ES2177409A1 - Production of pyridine derivatives, useful for hypertension treatment, comprises reaction of an acetoacetate with an amino crotonate, for solvent treatment and evaporation - Google Patents
Production of pyridine derivatives, useful for hypertension treatment, comprises reaction of an acetoacetate with an amino crotonate, for solvent treatment and evaporationInfo
- Publication number
- ES2177409A1 ES2177409A1 ES200001967A ES200001967A ES2177409A1 ES 2177409 A1 ES2177409 A1 ES 2177409A1 ES 200001967 A ES200001967 A ES 200001967A ES 200001967 A ES200001967 A ES 200001967A ES 2177409 A1 ES2177409 A1 ES 2177409A1
- Authority
- ES
- Spain
- Prior art keywords
- treatment
- acetoacetate
- production
- pyridine derivatives
- evaporation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 206010020772 Hypertension Diseases 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 150000003222 pyridines Chemical class 0.000 title abstract 2
- WDJHALXBUFZDSR-UHFFFAOYSA-M acetoacetate Chemical compound CC(=O)CC([O-])=O WDJHALXBUFZDSR-UHFFFAOYSA-M 0.000 title 1
- RLKBOGLIOLFMEK-NSCUHMNNSA-N amino (e)-but-2-enoate Chemical compound C\C=C\C(=O)ON RLKBOGLIOLFMEK-NSCUHMNNSA-N 0.000 title 1
- 230000008020 evaporation Effects 0.000 title 1
- 238000001704 evaporation Methods 0.000 title 1
- 239000002904 solvent Substances 0.000 title 1
- 125000000217 alkyl group Chemical group 0.000 abstract 2
- YNGDWRXWKFWCJY-UHFFFAOYSA-N 1,4-Dihydropyridine Chemical class C1C=CNC=C1 YNGDWRXWKFWCJY-UHFFFAOYSA-N 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Landscapes
- Pyridine Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
Production pyridine derivatives, for treatment of hypertension, comprises: (1) reaction of an alkyl 2-methylidene acetoacetate with an alkyl 3-amino crotonate adsorbed on a porous solid surface and (2) dissolving the mixture in an organic solvent which is then evaporated for purification of substituted 1,4-dihydro pyridines.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200001967A ES2177409B1 (en) | 2000-08-02 | 2000-08-02 | PROCEDURE FOR OBTAINING SUBSTITUTED 1,4-DIHYDROPIRIDINES USEFUL FOR THE TREATMENT OF HYPERTENSION. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES200001967A ES2177409B1 (en) | 2000-08-02 | 2000-08-02 | PROCEDURE FOR OBTAINING SUBSTITUTED 1,4-DIHYDROPIRIDINES USEFUL FOR THE TREATMENT OF HYPERTENSION. |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES2177409A1 true ES2177409A1 (en) | 2002-12-01 |
| ES2177409B1 ES2177409B1 (en) | 2003-08-01 |
Family
ID=8494565
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES200001967A Expired - Fee Related ES2177409B1 (en) | 2000-08-02 | 2000-08-02 | PROCEDURE FOR OBTAINING SUBSTITUTED 1,4-DIHYDROPIRIDINES USEFUL FOR THE TREATMENT OF HYPERTENSION. |
Country Status (1)
| Country | Link |
|---|---|
| ES (1) | ES2177409B1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7671208B2 (en) | 2007-03-30 | 2010-03-02 | Esteve Quimica, S.A. | Acetone solvate of phthaloyl amlodipine |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2009136A6 (en) * | 1985-08-06 | 1989-09-01 | Boehringer Biochemia Srl | Pharmaceutically active 2-thiomethyl-substituted-1,4-dihydropyridines. |
| ES2055655A1 (en) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedure for obtaining 3-isobutyl-5-methyl 2,6-dimethyl- 4-(2'-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate |
| ES2055652A1 (en) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedure for obtaining 3-ethyl-5-methyl 2,6-dimethyl-4- (2',3'-dichlorophenyl)-1,4-dihydropyridine-3,5- dicarboxylate |
-
2000
- 2000-08-02 ES ES200001967A patent/ES2177409B1/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES2009136A6 (en) * | 1985-08-06 | 1989-09-01 | Boehringer Biochemia Srl | Pharmaceutically active 2-thiomethyl-substituted-1,4-dihydropyridines. |
| ES2055655A1 (en) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedure for obtaining 3-isobutyl-5-methyl 2,6-dimethyl- 4-(2'-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate |
| ES2055652A1 (en) * | 1992-09-22 | 1994-08-16 | Elmuquimica Farm Sl | Procedure for obtaining 3-ethyl-5-methyl 2,6-dimethyl-4- (2',3'-dichlorophenyl)-1,4-dihydropyridine-3,5- dicarboxylate |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7671208B2 (en) | 2007-03-30 | 2010-03-02 | Esteve Quimica, S.A. | Acetone solvate of phthaloyl amlodipine |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2177409B1 (en) | 2003-08-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EC2A | Search report published |
Date of ref document: 20021201 Kind code of ref document: A1 |
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| FG2A | Definitive protection |
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| FD1A | Patent lapsed |
Effective date: 20100412 |