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ES2111800T3 - Recuperacion de acido citrico a partir de corrientes de proceso impuras por adicion de acidos fuertes y sales de los mismos. - Google Patents

Recuperacion de acido citrico a partir de corrientes de proceso impuras por adicion de acidos fuertes y sales de los mismos.

Info

Publication number
ES2111800T3
ES2111800T3 ES94109709T ES94109709T ES2111800T3 ES 2111800 T3 ES2111800 T3 ES 2111800T3 ES 94109709 T ES94109709 T ES 94109709T ES 94109709 T ES94109709 T ES 94109709T ES 2111800 T3 ES2111800 T3 ES 2111800T3
Authority
ES
Spain
Prior art keywords
acid
citric acid
recovery
salts
addition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES94109709T
Other languages
English (en)
Inventor
Steven W Felman
Chetna Patel
Bhalchandra H Patwardhan
David J Solow
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Haarmann and Reimer Corp
Original Assignee
Haarmann and Reimer Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Haarmann and Reimer Corp filed Critical Haarmann and Reimer Corp
Application granted granted Critical
Publication of ES2111800T3 publication Critical patent/ES2111800T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

LA INVENCION SUMINISTRA UN PROCESO MEJORADO PARA RECUPERAR ACIDO CITRICO A PARTIR DE UNA CORRIENTE DE PROCESAMIENTO IMPURA TAL COMO UN CALDO DE FERMENTACION MEDIANTE LA ADICION DE UN ACIDO FUERTE O SALES DEL MISMO A UNA SOLUCION CONCENTRADA DE ACIDO CITRICO. EL PROCESO SUMINISTRA UNA PURIFICACION ESENCIALMENTE DE UN SOLO PASO SIN PROBLEMAS PARA HACER DESAPARECER LOS DESECHOS O SIN REQUERIR UNA GRAN INVERSION DE CAPITAL. LA RECUPERACION PUEDE MEJORARSE ADICIONALMENTE TRATANDO EL LICOR MADRE QUE QUEDA DESPUES DE LA SEPARACION DE LOS CRISTALES DE ACIDO CITRICO PARA OBTENER UN RENDIMIENTO ADICIONAL. EL ACIDO FUERTE MAS ADECUADO ES EL ACIDO SULFURICO Y EL TRATAMIENTO DEL LICOR MADRE PREFERIDO ES UNA COLUMNA DE RESINA DE EXCLUSION DE IONES. MIENTRAS QUE EL PROCESO MEJORADO ES PARTICULARMENTE VENTAJOSO CUANDO SE UTILIZA EN UN PROCESO DE PURIFICACION DE UN SOLO PASO PARA EL ACIDO CITRICO DIRECTAMENTE PROVENIENTE DEL CALDO DE FERMENTACION, TAMBIEN PUEDE UTILIZARSE EN CONJUNCION CON LAS DIFERENTES CORRIENTES DE PROCESAMIENTO IMPURAS GENERADAS POR PROCESOS DE RECUPERACION DE EXTRACCION DE SULFURICO DE CAL O SOLVENTE.
ES94109709T 1993-07-06 1994-06-23 Recuperacion de acido citrico a partir de corrientes de proceso impuras por adicion de acidos fuertes y sales de los mismos. Expired - Lifetime ES2111800T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US8821993A 1993-07-06 1993-07-06

Publications (1)

Publication Number Publication Date
ES2111800T3 true ES2111800T3 (es) 1998-03-16

Family

ID=22210093

Family Applications (1)

Application Number Title Priority Date Filing Date
ES94109709T Expired - Lifetime ES2111800T3 (es) 1993-07-06 1994-06-23 Recuperacion de acido citrico a partir de corrientes de proceso impuras por adicion de acidos fuertes y sales de los mismos.

Country Status (10)

Country Link
US (2) US5712131A (es)
EP (1) EP0633240B1 (es)
JP (1) JPH0767671A (es)
AT (1) ATE162512T1 (es)
AU (1) AU662093B2 (es)
CA (1) CA2126365C (es)
DE (1) DE69408047T2 (es)
ES (1) ES2111800T3 (es)
GR (1) GR3026053T3 (es)
MX (1) MX9405126A (es)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0251582A (ja) * 1988-08-12 1990-02-21 Kyokado Eng Co Ltd 地盤注入用薬液
EP1198444A1 (en) 1999-07-23 2002-04-24 Chemintel (India) Private Limited Process for crystallization of dicarboxylic acids
US6670505B1 (en) 2000-03-07 2003-12-30 Eastman Chemical Company Process for the recovery of organic acids from aqueous solutions
US6320061B1 (en) 2000-06-05 2001-11-20 Eastman Chemical Company Solvent exchange process
PL361230A1 (en) * 2000-10-05 2004-10-04 Biogal Gyogyszergyar Rt. Pravastatin sodium substantially free of pravastatin lactone and epi-pravastatin, and compositions containing same
JP2002121172A (ja) * 2000-10-16 2002-04-23 Sankyo Co Ltd プラバスタチン又はその薬理上許容される塩の精製方法
US7241918B1 (en) * 2003-03-18 2007-07-10 Uop Llc Separation of citric acid from gluconic acid in fermentation broth using a weakly or strongly basic anionic exchange resin adsorbent
JP4469568B2 (ja) * 2003-07-09 2010-05-26 三菱化学株式会社 有機酸の製造方法
BRPI0413403A (pt) * 2003-08-28 2006-10-17 Mitsubishi Chem Corp método para produzir ácido succìnico
JP4631706B2 (ja) * 2003-09-30 2011-02-16 味の素株式会社 発酵液からのコハク酸の精製方法
EP1760143B1 (en) * 2004-05-20 2012-05-16 Ajinomoto Co., Inc. Succinic acid-producing bacterium and process for producing succinic acid
WO2005113745A1 (ja) * 2004-05-20 2005-12-01 Ajinomoto Co., Inc. コハク酸生産菌及びコハク酸の製造方法
JP5088136B2 (ja) * 2005-10-18 2012-12-05 味の素株式会社 コハク酸の製造方法
JP5180060B2 (ja) * 2006-02-24 2013-04-10 三菱化学株式会社 有機酸生産菌及び有機酸の製造法
CN102964242B (zh) * 2012-12-07 2015-01-28 中粮生物化学（安徽）股份有限公司 一种柠檬酸晶体及其生产方法
CN102964241B (zh) * 2012-12-07 2014-10-29 中粮生物化学（安徽）股份有限公司 一种一水柠檬酸晶体的生产方法
CN103145547B (zh) * 2013-03-28 2015-03-25 中粮生物化学（安徽）股份有限公司 一种柠檬酸晶体及其生产方法
CN103145546B (zh) * 2013-03-28 2015-05-06 中粮生物化学（安徽）股份有限公司 一种柠檬酸晶体及其生产方法
DE102015216815A1 (de) * 2015-09-02 2017-03-02 Thyssenkrupp Ag Verfahren und Anlage zur Gewinnung einer in einem Fermentationsprozess hergestellten Carbonsäure
CN109053430A (zh) * 2018-08-30 2018-12-21 河北乐开节能科技股份有限公司 一种高效分离柠檬酸中杂酸的方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE627445C (de) * 1934-04-07 1936-03-16 Chem Fab Joh A Benckiser G M B Verfahren zur Herstellung wasserfreier Citronensaeure
US4851573A (en) * 1986-12-18 1989-07-25 Uop Separation of citric acid from fermentation broth with a weakly basic anionic exchange resin adsorbent
FR2632302B1 (fr) * 1988-06-06 1991-02-22 Roquette Freres Procede de recuperation d'acide citrique a partir d'une liqueur en contenant
US5034105A (en) * 1989-07-27 1991-07-23 Michigan Biotechnology Institute Carboxylic acid purification and crystallization process
US4994609A (en) * 1990-06-06 1991-02-19 Innova S.A. Production of citric acid

Also Published As

Publication number Publication date
DE69408047T2 (de) 1998-05-07
ATE162512T1 (de) 1998-02-15
EP0633240A1 (en) 1995-01-11
EP0633240B1 (en) 1998-01-21
CA2126365A1 (en) 1995-01-07
JPH0767671A (ja) 1995-03-14
MX9405126A (es) 1995-01-31
AU6615894A (en) 1995-01-27
AU662093B2 (en) 1995-08-17
CA2126365C (en) 1999-08-24
DE69408047D1 (de) 1998-02-26
US5827700A (en) 1998-10-27
GR3026053T3 (en) 1998-05-29
US5712131A (en) 1998-01-27

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