[go: up one dir, main page]

EP2627818B1 - Method and arrangement for treating pulp - Google Patents

Method and arrangement for treating pulp Download PDF

Info

Publication number
EP2627818B1
EP2627818B1 EP11779190.5A EP11779190A EP2627818B1 EP 2627818 B1 EP2627818 B1 EP 2627818B1 EP 11779190 A EP11779190 A EP 11779190A EP 2627818 B1 EP2627818 B1 EP 2627818B1
Authority
EP
European Patent Office
Prior art keywords
pulp
tower
dilution
consistency
homogenizing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
EP11779190.5A
Other languages
German (de)
French (fr)
Other versions
EP2627818A1 (en
Inventor
Simo Kiero
Kari Peltonen
Sami Siik
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Andritz Oy
Original Assignee
Andritz Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Andritz Oy filed Critical Andritz Oy
Publication of EP2627818A1 publication Critical patent/EP2627818A1/en
Application granted granted Critical
Publication of EP2627818B1 publication Critical patent/EP2627818B1/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21DTREATMENT OF THE MATERIALS BEFORE PASSING TO THE PAPER-MAKING MACHINE
    • D21D5/00Purification of the pulp suspension by mechanical means; Apparatus therefor
    • D21D5/28Tanks for storing or agitating pulp

Definitions

  • the present invention relates to a method and arrangement for treating pulp to be fed to a screen room at a pulp mill.
  • the wood material is fed into a digester where wood chips are treated so that pulp (brown stock) is produced and subsequent to the digester the pulp is mainly in fibrous state or it can at least be easily disintegrated into fibrous state.
  • pulp brown stock
  • the so-called brown stock discharged from the digester is washed and taken typically into a delignification stage, in which oxygen is usually used as the delignification chemical.
  • the delignification stage ends with washing.
  • the brown stock discharged from the digester or the oxygen-delignified pulp is typically screened at a screen room at a suitable process stage.
  • the aim of the pulp screening is to separate the material unwanted for further process and especially for the final product from the pulp. Screening is, however, an operation requiring the consistency of the pulp to be diluted to about 1-4%, depending to some extent on the apparatus to be used.
  • the pulp is typically fed to the screening from a blow tank of the digester plant or a tank following the oxygen delignification reactor where the consistency of the pulp is at medium consistency of 8-14 %.
  • a dilution system is arranged in the tank for pumping the necessary amount of dilution liquid.
  • the pulp is fed into the tank through the top thereof, and the pulp is discharged directly adjacent the dilution mixer located at the bottom of the tank.
  • the pulp is quickly mixed with the dilution liquid introduced preferably through the mixer so that pulp at a relatively even consistency can be pumped from the tank into the subsequent process stage, the screening apparatus.
  • the screen room consists of different types of screening devices, such as knot separation devices, screens, knot washers, etc.
  • the screen room can be located either after a digester or after an oxygen delignification stage or in another location in a pulp mill where an increase in purity of the pulp is required.
  • typically a screen room is fed from a tank or tower in which there is a low consistency zone having a volume of several tens of cubic meters. To homogenize the low consistency volume tank agitators and reasonable amount of dilution water are used.
  • the bottom portion In the smallest tanks or towers having a diameter of about 3.5 to 7.0 m, the bottom portion may be either straight cylindrical or first somewhat narrowing and below that cylindrical. In bigger towers having a diameter typically larger than 5.0 m, a so-called bottom pillar may be disposed at the center of the tower bottom. The purpose of the bottom pillar is to uphold pulp above the bottom portion and to divide the bottom portion into an annular mixing zone.
  • the shape of the prior art bottom pillars may be either an evenly converging cone ( Fig. 1 ), cylindrical pillar or a cylindrical pillar, the upper end whereof is arranged with an upwardly converging cone.
  • Fig. 1 illustrates a known high consistency pulp tower 10 ( Fig. 2a of US Patent 5,711,600 ) having a tower wall 12, a bottom portion 20, a tower bottom 22, a bottom pillar 30, mixers 40, conduits 50 for feeding dilution liquid, and discharge means 60 for diluted pulp..
  • Fig. 2a of US Patent 5,711,600
  • the bottom portion 20 and the upper part of the tower 10 have a conical wall section 14 between them.
  • Mixers 40 are arranged at about 1.1 m height from the tower bottom and so that the dilution liquid is fed through conduits 50 to the dilution zone of the bottom portion, to a level which is a little higher than the mixer shafts.
  • the mixers are disposed in the bottom portion of the tower so that they cause the pulp to be diluted to circulate fast around the bottom pillar.
  • US Patent 7,622,018 describes a similar arrangement in which the dilution is further improved so that at least a part of the dilution liquid required to dilute the pulp into the tower outlet consistency is introduced between the tower wall and the pillar (or another parting member) at the area substantially at the level of the smallest cross-section of the tower ( Fig. 2 ).
  • the dilution liquid is introduced in at least two portions in the dilution part of the tower.
  • FIG. 2 shows an improved prior art high-consistency pulp tower 10 in accordance with U.S. Pat. No 7,622,018 .
  • the bottom part 20 of the tower 10 is provided with a stationary bottom pillar 30.
  • the upper end of the pillar 30 has been shaped so that the diameter of an also stationary parting member 31 disposed therein is at least in one point larger than the diameter of the lower part of the pillar 30.
  • the cross-sectional area between the parting member 31 and the wall 12 of the tower 10 is smaller than in the bottom area of the pillar 30 below the parting member.
  • the parting member 31 has an upper section 34, the diameter of which converges conically upwards.
  • baffles 36 have been provided with an annular duct 46 located between the bottom pillar 30 and the tower wall 12, said duct 46 being provided with nozzles 48 for introducing dilution liquid into the high-consistency fiber suspension substantially simultaneously with the discharge of the pulp down to the dilution zone.
  • the bottom part of the tower contains several diluting agitators 40. The pulp is discharged through a conduit 60.
  • a screen room feed tank can have a total height of 6-30 meters and a diameter of 2 - 10 m, sometimes the upper part of a screen room feed tank is bigger than the bottom part, for example if more retention time is required because of process demands.
  • the low consistency mixing zone in the tank may be 3-6 meters in diameter and 2-6 meters in height.
  • the mixing zone in a tank or tower can be 6-10 meters in diameter and 3-10 meters in height.
  • special tank agitators are used. Typically a tank agitator operates within a consistency range of 2-5% consistency, but the performance of an agitator becomes poor if the consistency is about 4.5-6% or more.
  • the retention time of pulp in the low consistency mixing zone is typically 2-5 minutes, but in any case less than 10 minutes.
  • Tank agitators move diluted stock in the tank in such a way that consistency variations become more even and the stock consistency variation from a tank is small enough so that the screen room can handle the flow.
  • 1--4 tank agitators are required to provide adequately good mixing performance.
  • the number of tank agitators used in mixing depends on the production rate, but also on the volume of the mixing zone.
  • EP 0 965 682 A1 discloses an arrangement for treating pulp and a related method according to the preamble of claims 1 and 9, respectively.
  • An object of the new innovation is to eliminate the above mentioned problems and provide a screen room feed tank arrangement, which is more energy-efficient, space-saving and in which the consistency of the pulp to be fed to screening is even so that harmful consistency peaks may be avoided.
  • a novel screen room feed tower for pulp the mixing volume is reduced, and therefore traditional tank agitators are not required.
  • the dilution liquid water or filtrate
  • the dilution liquid is fed to the upper section of the bottom part of the tower.
  • a discharge pump the pulp is treated in a homogenizing zone where a rotating and a static homogenizer are installed.
  • the purpose of the homogenization zone is to mix the fiber suspension so that the consistency differences in the pulp suspension are equalized and dilution liquid is distributed evenly into the pulp suspension, i.e. the consistency of the pulp is homogenized.
  • a normal process pump conventional centrifugal pump
  • a pulp tower (or tank) according to the embodiments of the present invention comprises an upper part to which the pulp is fed, and a bottom part which is divided into a dilution zone, homogenizing zone and discharge (pumping) zone.
  • the upper part of the tower may act as a blow tank or storage (retention) tank, the size of which depends on the needs of the process, if any buffering effect is required.
  • the cross-section of the tower is typically round.
  • the diameter of the upper part is bigger than the diameter of the bottom part of the tower. The difference between the upper and bottom part depends on process requirements, such as retention time for storing pulp in the upper part of the tower.
  • a device for feeding dilution liquid to the pulp flowing downwards in the tower is located substantially at a level which divides the tower to the upper part and the bottom part and a discharge device for diluted pulp is arranged in the bottom part of the tower.
  • a device for homogenizing the consistency of the diluted pulp flow is arranged at a distance downstream of the dilution device in the pulp flow direction and upstream of the discharge device. The majority of the dilution liquid is added in the uppermost section of the bottom part of the tower. Smaller parts of the dilution liquid may be added between the uppermost dilution point and the homogenizing zone.
  • the dilution device defines a dilution point in the bottom part of the tower having a diameter.
  • the distance between the dilution device and the homogenizing device is 1.5-10 times the diameter of the tower at the dilution point, where the majority of the dilution liquid is added. Thus said distance is between the first dilution point and the homogenizing device.
  • the distance between a dilution point and a homogenization point is determined by the required retention time but also by the maintenance demands of a homogenizer.
  • the retention time between the dilution point and homogenizer should be so long that non-diluted pulp does not enter the screen room feed pump.
  • the retention time as short as 5-10 seconds should be sufficient, but in practical applications the retention time is typically 15-120 seconds, but preferably 20-60 seconds.
  • dilution liquid can be fed by using normal pipe connections.
  • the dilution is divided to a required number of connections around the mixing tank.
  • the dilution device comprises a number of feed nozzles/outlets arranged in the periphery of the tower wall.
  • the dilution liquid is fed from a supply tank and directed inwards, towards the centre of the tower.
  • the pressure is such that the dilution liquid is sprayed into the tower towards the downwards flowing pulp.
  • the pressure control, the shape of the outlet and the quantity of outlets may vary in a number of different ways, which are evident to the skilled person. The object is, however, to yield maximal penetration into the pulp flow.
  • the dilution liquid can also be fed via a feed pipe that is piped so that it goes through the dilution point.
  • the dilution liquid is led through several holes into the pulp so that dilution liquid flows into the pulp flow that is flowing downwards.
  • the dilution device comprises at least one pipe extending from the wall of the pulp tower inwards, towards the center of the tower, which pipe is provided with a number of outlet holes for the addition of the dilution liquid.
  • the homogenization volume (i.e. the size of the homogenization zone) is small, normally from 0.1m 3 (100 liters) up to 3 m 3 , when a traditional mixing tank volume is within a range of 10-300 m 3 .
  • the retention time in the homogenization zone of the new arrangement is typically only 2-10 seconds, when in traditional mixing tanks the retention time is typically several minutes.
  • a homogenizer having a rotating member(s) that generates turbulence in the homogenization zone makes the stock dilution liquid suspension flow even and makes the consistency fluctuations smaller.
  • a rotating homogenizer typically comprises a shaft which is mounted in the wall of the tower and which is provided extensions which mix the pulp flow when rotating. Lower power consumption can be achieved because of smaller volume in mixing and because of low rotation speed.
  • a homogenizer can operate within a rotation speed range of 600-1200 rpm.
  • a circumferential speed of the homogenizer is 5-20 meters per second, typically 10-15 meters per second.
  • the required amount of turbulence is also generated by using static constructions in the homogenization zone.
  • the homogenizer is a device or construction in the tower that provides a treatment which evens the flow of the pulp and dilution liquid that flows through the bottom part of the tower.
  • the static homogenizer by throttling the flow, i.e. decreasing the cross-sectional area, an increase in the flow rate and a higher turbulence are achieved, whereby the introduced dilution liquid will mix into the flowing pulp.
  • the static homogenizers preferably consist of protrusions, or annular flange or ring arranged on the inner wall of the tank.
  • Static homogenizers may be provided with, in addition to the throttling, turbulence-raising devices, such as baffles, ribs, pins, nubs or the like, arranged in the homogenization zone.
  • turbulence-raising devices such as baffles, ribs, pins, nubs or the like, arranged in the homogenization zone.
  • the used design of rotating and static homogenizers depends on the required quality of mixing that can be estimated by consistency variations after the screen room feed pump and total energy used in the application.
  • the inventive arrangement further comprises a construction for at least one flow guidance element, such as a cylindrical pipe, rectangle bar or beam, which is located after the dilution point but above the homogenizer to guide the diluted pulp flow to the homogenization zone.
  • a pipe or bar can be installed so that it is typically located horizontally across the tower. It is fixed at both ends to a wall of the tower. The distance and the location of the guidance element from the homogenizer should be determined so that the flow to the homogenization zone is even and the pulp can flow freely downwards but the flow is guided to the location that gives the best homogenization result.
  • a normal process pump that can pump pulp at a 3-8 % consistency can be used for discharging the pulp through an outlet from the bottom of the tower to the screen.
  • the feed consistency of pulp is typically 8-14 % in the upper part of the tower.
  • the bottom part of the tower of the invented arrangement and method is devoid of agitators which mix and dilute the pulp.
  • the dilution liquid which is needed to obtain a discharging (pumping) consistency is introduced into the pulp before the homogenizing device.
  • the stability of screening consistency is a requirement which has to be taken into account in traditional screen room applications, but also in the invented system.
  • a screen feed tank can generate unexpected consistency peaks, making the screen room operation difficult because of too high screening consistency.
  • the screen feed tank mixing (homogenizing) volume is essentially smaller compared to traditional systems. Because of short retention times a faster response from the consistency control would be needed.
  • the screen room consistency control is carried out using a consistency meter that controls dilution flows into the screen room feed tank and into the suction side of the screen room feed pump. This kind of consistency control allows consistency peaks to enter the screening where peaks can generate serious problems such as clogging of screens, pressure and flow fluctuations etc.
  • the outlet of the tower is connected to a conduit provided with a pump for conveying the diluted pulp from the tower to a screening device and with a feeder for adding dilution liquid to the pulp so as to control the pulp consistency, which feeder is located between the pump and screening device. Up to 5-10 % of the dilution liquid may be added to the discharged pulp.
  • Fig. 3 illustrates a screen room feed tower according to an embodiment of the present invention.
  • the tower 100 comprises a tower wall 102, an upper portion 104, a bottom portion 106 and a tower bottom 108.
  • the top of the tower may be provided with a device or conduit 110 for discharging gas.
  • the diameter of the upper portion 104 is larger than the diameter of the bottom portion 106.
  • the upper portion of the tower may act as a blow tank or a storage (retention) tank, the size of which depends on the needs of the process, if any buffering effect is required.
  • Pulp from a digester or an oxygen delignification reactor is fed to the tower through a conduit 112.
  • the bottom portion 106 is divided into a dilution zone 107 and homogenization zone 109, the latter being located after the dilution in the pulp flow direction.
  • conduits 114 are arranged for introducing dilution liquid to the pulp that flows downward in the tank.
  • homogenization zone which is located below the dilution zone, homogenization devices are arranged.
  • the purpose of the homogenization zone is to mix the pulp suspension so that its consistency is homogenized.
  • the pump 120 is connected adjacent the bottom or to the bottom. It pumps the diluted and homogenized pulp from a discharge zone 121 of the tower to a screen.
  • the rotating homogenizer 116 comprises a driving means 122, a shaft 124 equipped with blades or extensions 126. The blades are rotated so that the dilution liquid is distributed evenly into the pulp suspension.
  • This is only one preferred design of homogenizers. Also other designs which are able to homogenize the pulp consistency can be used.
  • a static homogenizer 118 which is a throttling in form of an annular flange or a ring. It further improves the turbulence in the pulp suspension and thus evens out possible consistency differences.
  • the dilution point 114 in the bottom part of the tower has a diameter D, wherein the distance C between the dilution device 114 and the homogenizing device 116 is 1.5-10 times the diameter D of the tower at the dilution point.
  • Fig. 4 shows, as an example not forming part of the present invention, a bottom portion of the tower 106, in which pulp flows (arrows) from the upper portion through the bottom portion and is discharged from the tank.
  • the tower is provided with a dilution device 128 which comprises openings 130 in the tower wall, through which openings dilution liquid is fed into the pulp flow.
  • the openings are located around the tower and are connected to a conduit or conduits for supplying liquid into the openings.
  • Two or more openings 130 are arranged at a distance from each other around the tank.
  • the homogenization is effected by protrusions arranged on the inner surface of the tank.
  • protrusions By throttling the flow, i.e. decreasing the cross-sectional area by the use of protrusions 132, an increase in the flow rate is achieved and due to the throttling a higher turbulence, whereby the introduced dilution liquid will further mix into the flowing pulp.
  • the protrusions extend in the vertical direction at a distance X so that the bottom portion of the tower has a reduced cross-section. After the protrusions the cross section of the bottom portion widens again.
  • FIG. 5 shows static homogenization cross section drawings.
  • Figure 5a is a cut view along section A-A of the embodiment of Figure 4 .
  • Fig. 5a shows the protrusions 132 arranged on the inner surface of the tank.
  • Fig. 5 b illustrates turbulence-raising devices, such as plates 134 or protrusions having different kinds of forms, such as rectangular, triangular.
  • Fig. 6 shows another embodiment for a dilution device 136.
  • the dilution liquid (arrow 140) can be fed via a feed pipe 138 that is piped so that it extends at least partly through the tower and thus through the dilution zone.
  • the dilution liquid is led through several holes 142 into the pulp so that dilution liquid flows into the pulp that is flowing downwards.
  • Fig. 7 illustrates a control system, which may be applied in connection with the embodiments of the present invention.
  • the consistency control is arranged so that a portion of the dilution liquid is fed also downstream from the consistency measurement point QIC close to the following screen 148.
  • the major portion of the dilution liquid is fed through line 144 to the bottom portion 106 of the tank, but some liquid (up to 5-10 %) may be introduced also through line 146 to an inlet of screen 148.
  • the feed line 150 is provided with consistency measurement QIC and dilution liquid conduit 146 for adjusting the feed consistency and maintaining it at a set value. If there are production disturbances, the steady consistency can be kept essentially at the set value by measuring the consistency and reacting quickly to a possible consistency increase by adding dilution liquid also through line 146.
  • Fig. 8 illustrates a screen room feed tower according to a further embodiment of the present invention.
  • the tower shown in Fig. 8 corresponds to the tower of Fig. 3 , but it is provided with two homogenizers 116 installed to the tower wall.
  • the tower further comprises a construction for at least one flow guidance element.
  • the figure also shows a cut view along cross-section B-B.
  • a cylindrical pipe 123 is disposed horizontally across the tower.
  • the pipe 123 is located after the dilution point 114 but above the homogenizers 116 to guide the diluted pulp flow to the homogenization zone 109.
  • the pipe 123 is installed so that it is fixed at both ends to the wall 102 of the tower.
  • the distance and the location of the pipe from the homogenizer 116 should be determined so that the flow to the homogenization zone is even and the pulp can flow freely downwards but the flow is guided to the location that gives the best homogenization result.
  • Fig. 9 illustrates a screen room feed tower according to a further example not forming part of the present invention.
  • a static homogenizer it may be preferable to use a vertical pillar or bar in the middle of the discharge (pumping) and homogenization zones.
  • the tower shown in Fig. 9 corresponds to the embodiment according to Fig. 4 , but a pillar 131 is disposed in the bottom part of the tower.
  • the pillar 131 has a lower end which is supported by the bottom 108 of the tower.
  • the pillar extends towards the dilution device 128 through the discharge (pumping) zone 121 and also through the homogenization zone 109 where static homogenizer elements 132 are fixed to the tower wall.
  • the pillar contributes to throttling.
  • the diameter of the pillar 131 is determined so that the homogenization is optimum.
  • the pillar itself may further comprise constructions, such as obstacles or other extensions (ribs, pins, nubs or the like), which raise the turbulence level and thus intensify the homogenization of the pulp flow.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Paper (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Description

    FIELD OF THE INVENTION
  • The present invention relates to a method and arrangement for treating pulp to be fed to a screen room at a pulp mill.
  • BACKGROUND OF THE INVENTION
  • In chemical wood processing the wood material is fed into a digester where wood chips are treated so that pulp (brown stock) is produced and subsequent to the digester the pulp is mainly in fibrous state or it can at least be easily disintegrated into fibrous state. The so-called brown stock discharged from the digester is washed and taken typically into a delignification stage, in which oxygen is usually used as the delignification chemical. The delignification stage ends with washing.
  • The brown stock discharged from the digester or the oxygen-delignified pulp is typically screened at a screen room at a suitable process stage. The aim of the pulp screening is to separate the material unwanted for further process and especially for the final product from the pulp. Screening is, however, an operation requiring the consistency of the pulp to be diluted to about 1-4%, depending to some extent on the apparatus to be used. The pulp is typically fed to the screening from a blow tank of the digester plant or a tank following the oxygen delignification reactor where the consistency of the pulp is at medium consistency of 8-14 %. In order to dilute the pulp from this discharge consistency to the consistency of a few percent required by the screening apparatus, a dilution system is arranged in the tank for pumping the necessary amount of dilution liquid. In most cases the pulp is fed into the tank through the top thereof, and the pulp is discharged directly adjacent the dilution mixer located at the bottom of the tank. The pulp is quickly mixed with the dilution liquid introduced preferably through the mixer so that pulp at a relatively even consistency can be pumped from the tank into the subsequent process stage, the screening apparatus.
  • The screen room consists of different types of screening devices, such as knot separation devices, screens, knot washers, etc. The screen room can be located either after a digester or after an oxygen delignification stage or in another location in a pulp mill where an increase in purity of the pulp is required. As mentioned above, typically a screen room is fed from a tank or tower in which there is a low consistency zone having a volume of several tens of cubic meters. To homogenize the low consistency volume tank agitators and reasonable amount of dilution water are used.
  • In the smallest tanks or towers having a diameter of about 3.5 to 7.0 m, the bottom portion may be either straight cylindrical or first somewhat narrowing and below that cylindrical. In bigger towers having a diameter typically larger than 5.0 m, a so-called bottom pillar may be disposed at the center of the tower bottom. The purpose of the bottom pillar is to uphold pulp above the bottom portion and to divide the bottom portion into an annular mixing zone. The shape of the prior art bottom pillars may be either an evenly converging cone (Fig. 1), cylindrical pillar or a cylindrical pillar, the upper end whereof is arranged with an upwardly converging cone. In all those towers which are provided with a bottom pillar, the dilution mixer/dilution mixers are disposed on the sides of the bottom pillar so that they direct the flow to circulate along the annular mixing zone. The bottom pillars are of solid construction and when disposed on the tower bottom they are merely supported by the tower bottom or the foundation therebelow, in any case by the very point which would also otherwise carry the weight of the pulp in the tower. Fig. 1 illustrates a known high consistency pulp tower 10 (Fig. 2a of US Patent 5,711,600 ) having a tower wall 12, a bottom portion 20, a tower bottom 22, a bottom pillar 30, mixers 40, conduits 50 for feeding dilution liquid, and discharge means 60 for diluted pulp.. In the arrangement of Fig. 1, the bottom portion 20 and the upper part of the tower 10, have a conical wall section 14 between them. Mixers 40 are arranged at about 1.1 m height from the tower bottom and so that the dilution liquid is fed through conduits 50 to the dilution zone of the bottom portion, to a level which is a little higher than the mixer shafts.
  • A problem with these constructions still is the unevenness of the pulp discharge consistency. In order to eliminate this problem US Patent 5,711,600 discloses a more developed design of a bottom pillar. According to this patent it is essential to the upper end of the pillar that the diameter of a parting member disposed therein is at least in one point larger than the diameter of the lower part of the pillar. In other words, it is a feature of the parting member that in the area of the parting member, the cross section between the parting member and the wall of the tower is smaller than in the bottom area of the pillar. This design still requires several mixers (the number of the mixers may range from two to six, mainly depending on the tower size), each mixer being connected with a feed conduit for dilution liquid. The mixers are disposed in the bottom portion of the tower so that they cause the pulp to be diluted to circulate fast around the bottom pillar. US Patent 7,622,018 describes a similar arrangement in which the dilution is further improved so that at least a part of the dilution liquid required to dilute the pulp into the tower outlet consistency is introduced between the tower wall and the pillar (or another parting member) at the area substantially at the level of the smallest cross-section of the tower (Fig. 2). Preferably the dilution liquid is introduced in at least two portions in the dilution part of the tower. One portion is introduced to the thick pulp suspension simultaneously as the suspension is taken from the storage part of the tower into the dilution zone, and another portion is introduced with the aid of the agitators positioned in the dilution zone. FIG. 2 shows an improved prior art high-consistency pulp tower 10 in accordance with U.S. Pat. No 7,622,018 . The bottom part 20 of the tower 10 is provided with a stationary bottom pillar 30. The upper end of the pillar 30 has been shaped so that the diameter of an also stationary parting member 31 disposed therein is at least in one point larger than the diameter of the lower part of the pillar 30. More broadly expressed, at the level of the parting member 31, the cross-sectional area between the parting member 31 and the wall 12 of the tower 10 is smaller than in the bottom area of the pillar 30 below the parting member. The parting member 31 has an upper section 34, the diameter of which converges conically upwards. In FIG. 2 baffles 36 have been provided with an annular duct 46 located between the bottom pillar 30 and the tower wall 12, said duct 46 being provided with nozzles 48 for introducing dilution liquid into the high-consistency fiber suspension substantially simultaneously with the discharge of the pulp down to the dilution zone. The bottom part of the tower contains several diluting agitators 40. The pulp is discharged through a conduit 60.
  • A screen room feed tank can have a total height of 6-30 meters and a diameter of 2 - 10 m, sometimes the upper part of a screen room feed tank is bigger than the bottom part, for example if more retention time is required because of process demands.
  • In a pulp mill having a production of 1000 admt/d the low consistency mixing zone in the tank may be 3-6 meters in diameter and 2-6 meters in height. In a 3000 admt/d pulp mill the mixing zone in a tank or tower can be 6-10 meters in diameter and 3-10 meters in height. To homogenize the diluted zone of the tank, special tank agitators are used. Typically a tank agitator operates within a consistency range of 2-5% consistency, but the performance of an agitator becomes poor if the consistency is about 4.5-6% or more.
  • In a traditional system the retention time of pulp in the low consistency mixing zone is typically 2-5 minutes, but in any case less than 10 minutes. Tank agitators move diluted stock in the tank in such a way that consistency variations become more even and the stock consistency variation from a tank is small enough so that the screen room can handle the flow. Typically 1--4 tank agitators are required to provide adequately good mixing performance. The number of tank agitators used in mixing depends on the production rate, but also on the volume of the mixing zone.
  • Although traditional screen room mixing tanks are widely used, they also may create problems, such as unexpected consistency variations. They also need a lot of equipment and instrumentation for agitators. Neither are the tanks very energy-efficient because of agitators. A further problem is also their high space requirements and construction costs.
  • EP 0 965 682 A1 discloses an arrangement for treating pulp and a related method according to the preamble of claims 1 and 9, respectively.
  • An object of the new innovation is to eliminate the above mentioned problems and provide a screen room feed tank arrangement, which is more energy-efficient, space-saving and in which the consistency of the pulp to be fed to screening is even so that harmful consistency peaks may be avoided.
  • SUMMARY OF THE INVENTION
  • The objects of the invention are fulfilled with an arrangement and a method according to the independent claims. Additionally, other preferred embodiments of the invention become known in the dependent claims.
  • In a novel screen room feed tower for pulp the mixing volume is reduced, and therefore traditional tank agitators are not required. The dilution liquid (water or filtrate) is fed to the upper section of the bottom part of the tower. Before the diluted pulp enters a discharge pump the pulp is treated in a homogenizing zone where a rotating and a static homogenizer are installed. The purpose of the homogenization zone is to mix the fiber suspension so that the consistency differences in the pulp suspension are equalized and dilution liquid is distributed evenly into the pulp suspension, i.e. the consistency of the pulp is homogenized. After the homogenization zone the pup consistency is even and a normal process pump (conventional centrifugal pump) may be used to pump the pulp into the screening.
  • A pulp tower (or tank) according to the embodiments of the present invention comprises an upper part to which the pulp is fed, and a bottom part which is divided into a dilution zone, homogenizing zone and discharge (pumping) zone. The upper part of the tower may act as a blow tank or storage (retention) tank, the size of which depends on the needs of the process, if any buffering effect is required. The cross-section of the tower is typically round. The diameter of the upper part is bigger than the diameter of the bottom part of the tower. The difference between the upper and bottom part depends on process requirements, such as retention time for storing pulp in the upper part of the tower.
  • A device for feeding dilution liquid to the pulp flowing downwards in the tower is located substantially at a level which divides the tower to the upper part and the bottom part and a discharge device for diluted pulp is arranged in the bottom part of the tower. A device for homogenizing the consistency of the diluted pulp flow is arranged at a distance downstream of the dilution device in the pulp flow direction and upstream of the discharge device. The majority of the dilution liquid is added in the uppermost section of the bottom part of the tower. Smaller parts of the dilution liquid may be added between the uppermost dilution point and the homogenizing zone.
  • The dilution device defines a dilution point in the bottom part of the tower having a diameter. According to an embodiment the distance between the dilution device and the homogenizing device is 1.5-10 times the diameter of the tower at the dilution point, where the majority of the dilution liquid is added. Thus said distance is between the first dilution point and the homogenizing device.
  • The distance between a dilution point and a homogenization point is determined by the required retention time but also by the maintenance demands of a homogenizer.
  • The retention time between the dilution point and homogenizer should be so long that non-diluted pulp does not enter the screen room feed pump. When taking into account different controlling systems and delays in the process, the retention time as short as 5-10 seconds should be sufficient, but in practical applications the retention time is typically 15-120 seconds, but preferably 20-60 seconds.
  • According to an embodiment dilution liquid can be fed by using normal pipe connections. The dilution is divided to a required number of connections around the mixing tank. The dilution device comprises a number of feed nozzles/outlets arranged in the periphery of the tower wall. The dilution liquid is fed from a supply tank and directed inwards, towards the centre of the tower. The pressure is such that the dilution liquid is sprayed into the tower towards the downwards flowing pulp. The pressure control, the shape of the outlet and the quantity of outlets may vary in a number of different ways, which are evident to the skilled person. The object is, however, to yield maximal penetration into the pulp flow.
  • According to another embodiment the dilution liquid can also be fed via a feed pipe that is piped so that it goes through the dilution point. In this kind of feed pipe the dilution liquid is led through several holes into the pulp so that dilution liquid flows into the pulp flow that is flowing downwards. The dilution device comprises at least one pipe extending from the wall of the pulp tower inwards, towards the center of the tower, which pipe is provided with a number of outlet holes for the addition of the dilution liquid. Depending on the dilution zone diameter and dilution rate, there can be a number of these kinds of dilution feed pipes through the dilution zone.
  • The homogenization volume (i.e. the size of the homogenization zone) is small, normally from 0.1m3 (100 liters) up to 3 m3, when a traditional mixing tank volume is within a range of 10-300 m3. The retention time in the homogenization zone of the new arrangement is typically only 2-10 seconds, when in traditional mixing tanks the retention time is typically several minutes.
  • A homogenizer having a rotating member(s) that generates turbulence in the homogenization zone makes the stock dilution liquid suspension flow even and makes the consistency fluctuations smaller.
  • When estimating the mixing of a traditional screen room feed tank, a volumetric space close to the rotating agitator blades presents only 0.5-3 % of the total mixing volume. When performing the same calculation for the novel tower and homogenization design the volumetric space of the rotating homogenizer blade presents 15-20 % of the total homogenization volume. This greater volumetric space results in a more homogenized pulp flow, whereby harmful consistency peaks can be avoided. Said smaller space in the traditional agitator tanks allows consistency peaks to more easily pass the mixing zone.
  • While the mixing volume is small, the energy input can be divided more evenly but also less mixing energy is needed to achieve a required mixing quality. When comparing traditional screen feed tank arrangement with tank agitators to the novel system where homogenizers are used the installed power can be reduced by 50-80 %, for example by 66 %. A rotating homogenizer typically comprises a shaft which is mounted in the wall of the tower and which is provided extensions which mix the pulp flow when rotating. Lower power consumption can be achieved because of smaller volume in mixing and because of low rotation speed. A homogenizer can operate within a rotation speed range of 600-1200 rpm. A circumferential speed of the homogenizer is 5-20 meters per second, typically 10-15 meters per second. With 5000 admt/d pulp line the installed power to the traditional tank agitators can be 490kW = 360kW, but with a homogenizer the installed power can be only 110kW.
  • The required amount of turbulence is also generated by using static constructions in the homogenization zone. The homogenizer is a device or construction in the tower that provides a treatment which evens the flow of the pulp and dilution liquid that flows through the bottom part of the tower.
  • In the static homogenizer, by throttling the flow, i.e. decreasing the cross-sectional area, an increase in the flow rate and a higher turbulence are achieved, whereby the introduced dilution liquid will mix into the flowing pulp. The static homogenizers preferably consist of protrusions, or annular flange or ring arranged on the inner wall of the tank.
  • Static homogenizers may be provided with, in addition to the throttling, turbulence-raising devices, such as baffles, ribs, pins, nubs or the like, arranged in the homogenization zone.
  • The used design of rotating and static homogenizers depends on the required quality of mixing that can be estimated by consistency variations after the screen room feed pump and total energy used in the application.
  • In a further embodiment of the inventive arrangement it further comprises a construction for at least one flow guidance element, such as a cylindrical pipe, rectangle bar or beam, which is located after the dilution point but above the homogenizer to guide the diluted pulp flow to the homogenization zone. A pipe or bar can be installed so that it is typically located horizontally across the tower. It is fixed at both ends to a wall of the tower. The distance and the location of the guidance element from the homogenizer should be determined so that the flow to the homogenization zone is even and the pulp can flow freely downwards but the flow is guided to the location that gives the best homogenization result.
  • After homogenization of the pulp flow a normal process pump that can pump pulp at a 3-8 % consistency can be used for discharging the pulp through an outlet from the bottom of the tower to the screen. Depending on the consistency and/or location of the screen room in a process, there may be a need to equip a screen room feed pump with gas removal. The feed consistency of pulp is typically 8-14 % in the upper part of the tower. The bottom part of the tower of the invented arrangement and method is devoid of agitators which mix and dilute the pulp. In the novel tower the dilution liquid which is needed to obtain a discharging (pumping) consistency is introduced into the pulp before the homogenizing device.
  • In screen room operation the stability of screening consistency is a requirement which has to be taken into account in traditional screen room applications, but also in the invented system. In a traditional system a screen feed tank can generate unexpected consistency peaks, making the screen room operation difficult because of too high screening consistency. In the invented system the screen feed tank mixing (homogenizing) volume is essentially smaller compared to traditional systems. Because of short retention times a faster response from the consistency control would be needed. Traditionally the screen room consistency control is carried out using a consistency meter that controls dilution flows into the screen room feed tank and into the suction side of the screen room feed pump. This kind of consistency control allows consistency peaks to enter the screening where peaks can generate serious problems such as clogging of screens, pressure and flow fluctuations etc.
  • If the consistency control is arranged so that some of the dilution liquid is fed also downstream from the consistency measurement point close to the following screen, problematic consistency peaks would be smaller and the screening consistency can be kept between the required values. According to an embodiment of the invented arrangement the outlet of the tower is connected to a conduit provided with a pump for conveying the diluted pulp from the tower to a screening device and with a feeder for adding dilution liquid to the pulp so as to control the pulp consistency, which feeder is located between the pump and screening device. Up to 5-10 % of the dilution liquid may be added to the discharged pulp.
  • BRIEF DESCRIPTION OF THE DRAWINGS
  • The inventive arrangement and method that have been developed are described in more detail with reference to the drawings, in which:
    • Fig. 1 illustrates the bottom part of a pulp tower in accordance of prior art;
    • Fig. 2 illustrates the bottom part of a pulp tower in accordance of prior art;
    • Fig. 3 illustrates a screen room feed tower according to an embodiment of the present invention;
    • Fig. 4 illustrates the bottom portion of a screen room feed tower according to an an example not forming part of the present invention;
    • Fig. 5 illustrates, as an example, a static homogenizer, which may be used in connection with the embodiments of the present invention. Figure 5 is a cut view along section A-A of the embodiment of Figure 4.
    • Fig. 6 illustrates a device for introducing dilution liquid,
    • Fig. 7 illustrates a control system, which may be applied in connection with the present invention,
    • Fig. 8 illustrates a screen room feed tower according to a further embodiment of the present invention, and
    • Fig. 9 illustrates a screen room feed tower according to an example not forming part of the present invention.
    DETAILED DESCRIPTION OF THE INVENTION
  • Fig. 3 illustrates a screen room feed tower according to an embodiment of the present invention. The tower 100 comprises a tower wall 102, an upper portion 104, a bottom portion 106 and a tower bottom 108. The top of the tower may be provided with a device or conduit 110 for discharging gas. In this embodiment the diameter of the upper portion 104 is larger than the diameter of the bottom portion 106. The upper portion of the tower may act as a blow tank or a storage (retention) tank, the size of which depends on the needs of the process, if any buffering effect is required. Pulp from a digester or an oxygen delignification reactor is fed to the tower through a conduit 112.
  • The bottom portion 106 is divided into a dilution zone 107 and homogenization zone 109, the latter being located after the dilution in the pulp flow direction. In the upper part of the bottom portion conduits 114 are arranged for introducing dilution liquid to the pulp that flows downward in the tank. In the homogenization zone, which is located below the dilution zone, homogenization devices are arranged. The purpose of the homogenization zone is to mix the pulp suspension so that its consistency is homogenized. In this embodiment, there are both rotating 116 and static 118 homogenizers. Connected to the tower through the wall thereof, is a pump 120. The pump 120 is connected adjacent the bottom or to the bottom. It pumps the diluted and homogenized pulp from a discharge zone 121 of the tower to a screen.
  • The rotating homogenizer 116 comprises a driving means 122, a shaft 124 equipped with blades or extensions 126. The blades are rotated so that the dilution liquid is distributed evenly into the pulp suspension. This is only one preferred design of homogenizers. Also other designs which are able to homogenize the pulp consistency can be used. A feature is that when homogenizers are used the installed power can be reduced by 50-80 %, for instance by 66%. Lower power consumption can be achieved because of smaller volume in mixing and because of low rotation speed. With 5000 admt/d pulp line the installed power to the traditional tank agitators would be 490kW = 360kW, but with a homogenizer the installed power would be only 110kW.
  • In the tower according to Figure 3 there is also a static homogenizer 118, which is a throttling in form of an annular flange or a ring. It further improves the turbulence in the pulp suspension and thus evens out possible consistency differences.
  • According to a preferred embodiment the dilution point 114 in the bottom part of the tower has a diameter D, wherein the distance C between the dilution device 114 and the homogenizing device 116 is 1.5-10 times the diameter D of the tower at the dilution point.
  • Fig. 4 shows, as an example not forming part of the present invention, a bottom portion of the tower 106, in which pulp flows (arrows) from the upper portion through the bottom portion and is discharged from the tank.
  • The tower is provided with a dilution device 128 which comprises openings 130 in the tower wall, through which openings dilution liquid is fed into the pulp flow. The openings are located around the tower and are connected to a conduit or conduits for supplying liquid into the openings. Two or more openings 130 are arranged at a distance from each other around the tank.
  • There is a homogenization zone 109 after the dilution point 107. The homogenization is effected by protrusions arranged on the inner surface of the tank. By throttling the flow, i.e. decreasing the cross-sectional area by the use of protrusions 132, an increase in the flow rate is achieved and due to the throttling a higher turbulence, whereby the introduced dilution liquid will further mix into the flowing pulp. The protrusions extend in the vertical direction at a distance X so that the bottom portion of the tower has a reduced cross-section. After the protrusions the cross section of the bottom portion widens again.
  • Fig. 5 shows static homogenization cross section drawings. Figure 5a is a cut view along section A-A of the embodiment of Figure 4. Fig. 5a shows the protrusions 132 arranged on the inner surface of the tank. Fig. 5 b illustrates turbulence-raising devices, such as plates 134 or protrusions having different kinds of forms, such as rectangular, triangular.
  • Fig. 6 shows another embodiment for a dilution device 136. The dilution liquid (arrow 140) can be fed via a feed pipe 138 that is piped so that it extends at least partly through the tower and thus through the dilution zone. In this kind of feed pipe the dilution liquid is led through several holes 142 into the pulp so that dilution liquid flows into the pulp that is flowing downwards.
  • Fig. 7 illustrates a control system, which may be applied in connection with the embodiments of the present invention. The consistency control is arranged so that a portion of the dilution liquid is fed also downstream from the consistency measurement point QIC close to the following screen 148. Thus, the screening consistency can be kept between the required values by using this fine adjustment. The major portion of the dilution liquid is fed through line 144 to the bottom portion 106 of the tank, but some liquid (up to 5-10 %) may be introduced also through line 146 to an inlet of screen 148. The feed line 150 is provided with consistency measurement QIC and dilution liquid conduit 146 for adjusting the feed consistency and maintaining it at a set value. If there are production disturbances, the steady consistency can be kept essentially at the set value by measuring the consistency and reacting quickly to a possible consistency increase by adding dilution liquid also through line 146.
  • Fig. 8 illustrates a screen room feed tower according to a further embodiment of the present invention. The tower shown in Fig. 8 corresponds to the tower of Fig. 3, but it is provided with two homogenizers 116 installed to the tower wall. In addition, the tower further comprises a construction for at least one flow guidance element. The figure also shows a cut view along cross-section B-B. In this embodiment a cylindrical pipe 123 is disposed horizontally across the tower. The pipe 123 is located after the dilution point 114 but above the homogenizers 116 to guide the diluted pulp flow to the homogenization zone 109. The pipe 123 is installed so that it is fixed at both ends to the wall 102 of the tower. The distance and the location of the pipe from the homogenizer 116 should be determined so that the flow to the homogenization zone is even and the pulp can flow freely downwards but the flow is guided to the location that gives the best homogenization result.
  • Fig. 9 illustrates a screen room feed tower according to a further example not forming part of the present invention. In case of a static homogenizer it may be preferable to use a vertical pillar or bar in the middle of the discharge (pumping) and homogenization zones. The tower shown in Fig. 9 corresponds to the embodiment according to Fig. 4, but a pillar 131 is disposed in the bottom part of the tower. The pillar 131 has a lower end which is supported by the bottom 108 of the tower. The pillar extends towards the dilution device 128 through the discharge (pumping) zone 121 and also through the homogenization zone 109 where static homogenizer elements 132 are fixed to the tower wall. The pillar contributes to throttling. The diameter of the pillar 131 is determined so that the homogenization is optimum. The pillar itself may further comprise constructions, such as obstacles or other extensions (ribs, pins, nubs or the like), which raise the turbulence level and thus intensify the homogenization of the pulp flow.
  • While the invention has been described in connection with what is presently considered to be the most practical and preferred embodiment, it is to be understood that the invention is not to be limited to the disclosed embodiment, but on the contrary, is intended to cover various modifications included within the scope of the appended claims.

Claims (11)

  1. An arrangement for treating pulp to be fed to a screening room of a pulp mill, which arrangement comprises:
    a tower (100) having an upstanding wall (102), and a bottom (108);
    a pulp inlet in an upper part (104) of the tower (100);
    a device (114, 136) for feeding dilution liquid into the pulp flowing downwards in the tower (100), said dilution device (114, 136) being located substantially at a level which divides the tower (100) into said upper part (104) and a bottom part (106), and
    a discharge device for diluted pulp arranged in the bottom part (106) of the tower (100),
    wherein a device for homogenizing the consistency of the diluted pulp flow is arranged at a distance downstream of the dilution device (114, 136) in the pulp flow direction and upstream of the discharge device, the homogenizing device comprising a rotating homogenizer (116) comprising a shaft (124) mounted in the wall (102) of the tower (100), the shaft (124) being equipped with at least one rotating member (126) that generates turbulence in the pulp suspension,
    characterized in that
    the homogenizing device comprises a static homogenizer (118) positioned downstream of the rotating homogenizer (116) in the pulp flow direction and comprising at least one throttling member configured for throttling the pulp flow to further improve the turbulence in the pulp suspension.
  2. An arrangement according to claim 1, in which the cross-section of the tower (100) is round, the dilution device (114, 136) defines a dilution point in the bottom part (106) of the tower (100), and the distance (C) between the dilution device (114, 136) and the rotating homogenizer (116) is 1.5-10 times a diameter (D) of the tower (100) at the dilution point.
  3. An arrangement according to claim 1 or 2, in which the at least one rotating member (126) is arranged to be rotatable at a circumferential speed of 5-20 meters per second.
  4. An arrangement according to any one of the preceding claims, in which the dilution device (114) comprises a number of feed nozzles or openings arranged in the periphery of the tower wall (102).
  5. An arrangement according to any one of the preceding claims, in which the dilution device (136) comprises at least one pipe (138) extending from the wall (102) of the pulp tower (100) inwards, towards the centre of tower (100), which pipe is provided with a number of outlet holes (142) for the addition of the dilution liquid.
  6. An arrangement according to any one of the preceding claims, in which the discharge device comprises an outlet for the diluted and homogenized pulp in the bottom part (106) of the tower (100).
  7. An arrangement according to claim 6, in which the outlet is connected to a conduit provided with a pump (120) for conveying the pulp from the tower (100) to a screening device and with a feeder for adding dilution liquid into the pulp so as to control the pulp consistency, which feeder is located between the pump (120) and the screening device.
  8. An arrangement according to any one of the preceding claims, in which a flow guidance element (123) is arranged between the dilution device (114, 136) and the homogenizing device.
  9. A method for treating pulp to be fed to a screening room of a pulp mill, in which method
    - pulp having a consistency of 8-14 % is fed to a tower (100) having an inlet in an upper part (104) of the tower (100) ;
    - the pulp flows from the upper part (104) of the tower (100) to a bottom part (106) thereof,
    - dilution liquid is introduced into the pulp in the bottom part (106) of the tower (100), and
    - the pulp having a decreased consistency is discharged from the bottom of the tower (100),
    wherein the pulp and the dilution liquid is treated by a homogenizing device in a homogenizing zone (109) for equalizing the consistency of the pulp flow and producing the pulp having the decreased consistency, which homogenizing zone (109) is located between the dilution zone (107) and discharge zone (121),
    wherein the homogenizing of the pulp in the homogenizing zone (109) is effected by generating turbulence in the pulp suspension by means of a rotating homogenizer (116) comprising a shaft (124) mounted in the wall (102) of the tower (100), the shaft (124) being equipped with at least one rotating member (126),
    characterized in that
    the turbulence in the pulp suspension is further improved by throttling the pulp flow by means of a static homogenizer (118) positioned in the homogenizing zone (109) downstream of the rotating homogenizer(116)in the pulp flow direction.
  10. A method according to claim 9, in which the pulp is discharged from the tower (100) and pumped to a screening device, wherein a portion of the dilution liquid is added upstream of the screening device for controlling the consistency of the discharged pulp.
  11. A method according to claim 10, further comprising the step of introducing up to 10 % of the dilution liquid to the discharged pulp.
EP11779190.5A 2010-10-13 2011-10-12 Method and arrangement for treating pulp Active EP2627818B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US39265510P 2010-10-13 2010-10-13
PCT/FI2011/050881 WO2012049367A1 (en) 2010-10-13 2011-10-12 Method and arrangement for treating pulp

Publications (2)

Publication Number Publication Date
EP2627818A1 EP2627818A1 (en) 2013-08-21
EP2627818B1 true EP2627818B1 (en) 2021-01-06

Family

ID=44907886

Family Applications (1)

Application Number Title Priority Date Filing Date
EP11779190.5A Active EP2627818B1 (en) 2010-10-13 2011-10-12 Method and arrangement for treating pulp

Country Status (8)

Country Link
EP (1) EP2627818B1 (en)
JP (1) JP5911873B2 (en)
CN (1) CN103154361B (en)
BR (1) BR112013009075B1 (en)
ES (1) ES2860750T3 (en)
PT (1) PT2627818T (en)
RU (1) RU2584519C2 (en)
WO (1) WO2012049367A1 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9333468B2 (en) 2012-09-24 2016-05-10 Abengoa Bioenergy New Technologies, Llc Soak vessels and methods for impregnating biomass with liquid
RU2650066C2 (en) 2013-01-04 2018-04-06 Зульцер Мэнэджмент Аг Method and device for transferring process liquid, industrial facility and method of simplifying layout of such
SE1650410A1 (en) * 2016-03-30 2017-10-01 Valmet Oy Screen feed arrangement
CN113308923B (en) * 2021-05-28 2022-06-10 北京三联虹普新合纤技术服务股份有限公司 Pulp homogenizing and conditioning system for preparing Lyocell fibers
CN113388897B (en) * 2021-06-29 2022-06-10 北京三联虹普新合纤技术服务股份有限公司 High-capacity Lyocell cellulose stock solution and continuous preparation process thereof

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SU1724767A1 (en) * 1988-09-12 1992-04-07 Центральный Научно-Исследовательский И Проектно-Конструкторский Институт По Проектированию Оборудования Для Целлюлозно-Бумажной Промышленности Tower for bleaching cellulose
DE4141865A1 (en) * 1991-12-18 1993-06-24 Rolf Kettler Paper machine mfg. appts. - is a vertical cylinder container with vertical stirring shaft moved forwards and back by a motor
FI98836C (en) * 1994-06-09 1997-08-25 Ahlstroem Pumput Oy Consistency pulp tower
DE19826879B4 (en) * 1998-06-17 2005-06-02 Voith Paper Patent Gmbh Method and container for stacking high consistency paper pulp
FI20030209A7 (en) * 2003-02-12 2004-08-13 Sulzer Pumpen Ag Arrangement and method for processing pulp and method for modernizing a pulp tower
FI20031045A0 (en) * 2003-07-09 2003-07-09 Sulzer Pumpen Ag Process and apparatus for treating pulp
FI20031164L (en) * 2003-07-09 2005-01-10 Sulzer Pumpen Ag Method and apparatus for processing pulp
DE102006008763B3 (en) * 2006-02-24 2007-12-06 Voith Patent Gmbh Reaction tower for bleaching of fiber materials, comprises cylindrical reaction container, dilution container, and a cylindrical homogenizing container, which has an inlet and outlet for the product to be bleached
WO2009037091A1 (en) * 2007-09-17 2009-03-26 Sulzer Pumpen Ag An apparatus for discharging pulp from a vessel, method of discharging pulp form a vessel and method of upgrading a pulp vessel

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
None *

Also Published As

Publication number Publication date
CN103154361B (en) 2015-09-09
WO2012049367A1 (en) 2012-04-19
JP2013539825A (en) 2013-10-28
JP5911873B2 (en) 2016-04-27
BR112013009075A2 (en) 2016-07-19
CN103154361A (en) 2013-06-12
ES2860750T3 (en) 2021-10-05
PT2627818T (en) 2021-04-07
BR112013009075B1 (en) 2021-01-26
EP2627818A1 (en) 2013-08-21
RU2013121675A (en) 2014-11-20
RU2584519C2 (en) 2016-05-20

Similar Documents

Publication Publication Date Title
EP2627818B1 (en) Method and arrangement for treating pulp
JP4871724B2 (en) Method and apparatus for supplying chemicals to a liquid stream
EP0344238B1 (en) A reactor for mixing liquids together
US5791778A (en) Method and apparatus for mixing gaseous chemical to fiber suspension
US5240327A (en) Method for creating double loop flow
US9708762B2 (en) Method of and an arrangement for transferring a process liquid, an industrial facility and a method of simplifying the layout of such
EP2193233B1 (en) An apparatus for discharging pulp from a vessel, method of discharging pulp form a vessel and method of upgrading a pulp vessel
EP1592838B1 (en) An arrangement for and a method of treating pulp, and a method of modernizing a pulp tower
EP0912796B1 (en) Method and apparatus for filling a pulp tower
WO2014184443A1 (en) A system and method to regulate consistency in a blow or pulp tank
US3138947A (en) Device for continuous bleaching of cellulose
US8444823B2 (en) Method and apparatus for paper stock mixing
WO2009053530A1 (en) A pulp container and a method for discharging pulp from a pulp container
US5772844A (en) Process distributing fluffed pulp into a static bed reactor for gaseous treatment
CN105637144A (en) A method of and an arrangement for introducing process liquid from a treatment step to a washing and/or filtering apparatus

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

17P Request for examination filed

Effective date: 20130418

AK Designated contracting states

Kind code of ref document: A1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

DAX Request for extension of the european patent (deleted)
STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: EXAMINATION IS IN PROGRESS

17Q First examination report despatched

Effective date: 20170804

GRAP Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOSNIGR1

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: GRANT OF PATENT IS INTENDED

INTG Intention to grant announced

Effective date: 20200730

GRAS Grant fee paid

Free format text: ORIGINAL CODE: EPIDOSNIGR3

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: THE PATENT HAS BEEN GRANTED

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AL AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HR HU IE IS IT LI LT LU LV MC MK MT NL NO PL PT RO RS SE SI SK SM TR

REG Reference to a national code

Ref country code: GB

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: AT

Ref legal event code: REF

Ref document number: 1352489

Country of ref document: AT

Kind code of ref document: T

Effective date: 20210115

Ref country code: CH

Ref legal event code: EP

REG Reference to a national code

Ref country code: DE

Ref legal event code: R096

Ref document number: 602011069890

Country of ref document: DE

REG Reference to a national code

Ref country code: IE

Ref legal event code: FG4D

REG Reference to a national code

Ref country code: SE

Ref legal event code: TRGR

REG Reference to a national code

Ref country code: FI

Ref legal event code: FGE

REG Reference to a national code

Ref country code: PT

Ref legal event code: SC4A

Ref document number: 2627818

Country of ref document: PT

Date of ref document: 20210407

Kind code of ref document: T

Free format text: AVAILABILITY OF NATIONAL TRANSLATION

Effective date: 20210331

REG Reference to a national code

Ref country code: NL

Ref legal event code: MP

Effective date: 20210106

REG Reference to a national code

Ref country code: LT

Ref legal event code: MG9D

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: BG

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210406

Ref country code: NL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: NO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210406

Ref country code: LT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: GR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210407

Ref country code: HR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: RS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: PL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: LV

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210506

REG Reference to a national code

Ref country code: DE

Ref legal event code: R097

Ref document number: 602011069890

Country of ref document: DE

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SM

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: CZ

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: EE

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: DK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

Ref country code: RO

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

26N No opposition filed

Effective date: 20211007

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: AL

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SI

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IS

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210506

REG Reference to a national code

Ref country code: BE

Ref legal event code: MM

Effective date: 20211031

GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20211012

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MC

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LU

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20211012

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20211012

Ref country code: BE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20211031

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20211031

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20211031

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20211012

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: HU

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT; INVALID AB INITIO

Effective date: 20111012

Ref country code: CY

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

P01 Opt-out of the competence of the unified patent court (upc) registered

Effective date: 20230510

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MK

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: TR

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: MT

Free format text: LAPSE BECAUSE OF FAILURE TO SUBMIT A TRANSLATION OF THE DESCRIPTION OR TO PAY THE FEE WITHIN THE PRESCRIBED TIME-LIMIT

Effective date: 20210106

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: DE

Payment date: 20241021

Year of fee payment: 14

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FI

Payment date: 20241025

Year of fee payment: 14

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: AT

Payment date: 20241022

Year of fee payment: 14

Ref country code: FR

Payment date: 20241021

Year of fee payment: 14

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: ES

Payment date: 20241127

Year of fee payment: 14

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: SE

Payment date: 20241021

Year of fee payment: 14

REG Reference to a national code

Ref country code: AT

Ref legal event code: UEP

Ref document number: 1352489

Country of ref document: AT

Kind code of ref document: T

Effective date: 20210106

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: PT

Payment date: 20251002

Year of fee payment: 15