tipo AType Probes TO LONGITUDINALLONGITUDINAL 193,20N; Ext: 2,42 mm193.20N; Ext: 2.42 mm 22 2 mm/seg2 mm / sec 233,96N; Ext: 2,86 mm233.96N; Ext: 2.86 mm 33 329,39N; Ext: 3,07 mm329.39N; Ext: 3.07 mm 0,850.85 5,68%5.68% 1one Alargamiento aElongation to UNE EN ISO 527-2UNE IN ISO 527-2 6,43%6.43% 1,61.6 la roturathe break probetas Tipo AType test tubes TO LONGITUDINALLONGITUDINAL 4,57%4.57% 22 2 mm/seg2 mm / sec 5,18%5.18% 33 4,20%4.20% 0,850.85 2,98N; Ext: 4,66 mm2.98N; Ext: 4.66 mm 1one UNE ENUNE IN 4,85N; Ext: 4,70 mm4.85N; Ext: 4.70 mm l,6l, 6 Resistencia a laResistance to ISO 178ISO 178 LONGITUDINALLONGITUDINAL 14,7N; Ext: 4,11 mm14.7N; Ext: 4.11 mm 22 flexiónflexion 21,82N; Ext: 4,01 mm21.82N; Ext: 4.01 mm 33 47,60N; Ext: 3,08 mm47.60N; Ext: 3.08 mm 0,850.85 10,23 Kj/m^{2}10.23 Kj / m2 1one Resistencia alResistance to the 10,46 Kj/m^{2}10.46 Kj / m2 1,61.6 choque CharpyCharpy shock UNE EN ISO 179JOIN IN ISO 179 LONGITUDINALLONGITUDINAL 14,10 Kj/m^{2}14.10 Kj / m2 22 16,05 Kj/m^{2}16.05 Kj / m2 33 >16,43 Kj/m^{2}> 16.43 Kj / m2 0,850.85 1one 1,61.6 Densidad realDensity real 1,25 gr/cm^{3}1.25 gr / cm3 22 33 0,850.85 1one Absorción deAbsorption from 0,09%0.09% 1,61.6 aguaWater 22 33

Tal como es de ver, los resultados conseguidos muestran excelentes características mecánicas con una reducida densidad real y casi inapreciable absorción de agua, es decir, paneles con excelentes características y cuya fabricación presenta sensibles ventajas económicas.As you can see, the results achieved show excellent mechanical characteristics with a reduced real density and almost negligible water absorption, that is, panels with excellent characteristics and whose manufacturing presents Sensitive economic advantages.

Todo cuanto no afecte, altere, cambie o modifique la esencia del procedimiento descrito, será variable a los efectos de la presente invención.Everything that does not affect, alter, change or modify the essence of the procedure described, it will be variable to The effects of the present invention.

Claims (6)

1. Procedimiento para la fabricación de paneles de materiales plásticos, estratificados, con cargas orgánicas o inorgánicas, por coextrusión, del tipo que comprende, como mínimo, una capa intermedia y sendas capas de recubrimiento externas aplicadas por coextrusión sobre cada una de las caras de la capa intermedia, realizando la coextrusión de la capa intermedia y las capas externas mediante máquinas de extrusión separadas, caracterizado porque la composición de la capa intermedia que se coextrusiona con las capas exteriores, comprende un porcentaje variable, que llega hasta 95% en peso, de poliolefinas recicladas, y/o de recuperación, con inclusión de un lubrificante de extrusión tanto para la extrusión de las capas externas como de la capa intermedia.1. Procedure for the manufacture of panels of plastic materials, laminated, with organic or inorganic fillers, by coextrusion, of the type comprising, at least, an intermediate layer and two external coating layers applied by coextrusion on each of the faces of the intermediate layer, by coextrusion of the intermediate layer and the external layers by means of separate extrusion machines, characterized in that the composition of the intermediate layer that coextrudes with the outer layers, comprises a variable percentage, which reaches up to 95% by weight, of recycled polyolefins, and / or recovery, including an extrusion lubricant for both extrusion of the outer layers and the intermediate layer. 2. Procedimiento para la fabricación de paneles de materiales plásticos, estratificados, con cargas orgánicas o inorgánicas, por coextrusión, según la reivindicación 1, caracterizado porque el lubrificante queda incluido en una proporción de 0,25 a 3% en peso.2. Process for the manufacture of panels of plastic materials, laminated, with organic or inorganic fillers, by coextrusion, according to claim 1, characterized in that the lubricant is included in a proportion of 0.25 to 3% by weight. 3. Procedimiento para la fabricación de paneles de materiales plásticos, estratificados, con cargas orgánicas o inorgánicas, por coextrusión, según la reivindicación 1, caracterizado porque las poliolefinas de reciclado proceden de los mismos paneles desechados y recortes de troquelado para la fabricación de piezas.3. Process for the manufacture of panels of plastic materials, stratified, with organic or inorganic fillers, by coextrusion, according to claim 1, characterized in that the recycled polyolefins come from the same discarded panels and die cuttings for the manufacture of parts. 4. Procedimiento para la fabricación de paneles de materiales plásticos, estratificados, con cargas orgánicas o inorgánicas, por coextrusión, según la reivindicación 1, caracterizado porque las poliolefinas de reciclado son poliolefinas recicladas procedentes de la fabricación de plásticos en general.4. Process for the manufacture of panels of plastic materials, stratified, with organic or inorganic fillers, by coextrusion, according to claim 1, characterized in that the recycle polyolefins are recycled polyolefins from the manufacture of plastics in general. 5. Procedimiento para la fabricación de paneles de materiales plásticos, estratificados, con cargas orgánicas o inorgánicas, por coextrusión, según la reivindicación 1, caracterizado porque la composición de las capas externas comprende poliolefinas de 25% a 75% en peso; cargas inorgánicas de 25% a 75% en peso y lubrificante de 0,25% a 3% en peso.5. Process for the manufacture of panels of plastic materials, laminated, with organic or inorganic fillers, by coextrusion, according to claim 1, characterized in that the composition of the outer layers comprises polyolefins of 25% to 75% by weight; inorganic fillers of 25% to 75% by weight and lubricant from 0.25% to 3% by weight. 6. Procedimiento para la fabricación de paneles de materiales plásticos, estratificados, con cargas orgánicas o inorgánicas, por coextrusión, según la reivindicación 1, caracterizado porque la capa intermedia está compuesta por materiales de poliolefinas reciclados y/o recuperados hasta 95% en peso; lubrificante de 0,25% a 3% en peso y carga orgánica de 4% a 60% en peso.6. Process for the manufacture of panels of plastic materials, stratified, with organic or inorganic fillers, by coextrusion, according to claim 1, characterized in that the intermediate layer is composed of recycled and / or recovered polyolefin materials up to 95% by weight; lubricant from 0.25% to 3% by weight and organic load from 4% to 60% by weight.
ES200200126A 2002-01-22 2002-01-22 PROCEDURE FOR THE MANUFACTURE OF PANELS OF PLASTIC, STRATIFIED MATERIALS, WITH ORGANIC OR INORGANIC LOADS, BY COEXTRUSION AND PANELS MANUFACTURED THROUGH THE SAME. Expired - Fee Related ES2255332B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
ES200200126A ES2255332B1 (en) 2002-01-22 2002-01-22 PROCEDURE FOR THE MANUFACTURE OF PANELS OF PLASTIC, STRATIFIED MATERIALS, WITH ORGANIC OR INORGANIC LOADS, BY COEXTRUSION AND PANELS MANUFACTURED THROUGH THE SAME.

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
ES200200126A ES2255332B1 (en) 2002-01-22 2002-01-22 PROCEDURE FOR THE MANUFACTURE OF PANELS OF PLASTIC, STRATIFIED MATERIALS, WITH ORGANIC OR INORGANIC LOADS, BY COEXTRUSION AND PANELS MANUFACTURED THROUGH THE SAME.

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ES2255332A1 true ES2255332A1 (en) 2006-06-16
ES2255332B1 ES2255332B1 (en) 2007-05-01

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ES200200126A Expired - Fee Related ES2255332B1 (en) 2002-01-22 2002-01-22 PROCEDURE FOR THE MANUFACTURE OF PANELS OF PLASTIC, STRATIFIED MATERIALS, WITH ORGANIC OR INORGANIC LOADS, BY COEXTRUSION AND PANELS MANUFACTURED THROUGH THE SAME.

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4402889A (en) * 1982-02-04 1983-09-06 Composite Container Corporation Making sheet with moisture barrier properties coextruded from scrap materials
US4647509A (en) * 1985-10-07 1987-03-03 The Dow Chemical Company Thermoformable multilayer barrier structures
US4877682A (en) * 1986-03-24 1989-10-31 Amoco Corporation Laminates containing coextruded scrap
US5928798A (en) * 1994-04-28 1999-07-27 Cryovac, Inc. Multi-layer polyolefin film containing recycle polymer from cross-linked films

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4402889A (en) * 1982-02-04 1983-09-06 Composite Container Corporation Making sheet with moisture barrier properties coextruded from scrap materials
US4647509A (en) * 1985-10-07 1987-03-03 The Dow Chemical Company Thermoformable multilayer barrier structures
US4877682A (en) * 1986-03-24 1989-10-31 Amoco Corporation Laminates containing coextruded scrap
US5928798A (en) * 1994-04-28 1999-07-27 Cryovac, Inc. Multi-layer polyolefin film containing recycle polymer from cross-linked films

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