EP3990165A4 - FLUIDIZED BED REACTOR SYSTEM ALLOWING SAMPLING OF PARTICLES DURING AN ON-GOING REACTION - Google Patents
FLUIDIZED BED REACTOR SYSTEM ALLOWING SAMPLING OF PARTICLES DURING AN ON-GOING REACTION Download PDFInfo
- Publication number
- EP3990165A4 EP3990165A4 EP20832615.7A EP20832615A EP3990165A4 EP 3990165 A4 EP3990165 A4 EP 3990165A4 EP 20832615 A EP20832615 A EP 20832615A EP 3990165 A4 EP3990165 A4 EP 3990165A4
- Authority
- EP
- European Patent Office
- Prior art keywords
- fluidized bed
- bed reactor
- reactor system
- particles during
- system allowing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1818—Feeding of the fluidising gas
- B01J8/1827—Feeding of the fluidising gas the fluidising gas being a reactant
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1809—Controlling processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/005—Separating solid material from the gas/liquid stream
- B01J8/007—Separating solid material from the gas/liquid stream by sedimentation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1818—Feeding of the fluidising gas
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1836—Heating and cooling the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
- B01J8/44—Fluidisation grids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
- B01J2208/0015—Plates; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
- B01J2208/00212—Plates; Jackets; Cylinders
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00389—Controlling the temperature using electric heating or cooling elements
- B01J2208/00415—Controlling the temperature using electric heating or cooling elements electric resistance heaters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
- B01J2208/00938—Flow distribution elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
- B01J2208/00946—Features relating to the reactants or products
- B01J2208/00955—Sampling of the particulate material, the reactants or the products
- B01J2208/00982—Particulate material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00796—Details of the reactor or of the particulate material
- B01J2208/00991—Disengagement zone in fluidised-bed reactors
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP25159387.7A EP4534194A3 (en) | 2019-06-26 | 2020-06-25 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US16/453,571 US10717061B1 (en) | 2019-06-26 | 2019-06-26 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
| PCT/US2020/039541 WO2020264104A1 (en) | 2019-06-26 | 2020-06-25 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
Related Child Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP25159387.7A Division-Into EP4534194A3 (en) | 2019-06-26 | 2020-06-25 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
| EP25159387.7A Division EP4534194A3 (en) | 2019-06-26 | 2020-06-25 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| EP3990165A1 EP3990165A1 (en) | 2022-05-04 |
| EP3990165A4 true EP3990165A4 (en) | 2023-07-19 |
| EP3990165B1 EP3990165B1 (en) | 2025-04-16 |
| EP3990165C0 EP3990165C0 (en) | 2025-04-16 |
Family
ID=71611868
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP25159387.7A Pending EP4534194A3 (en) | 2019-06-26 | 2020-06-25 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
| EP20832615.7A Active EP3990165B1 (en) | 2019-06-26 | 2020-06-25 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP25159387.7A Pending EP4534194A3 (en) | 2019-06-26 | 2020-06-25 | Fluidized bed reactor system allowing particle sampling during an ongoing reaction |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US10717061B1 (en) |
| EP (2) | EP4534194A3 (en) |
| JP (2) | JP7342151B2 (en) |
| KR (1) | KR102419304B1 (en) |
| CN (2) | CN114269466B (en) |
| CA (1) | CA3145411C (en) |
| EA (1) | EA202290153A1 (en) |
| ES (1) | ES3028839T3 (en) |
| WO (1) | WO2020264104A1 (en) |
| ZA (1) | ZA202200897B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2025503023A (en) * | 2022-01-21 | 2025-01-30 | エックス-エナジー, エルエルシー | Method for depositing ceramic layers using liquid organometallic precursors - Patents.com |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2007145474A1 (en) * | 2006-06-15 | 2007-12-21 | Korea Research Institute Of Chemical Technology | Method for continual preparation of polycrystalline silicon using a fluidized bed reactor |
| US20080267834A1 (en) * | 2006-02-07 | 2008-10-30 | Hee Young Kim | High-Pressure Fluidized Bed Reactor for Preparing Granular Polycrystalline Silicon |
| US20080299291A1 (en) * | 2007-05-04 | 2008-12-04 | Wacker Chemie Ag | Process For The Continuous Production Of Polycrystalline High-Purity Silicon Granules |
| US20100290970A1 (en) * | 2009-05-12 | 2010-11-18 | Staffin H Kenneth | Fluidized bed process for synthesizing trichlorosilane and a trichlorosilane synthesizer |
| CN201867312U (en) * | 2010-11-18 | 2011-06-15 | 安徽淮化股份有限公司 | Gas-liquid-solid three-phase simultaneously sampling device of fluidized bed reactor |
| US20140017137A1 (en) * | 2012-07-12 | 2014-01-16 | Siliken Chemicals, Sl | Cooled gas distribution plate, thermal bridge breaking system, and related methods |
| WO2014035878A1 (en) * | 2012-08-29 | 2014-03-06 | Hemlock Semiconductor Corporation | Tapered fluidized bed reactor and process for its use |
| US20140335008A1 (en) * | 2006-08-10 | 2014-11-13 | Korea Research Institute Of Chemical Technology | Method and Apparatus for Preparation of Granular Polysilicon |
| WO2017005501A1 (en) * | 2015-07-03 | 2017-01-12 | Outotec (Finland) Oy | Process and plant for roasting of dry ore particles in a fluidized bed |
Family Cites Families (30)
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| US3034657A (en) * | 1959-03-24 | 1962-05-15 | Lewis M Newmyer | Device for displaying a plurality of articles, such as bottles and the like |
| DE2203544A1 (en) * | 1972-01-26 | 1973-08-09 | Bergwerksverband Gmbh | DEVICE FOR SEPARATING THE LARGER AND / OR HEAVY PART OF A GRAIN SLIP FROM A FLUIDIZED MATERIAL MIXTURE |
| JPS50113474A (en) * | 1974-02-18 | 1975-09-05 | ||
| SE438729B (en) * | 1980-03-21 | 1985-04-29 | Asea Ab | DEVICE AT THE BOTTOM OF A FLUIDIZABLE BED |
| US4405561A (en) * | 1981-10-26 | 1983-09-20 | Foster Wheeler Energy Corporation | Drain and sampling valve assembly for a fluidized bed reactor |
| US4543399A (en) | 1982-03-24 | 1985-09-24 | Union Carbide Corporation | Fluidized bed reaction systems |
| FR2526182B1 (en) | 1982-04-28 | 1985-11-29 | Creusot Loire | METHOD AND DEVICE FOR CONTROLLING THE TEMPERATURE OF A FLUIDIZED BED |
| JPS5936028A (en) * | 1982-08-19 | 1984-02-28 | Denka Consult & Eng Co Ltd | Pneumatic conveyor being easily adjustable to dischage of powdery granular body |
| FR2559074B1 (en) * | 1984-02-07 | 1988-05-20 | Inst Francais Du Petrole | METHOD AND APPARATUS FOR SUPPORTING CATALYTIC PARTICLES OUTSIDE A REACTION ZONE |
| US4828581A (en) | 1985-09-20 | 1989-05-09 | Battelle Development Corporation | Low inlet gas velocity high throughput biomass gasifier |
| JPH0713557B2 (en) * | 1986-03-28 | 1995-02-15 | 川崎重工業株式会社 | Fluidized bed dispersion plate |
| US4906441A (en) * | 1987-11-25 | 1990-03-06 | Union Carbide Chemicals And Plastics Company Inc. | Fluidized bed with heated liners and a method for its use |
| US4973458A (en) | 1989-05-09 | 1990-11-27 | Westinghouse Electric Corp. | Fluidized bed system for removing particulate contaminants from a gaseous stream |
| US6025448A (en) | 1989-08-31 | 2000-02-15 | The Dow Chemical Company | Gas phase polymerization of olefins |
| CH685104A5 (en) * | 1993-05-25 | 1995-03-31 | Buehler Ag | Apparatus and method for dosing solid present in a gas / solid stream from a fluidized bed. |
| JPH06191818A (en) * | 1992-12-22 | 1994-07-12 | Tonen Chem Corp | Production of polycrystal silicon |
| US5453471B1 (en) | 1994-08-02 | 1999-02-09 | Carbide Chemicals & Plastics T | Gas phase polymerization process |
| US5798137A (en) | 1995-06-07 | 1998-08-25 | Advanced Silicon Materials, Inc. | Method for silicon deposition |
| JP3661317B2 (en) * | 1996-11-01 | 2005-06-15 | チッソ株式会社 | Granule coating apparatus and granule coating method |
| DE10124848A1 (en) | 2001-05-22 | 2002-11-28 | Solarworld Ag | Production of high-purity granular silicon by thermal decomposition of silanes or halosilanes in a fluidized-bed reactor comprises separating particles of the desired size in an external classifier |
| WO2009085109A2 (en) | 2007-12-27 | 2009-07-09 | Univation Technologies, Llc | Systems and methods for removing entrained particulates from gas streams, and reactor systems implementing the same |
| EP2303448B1 (en) * | 2008-06-30 | 2012-10-31 | MEMC Electronic Materials, Inc. | Fluidized bed reactor systems and methods for reducing the deposition of silicon on reactor walls |
| CN103787336B (en) * | 2008-09-16 | 2016-09-14 | 储晞 | The method producing high purity granular silicon |
| EP2174706A1 (en) | 2008-10-03 | 2010-04-14 | Ineos Europe Limited | Apparatus and process for gas phase fluidised bed polymerisation |
| EP2446960A1 (en) * | 2010-10-29 | 2012-05-02 | Borealis AG | Feeding solid material into a high density fluidized bed reactor |
| CN102032997B (en) * | 2010-11-18 | 2012-08-22 | 安徽淮化股份有限公司 | Gas-liquid-solid three-phase simultaneous sampling device of fluid bed reactor |
| KR101329032B1 (en) * | 2011-04-20 | 2013-11-14 | 주식회사 실리콘밸류 | Apparatus for manufacturing polycrystalline silicon and method for manufacturing polycrystalline silicon using the same |
| CN205061573U (en) * | 2015-07-24 | 2016-03-02 | 江苏中能硅业科技发展有限公司 | Prepare fluidized bed reactor of high pure silicon polycrystal |
| CN109126641B (en) * | 2017-06-15 | 2022-03-01 | 国家能源投资集团有限责任公司 | Fischer-Tropsch synthesis catalyst fluidized bed reduction device and online sampling method |
| CN114599447B (en) * | 2019-10-25 | 2025-05-02 | 埃克森美孚化学专利公司 | Fluidized bed reactor system |
-
2019
- 2019-06-26 US US16/453,571 patent/US10717061B1/en active Active
-
2020
- 2020-06-25 CN CN202080057210.8A patent/CN114269466B/en active Active
- 2020-06-25 EA EA202290153A patent/EA202290153A1/en unknown
- 2020-06-25 CA CA3145411A patent/CA3145411C/en active Active
- 2020-06-25 EP EP25159387.7A patent/EP4534194A3/en active Pending
- 2020-06-25 ES ES20832615T patent/ES3028839T3/en active Active
- 2020-06-25 EP EP20832615.7A patent/EP3990165B1/en active Active
- 2020-06-25 JP JP2021576105A patent/JP7342151B2/en active Active
- 2020-06-25 CN CN202310952596.4A patent/CN117225310A/en active Pending
- 2020-06-25 WO PCT/US2020/039541 patent/WO2020264104A1/en not_active Ceased
- 2020-06-25 KR KR1020227000506A patent/KR102419304B1/en active Active
-
2022
- 2022-01-19 ZA ZA2022/00897A patent/ZA202200897B/en unknown
-
2023
- 2023-06-06 JP JP2023092944A patent/JP2023113808A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20080267834A1 (en) * | 2006-02-07 | 2008-10-30 | Hee Young Kim | High-Pressure Fluidized Bed Reactor for Preparing Granular Polycrystalline Silicon |
| WO2007145474A1 (en) * | 2006-06-15 | 2007-12-21 | Korea Research Institute Of Chemical Technology | Method for continual preparation of polycrystalline silicon using a fluidized bed reactor |
| US20140335008A1 (en) * | 2006-08-10 | 2014-11-13 | Korea Research Institute Of Chemical Technology | Method and Apparatus for Preparation of Granular Polysilicon |
| US20080299291A1 (en) * | 2007-05-04 | 2008-12-04 | Wacker Chemie Ag | Process For The Continuous Production Of Polycrystalline High-Purity Silicon Granules |
| US20100290970A1 (en) * | 2009-05-12 | 2010-11-18 | Staffin H Kenneth | Fluidized bed process for synthesizing trichlorosilane and a trichlorosilane synthesizer |
| CN201867312U (en) * | 2010-11-18 | 2011-06-15 | 安徽淮化股份有限公司 | Gas-liquid-solid three-phase simultaneously sampling device of fluidized bed reactor |
| US20140017137A1 (en) * | 2012-07-12 | 2014-01-16 | Siliken Chemicals, Sl | Cooled gas distribution plate, thermal bridge breaking system, and related methods |
| WO2014035878A1 (en) * | 2012-08-29 | 2014-03-06 | Hemlock Semiconductor Corporation | Tapered fluidized bed reactor and process for its use |
| WO2017005501A1 (en) * | 2015-07-03 | 2017-01-12 | Outotec (Finland) Oy | Process and plant for roasting of dry ore particles in a fluidized bed |
Non-Patent Citations (1)
| Title |
|---|
| See also references of WO2020264104A1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| JP2022545149A (en) | 2022-10-26 |
| KR20220047967A (en) | 2022-04-19 |
| EP3990165B1 (en) | 2025-04-16 |
| CA3145411A1 (en) | 2020-12-30 |
| JP2023113808A (en) | 2023-08-16 |
| EA202290153A1 (en) | 2022-02-17 |
| KR102419304B1 (en) | 2022-07-11 |
| CN114269466A (en) | 2022-04-01 |
| CA3145411C (en) | 2023-02-14 |
| CN114269466B (en) | 2023-08-18 |
| EP3990165C0 (en) | 2025-04-16 |
| JP7342151B2 (en) | 2023-09-11 |
| EP4534194A2 (en) | 2025-04-09 |
| WO2020264104A1 (en) | 2020-12-30 |
| EP3990165A1 (en) | 2022-05-04 |
| ES3028839T3 (en) | 2025-06-20 |
| US10717061B1 (en) | 2020-07-21 |
| EP4534194A3 (en) | 2025-06-11 |
| ZA202200897B (en) | 2023-06-28 |
| CN117225310A (en) | 2023-12-15 |
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| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
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