ES2138351T3 - Procedimiento de purificacion de alcohol polivinilico. - Google Patents
Procedimiento de purificacion de alcohol polivinilico.Info
- Publication number
- ES2138351T3 ES2138351T3 ES96919873T ES96919873T ES2138351T3 ES 2138351 T3 ES2138351 T3 ES 2138351T3 ES 96919873 T ES96919873 T ES 96919873T ES 96919873 T ES96919873 T ES 96919873T ES 2138351 T3 ES2138351 T3 ES 2138351T3
- Authority
- ES
- Spain
- Prior art keywords
- pct
- content
- poly
- vinyl alcohol
- date nov
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/001—Removal of residual monomers by physical means
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B63/00—Purification; Separation; Stabilisation; Use of additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F116/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical
- C08F116/02—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical by an alcohol radical
- C08F116/04—Acyclic compounds
- C08F116/06—Polyvinyl alcohol ; Vinyl alcohol
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/008—Treatment of solid polymer wetted by water or organic solvents, e.g. coagulum, filter cakes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
LA PRESENTE INVENCION SE REFIERE A UN PROCEDIMIENTO DE PURIFICACION DE ALCOHOL POLIVINILICO. ESTE CONSISTE EN SOMETER UN ALCOHOL POLIVINILICO A UN TRATAMIENTO TERMICO BAJO AGITACION Y BAJO UNA ATMOSFERA NO SATURADA DE AGUA QUE PRESENTA UN PORCENTAJE EN MASA DE VAPOR DE AGUA COMPRENDIDO ENTRE EL 20 % Y EL 100 %. EL PROCEDIMIENTO SEGUN LA INVENCION PUEDE COMPRENDER ADEMAS UNA ETAPA DE SECADO ADICIONAL. LA PRESENTE INVENCION SE REFIERE TAMBIEN A UN ALCOHOL POLIVINILICO QUE PRESENTA UN CONTENIDO DE ALCOHOL, Y MAS EN PARTICULAR DE METANOL, INFERIOR AL 1 %, UN CONTENIDO DE ESTER, Y MAS EN PARTICULAR DE ACETATO DE METILO, INFERIOR AL 1 %, EN FORMA DE ESCAMAS DE ALGUNOS MILIMETROS O DE UN POLVO CUYA GRANULOMETRIA MEDIA ES VENTAJOSAMENTE SUPERIOR A 600 MI}M.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR9505893A FR2733756B1 (fr) | 1995-05-05 | 1995-05-05 | Procede de purification d'alcool polyvinylique |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES2138351T3 true ES2138351T3 (es) | 2000-01-01 |
Family
ID=9479111
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES96919873T Expired - Lifetime ES2138351T3 (es) | 1995-05-05 | 1996-05-06 | Procedimiento de purificacion de alcohol polivinilico. |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US6080814A (es) |
| EP (1) | EP0823917B1 (es) |
| JP (1) | JP3177914B2 (es) |
| KR (1) | KR100296785B1 (es) |
| CN (1) | CN1074424C (es) |
| AT (1) | ATE183755T1 (es) |
| AU (1) | AU5824896A (es) |
| DE (1) | DE69603953T2 (es) |
| ES (1) | ES2138351T3 (es) |
| FR (1) | FR2733756B1 (es) |
| TR (1) | TR199701300T1 (es) |
| WO (1) | WO1996034897A1 (es) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6451967B1 (en) * | 1999-09-20 | 2002-09-17 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Method of drying saponified ethylene-vinyl acetate copolymers |
| ATE281477T1 (de) | 2000-08-07 | 2004-11-15 | Kuraray Co | Verfahren zur verarbeitung von lösungen aus ethylen-vinylalkohol-copolymeren |
| DE60024810T2 (de) * | 2000-08-07 | 2006-08-31 | KURARAY CO., LTD, Kurashiki | Verfahren zur Herstellung von wässrigen Zusammensetzungen aus Ethylen-Vinylalkohol-Copolymeren |
| CN101747459B (zh) * | 2008-12-02 | 2011-09-07 | 卢金永 | 化学改性聚乙烯醇分散剂的制备方法 |
| TWI522373B (zh) | 2015-01-27 | 2016-02-21 | 長春石油化學股份有限公司 | 聚乙烯醇及其純化方法 |
| EP3392165B1 (en) * | 2015-12-18 | 2020-09-23 | Mitsubishi Chemical Corporation | Use of a packaging bag and method for storing melt-processable polyvinyl alcohol resin in which said packaging bag is used |
| CN105837710A (zh) * | 2016-03-31 | 2016-08-10 | 温州小伦包衣技术有限公司 | 药用聚乙烯醇的制备方法及其药用聚乙烯醇与应用 |
| CN110088147B (zh) * | 2016-12-21 | 2023-10-24 | 三菱化学株式会社 | 聚乙烯醇系树脂、分散剂和悬浮聚合用分散剂 |
| JP6981258B2 (ja) * | 2016-12-21 | 2021-12-15 | 三菱ケミカル株式会社 | ポリビニルアルコール系樹脂、分散剤及び懸濁重合用分散剤 |
| CN107151283B (zh) * | 2017-05-27 | 2020-10-27 | 中国石油化工集团公司 | 一种光学材料专用聚乙烯醇的制备方法 |
| US12065517B2 (en) | 2018-09-05 | 2024-08-20 | Kuraray Co., Ltd. | Production method of polyvinyl alcohol resin, and polyvinyl alcohol resin |
| US20240141082A1 (en) * | 2021-03-08 | 2024-05-02 | Sekisui Chemical Co., Ltd. | Poly(vinyl alcohol) resin |
| CN114409831A (zh) * | 2022-01-02 | 2022-04-29 | 浙江尚能实业股份有限公司 | 一种用于扩散源生产的聚乙烯醇树脂提纯方法 |
| CN116445135B (zh) * | 2023-03-31 | 2025-11-07 | 中国科学院武汉岩土力学研究所 | 一种新型生态修复水凝胶型环保抑尘剂及其制备方法 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB933104A (en) * | 1958-12-04 | 1963-08-08 | Kurashiki Rayon Kk | Process of and apparatus for purifying polyvinyl alcohol prepared by saponification |
| FR1360102A (fr) * | 1963-06-07 | 1964-04-30 | Air Reduction | Améliorations au procédé de traitement de l'alcool polyvinylique |
| DE1620946B2 (de) * | 1965-01-30 | 1973-07-05 | Kuraray Co, Ltd , Kurashiki, Oka yama (Japan) | Verfahren zur herstellung von polyvinylalkohol mit niedrigem quellgrad |
| GB1048120A (en) * | 1968-05-20 | 1966-11-09 | Denki Kagaku Kogyo Kk | Production of highly saponified polyvinyl alcohol |
| JPS5217870B2 (es) * | 1973-01-31 | 1977-05-18 | ||
| JPS5543158A (en) * | 1978-09-21 | 1980-03-26 | Nippon Synthetic Chem Ind Co Ltd:The | Preparation of polyvinyl alcohol having improved dispersiblity in water |
| US4731266A (en) * | 1981-06-03 | 1988-03-15 | Rhone-Poulenc, S.A. | Water-resistant polyvinyl alcohol film and its application to the preparation of gas-impermeable composite articles |
-
1995
- 1995-05-05 FR FR9505893A patent/FR2733756B1/fr not_active Expired - Lifetime
-
1996
- 1996-05-06 EP EP96919873A patent/EP0823917B1/fr not_active Expired - Lifetime
- 1996-05-06 ES ES96919873T patent/ES2138351T3/es not_active Expired - Lifetime
- 1996-05-06 KR KR1019970707868A patent/KR100296785B1/ko not_active Expired - Fee Related
- 1996-05-06 TR TR97/01300T patent/TR199701300T1/xx unknown
- 1996-05-06 CN CN96194785A patent/CN1074424C/zh not_active Expired - Fee Related
- 1996-05-06 AU AU58248/96A patent/AU5824896A/en not_active Abandoned
- 1996-05-06 US US08/945,553 patent/US6080814A/en not_active Expired - Lifetime
- 1996-05-06 JP JP53308896A patent/JP3177914B2/ja not_active Expired - Fee Related
- 1996-05-06 AT AT96919873T patent/ATE183755T1/de not_active IP Right Cessation
- 1996-05-06 WO PCT/FR1996/000686 patent/WO1996034897A1/fr not_active Ceased
- 1996-05-06 DE DE69603953T patent/DE69603953T2/de not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| DE69603953D1 (de) | 1999-09-30 |
| CN1074424C (zh) | 2001-11-07 |
| EP0823917A1 (fr) | 1998-02-18 |
| ATE183755T1 (de) | 1999-09-15 |
| DE69603953T2 (de) | 2000-01-27 |
| EP0823917B1 (fr) | 1999-08-25 |
| AU5824896A (en) | 1996-11-21 |
| JPH11504374A (ja) | 1999-04-20 |
| TR199701300T1 (xx) | 1998-02-21 |
| FR2733756B1 (fr) | 1997-08-01 |
| FR2733756A1 (fr) | 1996-11-08 |
| KR19990008342A (ko) | 1999-01-25 |
| WO1996034897A1 (fr) | 1996-11-07 |
| KR100296785B1 (ko) | 2001-10-25 |
| CN1187826A (zh) | 1998-07-15 |
| JP3177914B2 (ja) | 2001-06-18 |
| US6080814A (en) | 2000-06-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FG2A | Definitive protection |
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