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EP3625321B1 - Procédé de production de préparations gélifiées - Google Patents

Procédé de production de préparations gélifiées Download PDF

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Publication number
EP3625321B1
EP3625321B1 EP18720246.0A EP18720246A EP3625321B1 EP 3625321 B1 EP3625321 B1 EP 3625321B1 EP 18720246 A EP18720246 A EP 18720246A EP 3625321 B1 EP3625321 B1 EP 3625321B1
Authority
EP
European Patent Office
Prior art keywords
production line
premixture
batch production
line
filling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP18720246.0A
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German (de)
English (en)
Other versions
EP3625321B2 (fr
EP3625321A1 (fr
Inventor
Uwe Trebbe
Harald Müller
Thomas Holderbaum
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
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Henkel AG and Co KGaA
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Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Priority to PL18720246.0T priority Critical patent/PL3625321T5/pl
Publication of EP3625321A1 publication Critical patent/EP3625321A1/fr
Application granted granted Critical
Publication of EP3625321B1 publication Critical patent/EP3625321B1/fr
Publication of EP3625321B2 publication Critical patent/EP3625321B2/fr
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00—Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0094—Process for making liquid detergent compositions, e.g. slurries, pastes or gels
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
    • C11D17/003—Colloidal solutions, e.g. gels; Thixotropic solutions or pastes
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols

Definitions

  • the present invention relates to a method for producing gel-like substances, in particular gel-like washing or cleaning agents.
  • EP 2746379 A1 discloses the production of liquid detergent preparations by mixing a perfume-free solution with a solution containing surfactant and perfume.
  • the process should be suitable for the production of gel-form detergents and cleaning agents.
  • a method for producing substances in gel form comprises providing a premix on a batch production line, the premix containing at least water, glycerol and surfactants.
  • the method further comprises adding supplements to the premix, the supplements comprising at least fragrances, on a filling line following the batch production line.
  • supplements in particular fragrances
  • a filling line is understood to mean that part of a production line from which the finished product is filled, for example into single-volume containers. Upstream of the filling line is the batch production line, in which the mixing of all ingredients apart from the Supplements takes place and on which the almost finished product is optionally held in a collecting container in order to be fed to the filling line.
  • a first starting mixture containing water, glycerol and liquid nonionic surfactants and a second starting mixture containing at least fatty alcohol ethoxylates (FAEO) are prepared to provide the premix.
  • the two starting mixtures are mixed in a mixer on the batch production line. This can in particular be a static mixer.
  • the premix is particularly easy to process and the formation of bubbles is minimized.
  • the premix is provided at a temperature of at least 60 ° C., in particular of at least 75 ° C., on the batch production line.
  • a temperature of at least 60 ° C., in particular of at least 75 ° C. on the batch production line.
  • Such high temperatures on the batch production line have the advantage that the premix has a relatively low viscosity and the individual components can be mixed well.
  • the supplements are mixed in at temperatures of at most 40 ° C. on the filling line.
  • the supplements can be mixed in at room temperature on the filling line.
  • At least one color can also be added on the filling line.
  • the premix is divided into at least two parts after the batch production line, which are further treated on different filling lines, with a first part of the premix other supplements being added than a second part.
  • This approach has the advantage that different branches of filling lines provide different end products.
  • the production can thus be varied in some parameters in the last phase of the bottling process by adding different supplements.
  • This has the advantage that production is particularly economical and flexible. In particular, the cleaning effort and waste are reduced because the same premix can be used on the batch production line for different end products on different filling lines.
  • Figure 1 shows a production line 1 for the production of gel-like substances, in particular for the production of gel-like detergents or cleaning agents.
  • the production line 1 is divided into a batch production line 2 and a subsequent filling line 3.
  • a batch is produced, ie a large amount of the substance by mixing different starting substances.
  • the filling line 3 the finished substance is filled, for example, into a number of individual quantity containers. According to the invention, supplements are also added on the filling line 3.
  • the gel-like substance is not yet finished on the batch production line 2, but a premix is provided, which has to be supplemented by the supplements in order to obtain the finished gel-like substance.
  • a first starting mixture 4 is initially provided on the batch production line 2.
  • the first starting mixture 4 contains at least water, glycerine and liquid nonionic surfactants. This first starting mixture 4 is typically provided at a temperature of approximately 80.degree.
  • the components of the first starting mixture can be mixed statically or dynamically, for example by means of a planetary mixer. After mixing, the first starting mixture 4 can be kept in a collecting container 5 for further steps.
  • a second starting mixture 6 is then added to the first starting mixture 4, the second starting mixture 6 containing in particular fatty alcohol ethoxylates (FAEO).
  • the second starting mixture 6 is also typically at one temperature of 80 ° C provided.
  • the first starting mixture 4 and the second starting mixture 6 are mixed in a mixer 7, in particular a static mixer, to provide the premix.
  • the finished premix is thus available at the exit of the batch production line 2 at a temperature of 80 ° C.
  • the premix can be divided into different branches.
  • the premix is divided into a first branch 8 and a second branch 9 of the filling line 3.
  • a first supplement 10 is added to the premix and mixed with it in a mixer 11, in particular a static mixer.
  • the first supplement 10 contains in particular at least one first fragrance.
  • the first supplement 10 contains a first dye. The gel-like substance is thus obtained. It can be held in a collecting container 12 for filling and, if necessary, can be circulated until it is filled.
  • a second supplement 13 is added to the premix instead of the first supplement 10.
  • a second supplement 13 is used, which has at least a second fragrance and a second dye.
  • the second supplement 13 is metered into the premix at a temperature of 25 ° C. in order to obtain the finished gel-like substance with a second fragrance and a second color.
  • a collecting container 15 can also be provided in the second branch 9, in which the finished gel-like substance is kept ready for filling and, if necessary, is circulated.
  • FIG. 11 shows a flow chart of the based on FIG Figure 1 described procedure.
  • a first starting mixture 4 and a second starting mixture 6 are provided on the batch production line 2 at temperatures of approximately 80 ° C.
  • a second step 200 the two starting mixtures 4, 6 are mixed with one another, in particular with the aid of a static mixer 7.
  • a third step 300 the premix obtained in this way is fed to a filling line 3 of the production line 1.
  • a fourth step 400 at least one supplement 10, 13 is added to the premix.
  • a fifth step 500 the finished gel-like substance is filled.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Dispersion Chemistry (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Claims (8)

  1. Procédé de production de substances gélifiées, dans lequel le procédé comprend les étapes suivantes :
    - fourniture d'un prémélange sur une ligne de production en lots (2), le prémélange contenant au moins de l'eau, de la glycérine et des tensioactifs, et
    - mélange d'additifs (10, 13) permettant le prémélange sur une ligne de remplissage (3) suivant la ligne de production en lots (2), les additifs (10, 13) comprenant au moins des matières odorantes.
  2. Procédé selon la revendication 1,
    dans lequel un premier mélange initial (4) contenant de l'eau, de la glycérine et des tensioactifs non ioniques liquides et un second mélange initial (6) contenant au moins des éthoxylates d'alcool gras sont fournis pour fournir le prémélange, et les deux mélanges initiaux (4, 6) sont mélangés dans un mélangeur (7) de la ligne de production en lots (2).
  3. Procédé selon la revendication 1 ou 2,
    dans lequel le prémélange est fourni à une température d'au moins 60 °C sur la ligne de production en lots (2).
  4. Procédé selon l'une des revendications 1 à 3,
    dans lequel le prémélange est fourni à une température d'au moins 75 °C sur la ligne de production en lots (2).
  5. Procédé selon l'une des revendications 1 à 4,
    dans lequel les additifs (10, 13) sont mélangés à des températures d'au plus 40 °C sur la ligne de remplissage (3).
  6. Procédé selon l'une des revendications 1 à 5,
    dans lequel les additifs (10, 13) sont mélangés à température ambiante sur la ligne de remplissage (3).
  7. Procédé selon l'une des revendications 1 à 6,
    dans lequel, en plus des matières odorantes sur la ligne de remplissage (3), au moins un colorant est également ajouté au mélange.
  8. Procédé selon l'une des revendications 1 à 7,
    dans lequel le prémélange est divisé en au moins deux parties après la ligne de production en lots (2), lesquelles parties sont post-traitées sur différentes lignes de remplissage (3), d'autres additifs (10, 13) étant ajoutés à une première partie du prémélange par rapport à une seconde partie.
EP18720246.0A 2017-05-19 2018-04-26 Procédé de production de préparations gélifiées Active EP3625321B2 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
PL18720246.0T PL3625321T5 (pl) 2017-05-19 2018-04-26 Sposób wytwarzania preparatów w postaci żelu

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102017208559.2A DE102017208559A1 (de) 2017-05-19 2017-05-19 Verfahren zur Herstellung gelförmiger Substanzen
PCT/EP2018/060659 WO2018210542A1 (fr) 2017-05-19 2018-04-26 Procédé de production de préparations gélifiées

Publications (3)

Publication Number Publication Date
EP3625321A1 EP3625321A1 (fr) 2020-03-25
EP3625321B1 true EP3625321B1 (fr) 2021-06-09
EP3625321B2 EP3625321B2 (fr) 2024-05-01

Family

ID=62063074

Family Applications (1)

Application Number Title Priority Date Filing Date
EP18720246.0A Active EP3625321B2 (fr) 2017-05-19 2018-04-26 Procédé de production de préparations gélifiées

Country Status (5)

Country Link
EP (1) EP3625321B2 (fr)
DE (1) DE102017208559A1 (fr)
ES (1) ES2880777T5 (fr)
PL (1) PL3625321T5 (fr)
WO (1) WO2018210542A1 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US12042552B2 (en) 2020-09-10 2024-07-23 The Procter & Gamble Company Late-stage product differentiation process for personal care products

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102021200796A1 (de) 2021-01-28 2022-07-28 Psa Automobiles Sa Verstausystem für ein Ladekabel eines Elektrofahrzeugs
DE102022203706A1 (de) * 2022-04-13 2023-10-19 Henkel Ag & Co. Kgaa Verfahren zur Herstellung einer Waschmittelportionseinheit

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2217341A (en) 1988-02-04 1989-10-25 Colgate Palmolive Co Thixotropic aqueous automatic dishwashing detergent composition
US5296157A (en) 1991-03-05 1994-03-22 The Proctor & Gamble Company Liquid soap personal cleanser with critical heat cycle stabilizing system
US5518645A (en) 1992-05-19 1996-05-21 Henkel Kommanditgesellschaft Auf Aktien Process for the production of paste-form detergents
US20040116539A1 (en) 2002-12-16 2004-06-17 Unilever Home & Personal Care Usa, Division Of Conopco, Inc. Late variant addition process for personal care products
US20040247534A1 (en) 2003-06-06 2004-12-09 Sultan Dental Products, Ltd Foamable fluoride gel compositions and methods of treatment using the same
WO2010034736A1 (fr) 2008-09-25 2010-04-01 Unilever Plc Détergents liquides
WO2012061991A1 (fr) 2010-11-11 2012-05-18 Unilever Plc Compositions revitalisantes pour la peau sans rinçage à l'état non solide contenant de l'acide 12-hydroxystéarique

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2606393B1 (fr) † 1986-11-10 1989-03-10 Erca Procede et installation de remplissage de recipients avec un melange d'au moins deux produits pateux et/ou liquides
JP2008031115A (ja) † 2006-07-31 2008-02-14 Sunstar Inc 液体組成物の製造方法及び装置
DE102010055770A1 (de) 2010-12-23 2012-06-28 Beiersdorf Ag Verfahren zur Herstellung kosmetischer und/oder dermatologischer Emulsionen mit einem oder mehreren Glucosylglyceriden
EP2746379B1 (fr) * 2012-12-20 2017-03-29 The Procter & Gamble Company Procédé de production d'une composition liquide
EP3031891B1 (fr) * 2014-12-12 2019-03-20 The Procter and Gamble Company Sachet soluble dans l'eau de détergent de lessive à compartiments multiples
BR112017018719A2 (pt) * 2015-03-02 2018-04-17 Unilever Nv fluido de limpeza perfumado viscoso para uma limpeza de um substrato e método de fabricação de uma composição de limpeza fluida viscosa para limpeza de um substrato com uma alta viscosidade de escoamento

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2217341A (en) 1988-02-04 1989-10-25 Colgate Palmolive Co Thixotropic aqueous automatic dishwashing detergent composition
US5296157A (en) 1991-03-05 1994-03-22 The Proctor & Gamble Company Liquid soap personal cleanser with critical heat cycle stabilizing system
US5518645A (en) 1992-05-19 1996-05-21 Henkel Kommanditgesellschaft Auf Aktien Process for the production of paste-form detergents
US20040116539A1 (en) 2002-12-16 2004-06-17 Unilever Home & Personal Care Usa, Division Of Conopco, Inc. Late variant addition process for personal care products
US20040247534A1 (en) 2003-06-06 2004-12-09 Sultan Dental Products, Ltd Foamable fluoride gel compositions and methods of treatment using the same
WO2010034736A1 (fr) 2008-09-25 2010-04-01 Unilever Plc Détergents liquides
WO2012061991A1 (fr) 2010-11-11 2012-05-18 Unilever Plc Compositions revitalisantes pour la peau sans rinçage à l'état non solide contenant de l'acide 12-hydroxystéarique

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
"Handbook of Detergents", 1 January 2009, CRC PRESS, article BAYLY A. E., D. J. SMITH, NIGEL S. ROBERTS, DAVID W. YORK, S. CAPECI, URI ZOLLER, SOSIS P.: "Detergent Processing", pages: 323 - 331, XP055903245
"Perfumes, Cosmetics and Soaps", 1 January 1974, article HOWARD G M., POUCHER W. A.: "CHAPTER TWELVE The Skin-Preparations for the Face and Hands", pages: 310 - 401, XP055903238
"Waschmittel. Chemie, Umwelt, Nachhaltigkeit", 1 January 2005, WILEY-VCH, article WAGNER GÜNTER: "Herstellung von flüssigen Waschmitteln", pages: 140 - 142, XP055903254

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US12042552B2 (en) 2020-09-10 2024-07-23 The Procter & Gamble Company Late-stage product differentiation process for personal care products

Also Published As

Publication number Publication date
ES2880777T5 (es) 2024-12-02
WO2018210542A1 (fr) 2018-11-22
EP3625321B2 (fr) 2024-05-01
PL3625321T3 (pl) 2021-10-04
DE102017208559A1 (de) 2018-11-22
ES2880777T3 (es) 2021-11-25
EP3625321A1 (fr) 2020-03-25
PL3625321T5 (pl) 2024-07-15

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