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EP1648236A1 - Preparation de poudre recouverte - Google Patents

Preparation de poudre recouverte

Info

Publication number
EP1648236A1
EP1648236A1 EP03818178A EP03818178A EP1648236A1 EP 1648236 A1 EP1648236 A1 EP 1648236A1 EP 03818178 A EP03818178 A EP 03818178A EP 03818178 A EP03818178 A EP 03818178A EP 1648236 A1 EP1648236 A1 EP 1648236A1
Authority
EP
European Patent Office
Prior art keywords
lecithin
powder
oil
alkali metals
ratio
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP03818178A
Other languages
German (de)
English (en)
Other versions
EP1648236A4 (fr
Inventor
John Van De Sype
Ravindra L. Arudi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Cargill Inc
Original Assignee
Cargill Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cargill Inc filed Critical Cargill Inc
Publication of EP1648236A1 publication Critical patent/EP1648236A1/fr
Publication of EP1648236A4 publication Critical patent/EP1648236A4/fr
Withdrawn legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A21—BAKING; EDIBLE DOUGHS
    • A21D—TREATMENT OF FLOUR OR DOUGH FOR BAKING, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS
    • A21D10/00—Batters, dough or mixtures before baking
    • A21D10/002—Dough mixes; Baking or bread improvers; Premixes
    • A21D10/005—Solid, dry or compact materials; Granules; Powders
    • A—HUMAN NECESSITIES
    • A21—BAKING; EDIBLE DOUGHS
    • A21D—TREATMENT OF FLOUR OR DOUGH FOR BAKING, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS
    • A21D2/00—Treatment of flour or dough by adding materials thereto before or during baking
    • A21D2/08—Treatment of flour or dough by adding materials thereto before or during baking by adding organic substances
    • A21D2/30—Organic phosphorus compounds
    • A21D2/32—Phosphatides
    • A—HUMAN NECESSITIES
    • A21—BAKING; EDIBLE DOUGHS
    • A21D—TREATMENT OF FLOUR OR DOUGH FOR BAKING, e.g. BY ADDITION OF MATERIALS; BAKING; BAKERY PRODUCTS
    • A21D6/00—Other treatment of flour or dough before baking, e.g. cooling, irradiating or heating
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING OR TREATMENT THEREOF
    • A23C9/00—Milk preparations; Milk powder or milk powder preparations
    • A23C9/16—Agglomerating or granulating milk powder; Making instant milk powder; Products obtained thereby
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS OR COOKING OILS
    • A23D9/00—Other edible oils or fats, e.g. shortenings or cooking oils
    • A23D9/02—Other edible oils or fats, e.g. shortenings or cooking oils characterised by the production or working-up
    • A23D9/04—Working-up
    • A23D9/05—Forming free-flowing pieces
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G1/00—Cocoa; Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/30—Cocoa products, e.g. chocolate; Substitutes therefor
    • A23G1/56—Liquid products; Solid products in the form of powders, flakes or granules for making liquid products, e.g. for making chocolate milk, drinks and the products for their preparation, pastes for spreading or milk crumb
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J3/00—Working-up of proteins for foodstuffs
    • A23J3/14—Vegetable proteins
    • A23J3/16—Vegetable proteins from soybean
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J7/00—Phosphatide compositions for foodstuffs, e.g. lecithin
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
    • A23L29/10—Foods or foodstuffs containing additives; Preparation or treatment thereof containing emulsifiers
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/30—Encapsulation of particles, e.g. foodstuff additives
    • A23P10/35—Encapsulation of particles, e.g. foodstuff additives with oils, lipids, monoglycerides or diglycerides
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00—Shaping or working of foodstuffs characterised by the products
    • A23P10/40—Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added
    • A23P10/47—Shaping or working of foodstuffs characterised by the products free-flowing powder or instant powder, i.e. powder which is reconstituted rapidly when liquid is added using additives, e.g. emulsifiers, wetting agents or dust-binding agents
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P20/00—Coating of foodstuffs; Coatings therefor; Making laminated, multi-layered, stuffed or hollow foodstuffs
    • A23P20/10—Coating with edible coatings, e.g. with oils or fats
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
    • A23G2220/00—Products with special structure
    • A23G2220/20—Products with special structure with a composite structure, e.g. laminated products, coated products, microstructures, e.g. with encapsulated ingredients
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs

Definitions

  • the present invention relates to the production of powders coated with a specific lecithin, such that the coated particles have good wettability and dispersibility.
  • the lecithin products that are used in coating the powders in a first embodiment, are membrane, separated lecithins having a ratio of alkali metals to alkaline earthmetals ranging from greater than 0 to about 10 and preferably greater than 0 to about 5.
  • the lecithin products used in the present invention are described as lecithins having a ratio of alkali metals to alkaline earthmetals ranging from about 1.6 to about 3.0, preferably about 1.8 to about 2.8.
  • the present invention relates to the production of powders coated with a specific lecithin, such that the coated particles have good wettability and dispersibility.
  • the lecithin products that are used in coating the powders in a first embodiment, are membrane, separated lecithins having a ratio of alkali metals to alkaline earthmetals ranging from greater than 0 to about 10 and preferably greater than 0 to about 5.
  • the lecithin products used in the present invention are described as lecithins having a ratio of alkali metals to alkaline earthmetals ranging from about 1.6 to about 3.0, preferably about 1.8 to about 2.8.
  • any particle may be used.
  • Exemplary of the particles that are suitable for use in the present process are the following: Cocoa powder Soy isolate Flour Instant breakfast beverage Soups Ice tea Jell-O Processing aid for gums dispersal Insoluble fiber Infant formulas Thickeners Snack food coating High intensity sweeteners Beta Glucan Steryl Esters Sauces Gravy Sodium Casemate Milk Powders PreBlends (Powder gravies, salad dressings, mixes, high protein powders) Nutritional Powders Powders in oils Fats into oils Salad dressings Pharmaceutical applications Food Colors cheese Powder Spice Blends Marinades Yeast Flavor Emulsions Enterals Dessert mixes Cake mixes Muffin mixes Bullion cubes Leavening agents Powdered Eggs Sucrose Aspartame Powdered laundry detergent Pancake mixes Chemical sprays (Fruit trees) Fertilizers Drugs Fire extinguisher Colloidal Suspension Beauty products Hair dyes Inks Custard Finger Paints Easter egg dyes Pudding/healthy/chocolate Seed Alcohol
  • the powders are coated in any suitable manner with a specified lecithin product, in the form of an oil-containing lecithin, or a lecithin with oil, or a water- containing lecithin or a lecithin with aqueous phase such as water.
  • the lecithin products used in the present invention may be prepared by any suitable manner.
  • a vegetable oil miscella may be passed through a membrane, preferably polymeric or semi-permeable, to obtain a retentate and a permeate.
  • the lecithin products are in the retentate. Exemplary of such methods are those appearing in U.S. patent No. 6,207,209 to Jirjis, et ab; U.S. Patent Nos.
  • Example A Two samples of miscella were prepared by using the present technique. Miscella samples were obtained from two different oil seeds plants. A membrane was conditioned and used for removing phospholipids from each of the two samples of miscella. The membrane purchased was a PAN membrane from Osmonics, Inc. The membrane can be characterized as having an average pore size of 0.3 micron, and in the form of a spiral wound 25 inch x 40 inch membrane element. The membrane was conditioned by soaking the membrane in an intermediate solvent (propanol) for 24 hours.
  • an intermediate solvent propanol
  • Spiral wound 8 inch x 40 inch QX membranes were purchased from Osmonics, Inc.
  • the membranes were conditioned and used for removing phospholipids by soaking them in an intermediate solvent (100% isopropanol) for 12 hours.
  • the intermediate solvent was recirculated at a flow rate of 15 m 3 /hour per element and forced through the membrane pores for about 15 minutes using a pump (this recirculation or forcing through is referred to as "forced Permeation" for purposes of the Example B).
  • the resulting membrane was soaked in a 50:50 mixture of intermediate solvent (100% isopropanol) and extraction solvent (100% commercial hexane) for 12 hours.
  • This retentate stream was desolventized at a rate of 1800 kg/hour, 95°C and 260 mm Hg absolute pressure. The resulting concentration of hexane was 5%.
  • the retentate stream was further desolventized at a temperature of 110° at an absolute pressure of 20 mm Hg and sparge stream of 80kg/hour by using a stripper to product 600 kg/hour of lecithin product with less than 5 ppm of hexane.
  • the following test procedure is used.
  • Elemental analysis was performed by Inductively Coupled Plasma-Emission Spectroscopy (ICP-ES) with target elements of aluminum, calcium, chromium, iron, lead, magnesium, nickel, potassium, phosphorus, silicon, sodium, and zinc. This analysis was performed according to the American Oil Chemists' Society (AOCS) Official Method Ca 20- 99. Each sample was weighed on an analytical balance to the nearest 0.0001 g. Because of the range of concentration, two dilution levels are required. Approximately 0.8 g of sample was weighted out and recorded. To the sample approximately 4.2 g of kerosene was weighed and recorded. The sample/kerosene mixture was vortexed until the sample is completely dissolved.
  • ICP-ES Inductively Coupled Plasma-Emission Spectroscopy
  • the ICP data is reported typically as ppm calcium, magnesium, potassium, sodium and phosphorous, along with other metals.
  • the ppm values are divided by the atomic weight of the respective element (Ca:40, K:39, P:31 and Mg:24) and the atomic equivalents are used to calculate the ratio of monovalent to divalent (alkali metals to alkaline earthmetals).
  • the lecithin coating may be applied to the substrate by any conventional manner. For example, in U.S. Patent No. 3,291,614, several methods for applying a lecithin to a powder are shown. In one instance it is stated that whole milk powder is coated with a spray of soybean lecithin- water emulsion.
  • the lecithin used in the present invention can be derived from any vegetable oil, which may be solid or liquid at ambient temperature.
  • suitable vegetable oils for use include, for example, soybean oil, sunflower oil, rapeseed oil, cottonseed oil, olive oil, corn oil, ground nut oil, safflower oil, linola oil, linseed oil, palm oil, coconut oil, and mixtures thereof. Particularly useful is soybean oil.
  • Suitable oils of animal origin for use include, for example, butter fat and fish oil. The total of the animal fats should be below 30 wt.% of total oils in the food composition.
  • Wettability In this procedure a powder is brought into water. The wettability is the amount of time lapsed to wet all the powder.
  • the apparatus required for the test includes a 1000 ml glass beaker, a plastic plate (0.12m x 0.12m), and a cylinder having a diameter of 0.075 m and a height of 0.065 m.
  • Example 2 In this example, a hydrophilic powder, whole milk powder, BBA Lactalis Industry, 26% fat content is coated with a membrane separated lecithin having a ratio of alkali metals to alkaline earth metals of about 2.4, and containing about 58 to 72% soybean oil.
  • Example 3 Three hundred (300) grams of a soy protein isolate powder having an average particle size of 50 microns was injected in a high velocity air stream into a fluid bed coating chamber. The fluidized powder was sprayed with 40 g of a 15% aqueous dispersion of soybean lecithin having 2% oil and having a ratio of alkali metals to alkaline earthmetals of 2.5, at a spray rate of 14 g/minute with inlet/outlet temperatures at 55/25C, air flow of 8-10 SCFM and spray air pressure set at 10 psi. After coating, the lecithin coated soy protein isolate powder was transferred into a container.
  • Example 4 Five hundred (500) grams cocoa with 10-12% fat and average particle size 20-30 microns was injected in a high velocity air stream into a fluid bed coating chamber (FluidAIR Magnaflo Model 2).
  • the fluidized powder was sprayed with lOOg of 15% aqueous dispersion of lecithin having 28% oil and a ratio of alkali metals to alkaline earthmetals of 2.4 with the following process conditions: Inlet-outlet temperatures of 50C/30C, spray air pressure of 8 psi, airflow 8-10 of

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Nutrition Science (AREA)
  • Biochemistry (AREA)
  • Biophysics (AREA)
  • Molecular Biology (AREA)
  • General Preparation And Processing Of Foods (AREA)

Abstract

L'invention concerne des produits alimentaires cuits au four contenant des produits spécifiques à base de lécithine.
EP03818178A 2003-07-24 2003-07-24 Preparation de poudre recouverte Withdrawn EP1648236A4 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/US2003/023308 WO2005016005A1 (fr) 2003-07-24 2003-07-24 Preparation de poudre recouverte

Publications (2)

Publication Number Publication Date
EP1648236A1 true EP1648236A1 (fr) 2006-04-26
EP1648236A4 EP1648236A4 (fr) 2009-02-11

Family

ID=34192516

Family Applications (1)

Application Number Title Priority Date Filing Date
EP03818178A Withdrawn EP1648236A4 (fr) 2003-07-24 2003-07-24 Preparation de poudre recouverte

Country Status (4)

Country Link
EP (1) EP1648236A4 (fr)
AU (1) AU2003261256A1 (fr)
TW (1) TW200514511A (fr)
WO (1) WO2005016005A1 (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2474939A (en) * 2009-10-28 2011-05-04 St Giles Foods Ltd Sprayable flavoured edible compositions
EP2740369A1 (fr) * 2012-12-07 2014-06-11 Loders Croklaan B.V. Procédé de préparation d'un produit ou ingrédient de confiserie

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1509543A (en) * 1974-05-16 1978-05-04 Unilever Ltd Purification process
US4339465A (en) * 1979-10-15 1982-07-13 Strouss Oran L Method of de-panning baked goods
WO1983003843A1 (fr) * 1982-04-21 1983-11-10 Unilever Nv Raffinage
JPS60126036A (ja) * 1983-12-10 1985-07-05 Fuji Oil Co Ltd 粉末状大豆蛋白の製造法
US4501757A (en) * 1984-02-01 1985-02-26 Don L. Smith Yeast and dough condition compositions
US5023075A (en) * 1989-10-10 1991-06-11 Revlon, Inc. Microfine cosmetic powder comprising polymers, silicone, and lecithin
DE69323432T2 (de) * 1992-09-30 1999-07-15 The Pillsbury Co., Minneapolis, Minn. Mit mikrowellen behandelbare vorgebrannte pastösesystemen
US6833149B2 (en) * 1999-01-14 2004-12-21 Cargill, Incorporated Method and apparatus for processing vegetable oil miscella, method for conditioning a polymeric microfiltration membrane, membrane, and lecithin product
US6406729B1 (en) * 2000-04-14 2002-06-18 Land O′Lakes, Inc. Method and process for producing an improved milk replacer

Also Published As

Publication number Publication date
AU2003261256A1 (en) 2005-03-07
WO2005016005A1 (fr) 2005-02-24
EP1648236A4 (fr) 2009-02-11
TW200514511A (en) 2005-05-01

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