EP1070734A3 - Compositions de revêtement de silicone anti-adhésives - Google Patents
Compositions de revêtement de silicone anti-adhésives Download PDFInfo
- Publication number
- EP1070734A3 EP1070734A3 EP00305833A EP00305833A EP1070734A3 EP 1070734 A3 EP1070734 A3 EP 1070734A3 EP 00305833 A EP00305833 A EP 00305833A EP 00305833 A EP00305833 A EP 00305833A EP 1070734 A3 EP1070734 A3 EP 1070734A3
- Authority
- EP
- European Patent Office
- Prior art keywords
- units
- release coating
- coating compositions
- silicone release
- formula
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Paints Or Removers (AREA)
- Silicon Polymers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Laminated Bodies (AREA)
- Adhesive Tapes (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB9917372 | 1999-07-23 | ||
| GBGB9917372.6A GB9917372D0 (en) | 1999-07-23 | 1999-07-23 | Silicone release coating compositions |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| EP1070734A2 EP1070734A2 (fr) | 2001-01-24 |
| EP1070734A3 true EP1070734A3 (fr) | 2001-07-11 |
| EP1070734B1 EP1070734B1 (fr) | 2003-03-26 |
Family
ID=10857856
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP00305833A Expired - Lifetime EP1070734B1 (fr) | 1999-07-23 | 2000-07-11 | Compositions de revêtement de silicone anti-adhésives |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US6806339B2 (fr) |
| EP (1) | EP1070734B1 (fr) |
| JP (2) | JP5039250B2 (fr) |
| KR (1) | KR100748375B1 (fr) |
| CN (1) | CN1195789C (fr) |
| AT (1) | ATE235530T1 (fr) |
| DE (1) | DE60001779T2 (fr) |
| ES (1) | ES2194678T3 (fr) |
| GB (1) | GB9917372D0 (fr) |
Families Citing this family (117)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10235021A1 (de) * | 2002-07-31 | 2004-02-19 | Nordenia Deutschland Gronau Gmbh | Selbstklebende Oberflächenschutzfolie, insbesondere zur Abdeckung von lackierten Blechen und Hochglanzblechen aus Aluminium oder Edelstahl |
| US6774201B2 (en) * | 2002-11-15 | 2004-08-10 | General Electric Company | Star-branched silicone polymers as anti-mist additives for coating applications |
| US7135512B2 (en) * | 2002-11-15 | 2006-11-14 | General Electric Company | Star-branched silicone polymers as anti-mist additives for coating applications |
| GB0227066D0 (en) * | 2002-11-20 | 2002-12-24 | Dow Corning | Silicone release coatings |
| MXPA05006507A (es) * | 2002-12-20 | 2006-02-17 | Chemocentryx | Inhibidores de ccxckr2 expresado en tumor humano. |
| EP1603988B1 (fr) * | 2003-03-17 | 2008-07-02 | Dow Corning Corporation | Adhesifs sensibles a la pression sans solvant presentant une force de cohesion amelioree a temperature elevee |
| GB0316162D0 (en) | 2003-07-10 | 2003-08-13 | Dow Corning | Silicone release coating compositions |
| JP5525121B2 (ja) * | 2003-12-23 | 2014-06-18 | モーメンテイブ・パーフオーマンス・マテリアルズ・ゲゼルシヤフト・ミツト・ベシユレンクテル・ハフツング | 表面の性質の改変された硬化型シロキサン組成物 |
| US20070289495A1 (en) * | 2004-11-18 | 2007-12-20 | Dow Corning Corporation | Silicone Release Coating Compositions |
| WO2007015944A2 (fr) | 2005-07-28 | 2007-02-08 | Dow Corning Corporation | Compositions de revêtement antiadhésif ayant de meilleurs profils des forces de séparation |
| JP4892922B2 (ja) * | 2005-10-14 | 2012-03-07 | 信越化学工業株式会社 | 重剥離コントロール剤及びそれを用いた無溶剤型剥離紙用シリコーン組成物 |
| US7956123B2 (en) * | 2005-10-24 | 2011-06-07 | Momentive Performance Materials Inc. | Solvent resistant polyurethane adhesive compositions |
| US20070261342A1 (en) * | 2006-04-25 | 2007-11-15 | Building Materials Investment Corporation | Factory fabricated expansion joint cover |
| GB0616021D0 (en) | 2006-08-14 | 2006-09-20 | Dow Corning | Silicone release coating compositions |
| JP5420166B2 (ja) * | 2006-12-28 | 2014-02-19 | 東レ・ダウコーニング株式会社 | 無溶剤型剥離性硬化皮膜形成性オルガノポリシロキサン組成物および剥離性硬化皮膜を有するシート状基材 |
| JP4782046B2 (ja) * | 2007-03-05 | 2011-09-28 | 信越化学工業株式会社 | フィルム用無溶剤型シリコーン剥離剤組成物及びそれを用いてなる剥離フィルム |
| US8334037B2 (en) | 2007-05-11 | 2012-12-18 | 3M Innovative Properties Company | Multi-layer assembly, multi-layer stretch releasing pressure-sensitive adhesive assembly, and methods of making and using the same |
| PL2150575T3 (pl) * | 2007-05-25 | 2017-05-31 | Dow Corning Corporation | Kompozycja powłoki antyadhezyjnej i sposób jej wytwarzania |
| JP5060873B2 (ja) * | 2007-08-24 | 2012-10-31 | 東レ・ダウコーニング株式会社 | シリコーン系感圧接着剤組成物および感圧接着テープもしくはシート |
| EP2255394A2 (fr) | 2008-03-14 | 2010-12-01 | Dow Corning Corporation | Module de cellule photovoltaïque et procédé de formation associé |
| DE102008027501A1 (de) | 2008-06-10 | 2009-12-17 | Tesa Se | Haftklebemasse mit verbessertem Abzugsverhalten |
| DE102008027502A1 (de) | 2008-06-10 | 2009-12-17 | Tesa Se | Verfahren zur Herstellung von Releaselinern |
| CN102931260A (zh) | 2008-10-31 | 2013-02-13 | 陶氏康宁公司 | 光生伏打电池组件和形成方法 |
| KR20110103401A (ko) * | 2008-11-26 | 2011-09-20 | 다우 코닝 도레이 캄파니 리미티드 | 무용제형 박리성 경화 피막 형성성 오가노폴리실록산 조성물 및 박리성 경화 피막을 포함하는 시트형 기재 |
| DE102009011166A1 (de) | 2009-03-04 | 2010-09-09 | Tesa Se | Herstellung von Trennmaterialien für Haftklebebänder |
| KR101828999B1 (ko) | 2009-09-03 | 2018-02-13 | 다우 코닝 코포레이션 | 점액성 실리콘 유체를 이용한 퍼스널 케어 조성물 |
| JP2013516520A (ja) | 2009-12-30 | 2013-05-13 | ダウ コーニング コーポレーション | エアバッグ用シリコーンコーティング組成物 |
| WO2011082136A1 (fr) | 2009-12-30 | 2011-07-07 | Dow Corning Corporation | Revêtement de silicone sur des coussins de sécurité gonflables |
| EP2444450A1 (fr) * | 2010-10-19 | 2012-04-25 | Hinterwaldner Consulting & Partner (Gbr) | Compositions destinées à la fabrication de revêtements antiadhésifs |
| GB201018759D0 (en) | 2010-11-08 | 2010-12-22 | Dow Corning | Grease resistant coating for fibrous materials |
| JP5819606B2 (ja) * | 2010-12-17 | 2015-11-24 | 日華化学株式会社 | オルガノ変性シリコーン及びそれを含有する金型鋳造用離型剤、並びに、それらの製造方法 |
| DE102011077004A1 (de) * | 2011-06-06 | 2012-12-06 | Wacker Chemie Ag | Siliconlöser |
| GB201121124D0 (en) | 2011-12-08 | 2012-01-18 | Dow Corning | Hydrolysable silanes |
| GB201121132D0 (en) | 2011-12-08 | 2012-01-18 | Dow Corning | Modifying polymeric materials by amines |
| GB201121128D0 (en) | 2011-12-08 | 2012-01-18 | Dow Corning | Treatment of filler with silane |
| GB201121133D0 (en) | 2011-12-08 | 2012-01-18 | Dow Corning | Hydrolysable silanes |
| GB201121122D0 (en) | 2011-12-08 | 2012-01-18 | Dow Corning | Hydrolysable silanes and elastomer compositions containing them |
| CN102898650B (zh) * | 2012-05-11 | 2015-04-22 | 杭州师范大学 | 一种t链节含苯基的mtq类型硅树脂及其制备方法 |
| WO2014019840A2 (fr) | 2012-08-01 | 2014-02-06 | Dow Corning Corporation | Dispersions de silicone aqueuses et leur préparation |
| CN104395377B (zh) | 2012-08-01 | 2017-02-22 | 道康宁公司 | 水性有机硅分散体和膜及其制备 |
| KR102186328B1 (ko) | 2013-02-11 | 2020-12-03 | 다우 실리콘즈 코포레이션 | 알콕시-작용성 유기폴리실록산 수지 및 중합체와 이의 관련된 형성 방법 |
| US10370572B2 (en) | 2013-02-11 | 2019-08-06 | Dow Silicones Corporation | Moisture-curable hot melt silicone adhesive compositions including an alkoxy-functional siloxane reactive resin |
| CN105189685B (zh) | 2013-02-11 | 2017-08-08 | 道康宁公司 | 用于形成导热热自由基固化有机硅组合物的方法 |
| JP6370812B2 (ja) | 2013-02-11 | 2018-08-08 | ダウ シリコーンズ コーポレーション | クラスタ化官能性ポリオルガノシロキサン、これを生成するプロセス、及びこれを使用する方法 |
| GB201323041D0 (en) | 2013-12-23 | 2014-02-12 | Dow Corning | Curable coating compositions containing an unsaturated alkoxysilane |
| US9487677B2 (en) | 2014-05-27 | 2016-11-08 | Momentive Performance Materials, Inc. | Release modifier composition |
| WO2015196440A1 (fr) | 2014-06-27 | 2015-12-30 | Dow Corning (China) Holding Co., Ltd. | Composition de revêtement antiadhésif à base de silicone et revêtement antiadhésif à base de silicone en émulsion à faible force de décollement pour films et papiers comprenant un revêtement antiadhésif durci |
| FR3026346B1 (fr) * | 2014-09-26 | 2016-11-25 | Ahlstroem Oy | Support a base de fibres cellulosiques, son procede de fabrication et son utilisation en tant que support pour rubans adhesifs |
| KR102248716B1 (ko) * | 2014-09-30 | 2021-05-04 | 코오롱인더스트리 주식회사 | 이형필름 및 이의 제조방법 |
| KR101987005B1 (ko) * | 2015-04-08 | 2019-06-10 | 다우 실리콘즈 코포레이션 | 점액성 실리콘 에멀젼 |
| EP3368622B1 (fr) | 2015-10-26 | 2020-10-14 | Dow (Shanghai) Holding Co., Ltd. | Composition de revêtement anti-adhésif de silicone et article ayant un revêtement anti-adhésif polymérisé |
| EP3196229B1 (fr) * | 2015-11-05 | 2018-09-26 | Dow Silicones Corporation | Polyorganosiloxanes ramifiés et compositions durcissables associées, procédés, utilisations et dispositifs |
| EP3429551B1 (fr) * | 2016-03-14 | 2020-12-23 | Dow Silicones Corporation | Composition des siloxanes |
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| EP3645491B1 (fr) | 2017-10-19 | 2021-09-15 | Dow Silicones Corporation | Compositions de polyorganosiloxane contenant un 1-alcynyle-1-cyclohexanol à substitution en position 2 utiles en tant qu'inhibiteur de réaction d'hydrosilylation |
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| DE102018207182A1 (de) | 2018-05-09 | 2019-11-14 | Tesa Se | Klebeband mit Releaseliner auf Basis einer haftklebrigen Silikonbeschichtung |
| JP7328259B2 (ja) | 2018-06-29 | 2023-08-16 | ダウ シリコーンズ コーポレーション | アンカー添加剤並びにその調製方法及び使用 |
| US20210246337A1 (en) | 2018-06-29 | 2021-08-12 | Dow Silicones Corporation | Solventless silicone pressure sensitive adhesive and methods for making and using same |
| DE102018217567A1 (de) | 2018-10-15 | 2020-04-16 | Tesa Se | Zusammensetzung für eine Trennbeschichtung, welche einen niedrigen Reibungskoeffizienten und einen geringen Silikonübertrag aufweist |
| DE102018220199A1 (de) | 2018-11-23 | 2020-05-28 | Tesa Se | Zusammensetzung für eine Trennbeschichtung mit niedrigem Reibungskoeffizienten |
| DE102018220200A1 (de) | 2018-11-23 | 2020-05-28 | Tesa Se | Zusammensetzung für eine Trennbeschichtung mit niedrigem Reibungskoeffizienten |
| US20220041812A1 (en) | 2018-12-21 | 2022-02-10 | Dow Silicones Corporation | Method for preparing a functionalized polyorganosiloxane |
| EP3898775B1 (fr) | 2018-12-21 | 2025-03-12 | Dow Silicones Corporation | Organosiloxanes polyfonctionnels, compositions les contenant, et leurs procédés de préparation |
| WO2020131369A1 (fr) | 2018-12-21 | 2020-06-25 | Dow Silicones Corporation | Procédés de production d'organosiloxanes polyfonctionnels et compositions les contenant |
| KR102814239B1 (ko) | 2018-12-21 | 2025-05-29 | 다우 실리콘즈 코포레이션 | 다작용성 유기실록산, 이를 함유하는 조성물, 및 이의 제조 방법 |
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| JP7609808B2 (ja) | 2019-05-16 | 2025-01-07 | ダウ シリコーンズ コーポレーション | ポリシロキサン制御剥離添加剤、それを調製するための方法、及び剥離コーティング組成物 |
| EP3973025B1 (fr) * | 2019-05-21 | 2023-11-22 | Dow Silicones Corporation | Revêtement à libération de polyorganosiloxane et sa préparation et son utilisation |
| EP4051735A4 (fr) | 2019-10-30 | 2023-08-09 | Dow Silicones Corporation | Granulés de polyorganosiloxane sans solvant et processus pour leur préparation et leur utilisation |
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| EP4085090A1 (fr) * | 2019-12-30 | 2022-11-09 | Dow Silicones Corporation | Résines de silicate à l'état liquide |
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| WO2022261853A1 (fr) | 2021-06-16 | 2022-12-22 | Dow Silicones Corporation | Composition adhésive sensible à la pression au silicone contenant un additif polyfluoropolyéther silane et procédés de préparation et d'utilisation de ladite composition |
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| JP2024536162A (ja) | 2021-10-06 | 2024-10-04 | ダウ グローバル テクノロジーズ エルエルシー | イミン官能性有機ケイ素化合物及び一級アミノ官能性有機ケイ素化合物の調製 |
| CN113896894B (zh) * | 2021-11-03 | 2023-03-28 | 万华化学集团股份有限公司 | 一种支化型交联剂及其制备方法和应用 |
| EP4437031A2 (fr) | 2021-11-22 | 2024-10-02 | Dow Global Technologies LLC | Préparation de composés d'organosilicium à fonction carbinol |
| WO2023115340A1 (fr) | 2021-12-21 | 2023-06-29 | Dow Silicones Corporation | Composition de revêtement antiadhésive |
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| EP4496833A1 (fr) | 2022-03-21 | 2025-01-29 | Dow Global Technologies LLC | Préparation de composés organosiliciés à fonctionnalité carboxy |
| US20250145647A1 (en) | 2022-04-13 | 2025-05-08 | Dow Silicones Corporation | Preparation of organosilicon compounds with vinylester functionality |
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| CN120225613A (zh) | 2022-12-23 | 2025-06-27 | 美国陶氏有机硅公司 | 制备可固化导热组合物的方法 |
| CN121079337A (zh) | 2023-05-22 | 2025-12-05 | 美国陶氏有机硅公司 | 具有支化聚醚侧基的有机硅聚醚 |
| CN121002099A (zh) | 2023-05-22 | 2025-11-21 | 美国陶氏有机硅公司 | 具有直链聚醚侧基的有机硅聚醚 |
| WO2025029496A1 (fr) | 2023-08-01 | 2025-02-06 | Dow Global Technologies Llc | Compositions de siloxane durcissables par rayonnement et leurs procédés de préparation et d'utilisation |
| WO2025038266A1 (fr) | 2023-08-14 | 2025-02-20 | Dow Global Technologies Llc | Hydroformylation catalysée par du cobalt de polyorganosiloxanes à fonction vinyle |
| WO2025226433A1 (fr) | 2024-04-23 | 2025-10-30 | Dow Silicones Corporation | Revêtement antiadhésif au silicium présentant des propriétés de barrière contre la graisse et l'eau |
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| EP0464706A1 (fr) * | 1990-06-29 | 1992-01-08 | Toshiba Silicone Co., Ltd. | Composition de silicone durcissable par rayonnement ultraviolet |
| EP0652257A2 (fr) * | 1993-11-05 | 1995-05-10 | Dow Corning Limited | Composition de polysiloxane anticollant |
| US5446087A (en) * | 1992-12-04 | 1995-08-29 | Rhone-Poulenc Chimie | Curable release compositions comprising novel silicone adhesion modifier |
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| JPS55110155A (en) * | 1979-02-16 | 1980-08-25 | Toray Silicone Co Ltd | Organopolysiloxane composition forming releasable film |
| US4386135A (en) | 1982-01-11 | 1983-05-31 | Minnesota Mining And Manufacturing Company | Stable silicone-coated release liner for pressure-sensitive adhesive sheets |
| JPS6327560A (ja) | 1986-07-21 | 1988-02-05 | Shin Etsu Chem Co Ltd | 離型用シリコ−ン組成物 |
| US4774111A (en) | 1987-06-29 | 1988-09-27 | Dow Corning Corporation | Heat-curable silicone compositions comprising fumarate cure-control additive and use thereof |
| US5063254A (en) | 1988-04-04 | 1991-11-05 | Loctite Corporation | MTQ/polysiloxane hybrid resins, method of making the same, and coating/potting compositions containing the same |
| JP2750896B2 (ja) * | 1989-05-31 | 1998-05-13 | 東レ・ダウコーニング・シリコーン株式会社 | 剥離性硬化皮膜形成用オルガノポリシロキサン組成物 |
| DE3920269A1 (de) | 1989-06-21 | 1991-01-17 | Bayer Ag | Beschichtungsmittel zum herstellen haftungsmindernder beschichtungen |
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| CA2085673A1 (fr) * | 1992-01-23 | 1993-07-24 | Brian J. Ward | Elastomeres de silicone durcissant a un faible taux de compression |
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| JP3218872B2 (ja) * | 1994-07-20 | 2001-10-15 | 信越化学工業株式会社 | 有機ケイ素樹脂の製造方法 |
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1999
- 1999-07-23 GB GBGB9917372.6A patent/GB9917372D0/en not_active Ceased
-
2000
- 2000-07-11 DE DE60001779T patent/DE60001779T2/de not_active Expired - Lifetime
- 2000-07-11 ES ES00305833T patent/ES2194678T3/es not_active Expired - Lifetime
- 2000-07-11 EP EP00305833A patent/EP1070734B1/fr not_active Expired - Lifetime
- 2000-07-11 AT AT00305833T patent/ATE235530T1/de not_active IP Right Cessation
- 2000-07-18 JP JP2000217590A patent/JP5039250B2/ja not_active Expired - Fee Related
- 2000-07-21 KR KR1020000041965A patent/KR100748375B1/ko not_active Expired - Lifetime
- 2000-07-21 CN CNB001216279A patent/CN1195789C/zh not_active Expired - Lifetime
-
2001
- 2001-11-05 US US09/992,572 patent/US6806339B2/en not_active Expired - Lifetime
-
2012
- 2012-01-13 JP JP2012004990A patent/JP5194178B2/ja not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0464706A1 (fr) * | 1990-06-29 | 1992-01-08 | Toshiba Silicone Co., Ltd. | Composition de silicone durcissable par rayonnement ultraviolet |
| US5446087A (en) * | 1992-12-04 | 1995-08-29 | Rhone-Poulenc Chimie | Curable release compositions comprising novel silicone adhesion modifier |
| EP0652257A2 (fr) * | 1993-11-05 | 1995-05-10 | Dow Corning Limited | Composition de polysiloxane anticollant |
Also Published As
| Publication number | Publication date |
|---|---|
| ES2194678T3 (es) | 2003-12-01 |
| DE60001779D1 (de) | 2003-04-30 |
| US20020061998A1 (en) | 2002-05-23 |
| ATE235530T1 (de) | 2003-04-15 |
| US6806339B2 (en) | 2004-10-19 |
| JP5194178B2 (ja) | 2013-05-08 |
| EP1070734B1 (fr) | 2003-03-26 |
| DE60001779T2 (de) | 2004-02-05 |
| JP2001064390A (ja) | 2001-03-13 |
| KR100748375B1 (ko) | 2007-08-10 |
| EP1070734A2 (fr) | 2001-01-24 |
| GB9917372D0 (en) | 1999-09-22 |
| KR20010049836A (ko) | 2001-06-15 |
| CN1195789C (zh) | 2005-04-06 |
| JP2012117072A (ja) | 2012-06-21 |
| CN1281881A (zh) | 2001-01-31 |
| JP5039250B2 (ja) | 2012-10-03 |
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