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ES2124283T3 - FRUCTOSE CRYSTALLIZATION. - Google Patents

FRUCTOSE CRYSTALLIZATION.

Info

Publication number
ES2124283T3
ES2124283T3 ES93301560T ES93301560T ES2124283T3 ES 2124283 T3 ES2124283 T3 ES 2124283T3 ES 93301560 T ES93301560 T ES 93301560T ES 93301560 T ES93301560 T ES 93301560T ES 2124283 T3 ES2124283 T3 ES 2124283T3
Authority
ES
Spain
Prior art keywords
cooling
crystallization
fructose
reduced
rate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES93301560T
Other languages
Spanish (es)
Inventor
Donald W Lillard
Robert V Schanefelt
Daniel K Tang
Gary A Day
Francis M Mallee
Lawrence R Schwab
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Primary Products Ingredients Americas LLC
Original Assignee
Tate and Lyle Ingredients Americas LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US07/747,775 external-priority patent/US5234503A/en
Priority claimed from US07/747,773 external-priority patent/US5230742A/en
Priority claimed from US07/747,764 external-priority patent/US5350456A/en
Application filed by Tate and Lyle Ingredients Americas LLC filed Critical Tate and Lyle Ingredients Americas LLC
Application granted granted Critical
Publication of ES2124283T3 publication Critical patent/ES2124283T3/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K1/00—Glucose; Glucose-containing syrups
    • C13K1/10—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K11/00—Fructose
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K3/00—Invert sugar; Separation of glucose or fructose from invert sugar

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Seasonings (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Saccharide Compounds (AREA)

Abstract

During fructose crystallization by cooling a fructose solution, the rate of cooling is first reduced and then increased again. The reduced cooling rate is preferably in the temperature band 46 +/- 3 DEG C and this controlled cooling results in an improved product. The process preferably uses the mother liquor remaining after crystallization for the preparation of a liquid phase sweetener.
ES93301560T 1991-08-20 1993-03-01 FRUCTOSE CRYSTALLIZATION. Expired - Lifetime ES2124283T3 (en)

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US07/747,775 US5234503A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high-fructose, liquid-phase sweetener
US07/747,773 US5230742A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and high-fructose, liquid-phase sweetener
US07/747,764 US5350456A (en) 1987-02-02 1991-08-20 Integrated process for producing crystalline fructose and a high fructose, liquid-phase sweetener
EP93301560A EP0613954B1 (en) 1991-08-20 1993-03-01 Fructose crystallization
EP93301559A EP0613953B1 (en) 1991-08-20 1993-03-01 Fructose and dextrose containing liquid sweetener
AU33991/93A AU662391B2 (en) 1991-08-20 1993-03-04 Fructose and dextrose containing liquid sweetener
ZA931871A ZA931871B (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
CA002091706A CA2091706A1 (en) 1991-08-20 1993-03-16 Integrated process for producing crystalline fructose
JP07412893A JP3399576B2 (en) 1991-08-20 1993-03-31 Integrated process for producing crystalline fructose
HU9301156A HUT67470A (en) 1991-08-20 1993-04-19 Integrated process for producing crystalline fructose
BR9301098A BR9301098A (en) 1991-08-20 1993-05-17 Integrated process for the production of crystalline fructose

Publications (1)

Publication Number Publication Date
ES2124283T3 true ES2124283T3 (en) 1999-02-01

Family

ID=27581357

Family Applications (2)

Application Number Title Priority Date Filing Date
ES93301560T Expired - Lifetime ES2124283T3 (en) 1991-08-20 1993-03-01 FRUCTOSE CRYSTALLIZATION.
ES93301559T Expired - Lifetime ES2126627T3 (en) 1991-08-20 1993-03-01 LIQUID SWEETENER CONTAINING FRUCTOSE AND DEXTROSE.

Family Applications After (1)

Application Number Title Priority Date Filing Date
ES93301559T Expired - Lifetime ES2126627T3 (en) 1991-08-20 1993-03-01 LIQUID SWEETENER CONTAINING FRUCTOSE AND DEXTROSE.

Country Status (11)

Country Link
EP (2) EP0613953B1 (en)
JP (1) JP3399576B2 (en)
AT (2) ATE176503T1 (en)
AU (1) AU662391B2 (en)
BR (1) BR9301098A (en)
CA (1) CA2091706A1 (en)
DE (2) DE69321456T2 (en)
ES (2) ES2124283T3 (en)
GR (1) GR3029569T3 (en)
HU (1) HUT67470A (en)
ZA (1) ZA931871B (en)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR0103406A (en) 2001-08-15 2004-05-04 Getec Guanabara Quimica Ind S Process of producing high purity crystalline fructose using low fructose syrup originating from sucrose and product obtained
FI115919B (en) * 2002-06-27 2005-08-15 Danisco Sweeteners Oy Procedure for removing crystallization inhibitors from a solution containing monosaccharide sugar
KR101217137B1 (en) * 2012-03-05 2012-12-31 한국생산기술연구원 Method for manufacturing 5-hydroxymethyl-2-furfural from corn syrup containing fructose
IN2015DN01415A (en) * 2012-08-20 2015-07-03 Naturalia Ingredients S R L
CN103146849B (en) * 2013-03-25 2014-01-08 保龄宝生物股份有限公司 Method for co-producing crystalline fructose and fructose corn syrup by taking wheat as raw material, and preparation method of wheat starch
KR102283524B1 (en) 2015-02-24 2021-07-30 테이트 앤드 라일 인그리디언츠 어메리카즈 엘엘씨 allulose syrup
KR101695831B1 (en) * 2015-05-15 2017-01-12 주식회사 삼양사 Saccharide mixture containing psicose with improved sweetness quality and crystallization
US11254959B2 (en) 2016-05-23 2022-02-22 Annikki Gmbh Process for the conversion of sugars
KR102065155B1 (en) * 2016-12-08 2020-02-11 주식회사 삼양사 Production of psciose
FR3061413B1 (en) * 2017-01-05 2021-08-27 Roquette Freres PROCESS FOR MANUFACTURING D-ALLULOSE CRYSTALS
FR3061414B1 (en) 2017-01-05 2021-07-16 Roquette Freres D-ALLULOSE CRYSTALLIZABLE SYRUPS
KR102004940B1 (en) 2017-06-30 2019-07-29 주식회사 삼양사 production of allulose as sweetener

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2007971A (en) * 1926-11-29 1935-07-16 Richard F Jackson Process of making sugar products
FR1534746A (en) * 1966-04-29 1968-08-02 Boehringer & Soehne Gmbh Process for obtaining fructose in the crystallized state
US3883365A (en) * 1972-01-04 1975-05-13 Suomen Sokeri Oy PH adjustment in fructose crystallization for increased yield
US3816175A (en) * 1972-07-03 1974-06-11 Suomen Sokeri Oy Process for formation of crystalline fructose-glucose blends
JPS5239901B2 (en) * 1973-02-12 1977-10-07
US4199373A (en) * 1979-04-13 1980-04-22 Chimicasa Gmbh Process for the manufacture of crystalline fructose
US4517021A (en) * 1983-10-28 1985-05-14 A. E. Staley Manufacturing Company Semi-crystalline fructose
US4634472A (en) * 1985-08-23 1987-01-06 A. E. Staley Manufacturing Company Enrichment of fructose syrups
US5047088A (en) * 1989-06-30 1991-09-10 A. E. Staley Manufacturing Company Method for crystallization of fructose

Also Published As

Publication number Publication date
ATE171982T1 (en) 1998-10-15
AU3399193A (en) 1994-09-15
JP3399576B2 (en) 2003-04-21
BR9301098A (en) 1994-11-29
ATE176503T1 (en) 1999-02-15
ES2126627T3 (en) 1999-04-01
JPH06277099A (en) 1994-10-04
EP0613954A1 (en) 1994-09-07
DE69321456D1 (en) 1998-11-12
ZA931871B (en) 1993-10-06
HU9301156D0 (en) 1993-07-28
DE69323414D1 (en) 1999-03-18
EP0613953A1 (en) 1994-09-07
DE69321456T2 (en) 1999-06-17
DE69323414T2 (en) 1999-06-10
EP0613954B1 (en) 1998-10-07
AU662391B2 (en) 1995-08-31
HUT67470A (en) 1995-04-28
GR3029569T3 (en) 1999-06-30
EP0613953B1 (en) 1999-02-03
CA2091706A1 (en) 1994-09-17

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