EP0760713A1

EP0760713A1 - Device and process for separating and qualifying particles forming a granular product

Info

Publication number: EP0760713A1
Application number: EP95918502A
Authority: EP
Inventors: Laurent Dürst
Original assignee: Individual
Current assignee: Individual
Priority date: 1994-06-01
Filing date: 1995-05-31
Publication date: 1997-03-12
Anticipated expiration: 2015-05-31
Also published as: ATE166006T1; DE69502495D1; FR2720666B1; WO1995032810A1; EP0760713B1; CA2191365A1; US5871103A; FR2720666A1; JP3485572B2; DE69502495T2; JPH10500894A

Abstract

The device (10) comprises a separation vat (11) for separating the particles and comprising a cylindrical guiding channel (16) communicating with a lower container (17) formed with two parallel planar walls (21) separated by a distance smaller than the maximum width of the guiding channel. Said device is further provided with a motion generator (24) arranged to generate a substantially laminar fluid flow in the guiding channel, means (18) for conveying said particles to the guiding channel and means (13) for recovering the sorted particles. The particles introduced in the guiding channel (16) receive the kinetic energy of the fluid flow, fall in the lower container (17) and arrive to the recovery means (13) at positions which depend of the mass and the kinetic energy amount received.

Description

DEVICE AND METHOD FOR SEPARATING AND QUALIFYING PARTICLES FORMING A GRANULAR PRODUCT

The present invention relates to a device for separating and qualifying particles forming a granular product, this device comprising a particle separation tank, means for bringing the particles into the tank, a member for separating these particles formed from less a movement generator arranged to generate in said separation tank, a longitudinal flow of a fluid carrying said particles, and means for recovering said particles.

It also relates to a process for separating and qualifying particles forming a granular product, in which said particles are gradually introduced into a separation device as defined above, and the particles are collected on recovery means placed under said tank, taking into account their longitudinal position on these recovery means.

There are currently several methods for separating particles constituting a granular product such as a powder, pellets or seeds.

Among these methods, we can cite the separation by sieving which consists in placing the product on a series of superimposed sieves having increasingly fine meshes, and in recovering the product on each sieve.

This process has various drawbacks due in particular to clogging of the sieves and to the erosion of the particles against the mesh of the sieve.

Another process allowing the separation and the qualification of the particles of a granular product, as well as the device for its implementation, are described in the American patent published under the number US-A-4,213,852. The device comprises a tank closed in which is disposed a tube having an upstream end and a downstream end. A hopper is placed above this tube near its upstream end and allows the introduction of particles. A fan is mounted near the downstream opening of the tube and generates a closed-circuit air flow circulating in one direction in the tube and in the other direction between the tube and the closed container. Wires are placed near the upstream end of the tube so as to reduce the turbulence of the air flow and thus create the most laminar flow possible. Recovery bins are arranged in the bottom of the tube, perpendicular to the axis of this tube. The entire device is designed to minimize pressure losses in the tube.

When the particles are introduced into the tube through the hopper, they are entrained by the air flow over a distance depending on their weight and their surface perpendicular to the air flow. These particles then fall into the recovery tanks and are separated into slices.

This device has various drawbacks. In particular, the desired laminar flow is difficult to achieve with a device of this type because of the shape of the tank and the circuit that the air must perform. In practice, a substantially laminar flow can only be obtained for relatively low flow speeds, which does not make it possible to sort heavy particles. This device is intended to sort particles whose diameter is between 10 and 1000 μm.

The present invention proposes to overcome these drawbacks by providing a device and a method making it possible to obtain a homogeneous flow for high flow speeds, which makes it possible to separate particles of large size and thus to diversify the industrial applications of the device.

This object is achieved by a device as defined in the preamble and characterized in that the separation tank comprises a guide channel in which said fluid flow circulates, and a lower container in which the fluid flow does not circulate, this channel and this container being in communication over their entire length.

According to a preferred embodiment, the guide channel is substantially cylindrical and is open at its two ends.

The lower container preferably comprises two parallel flat walls and a bottom comprising at least one opening, the distance between these two flat walls being less than the maximum width of the guide channel. According to an advantageous embodiment, the movement generator comprises a pump arranged upstream of the guide channel and arranged to propel the fluid through this channel.

The device preferably comprises at least one source of fluid arranged to generate a downward flow of fluid, perpendicular to the longitudinal flow of fluid generated by the motion generator.

According to an advantageous embodiment, the device comprises at least one vibration generator arranged to generate a vibration of the fluid in the guide channel, in a direction transverse to the longitudinal flow generated by the motion generator.

According to a preferred embodiment, the device comprises weighing means arranged to measure the mass of the particles as a function of their position on said recovery means, and a data processing device arranged to record these masses and these positions.

This object is also achieved by a method as defined in the preamble and characterized in that a longitudinal flow of a fluid is generated in the guide channel, without generating a flow of the fluid in the lower container.

According to a first embodiment, each transverse portion of particles is weighed on the recovery means, a mass curve is established for each portion as a function of its position on the recovery means and the mass curve is compared of each portion as a function of its position on the recovery means to a similar curve produced using a granular reference product whose characteristics are known.

According to an alternative embodiment, a downward flow of fluid is generated in a direction substantially perpendicular to the direction of the longitudinal flow of fluid generated by said motion generator.

According to another alternative embodiment, transverse horizontal vibrations are generated in the separation device. The present invention and its advantages will appear better with reference to preferred embodiments of the present invention and to the accompanying drawings in which:

- Figure 1 is an overview of the device according to the present invention;

- Figure 2 is a perspective view of the separation tank and means for recovering the device according to the present invention;

- Figure 3 is a curve illustrating the amount of product obtained as a function of the position on the recovery means; and.

- Figures 4 to 6 illustrate alternative embodiments of the device according to the present invention.

With reference to FIGS. 1 and 2, the device 10 according to the present invention essentially comprises a separation tank 11 for the particles making up the granular product, a member 12 for separating said particles, means 13 for recovering these particles, means for weighing 14 and a data processing device 15.

The separation tank 11 is formed by a cylindrical guide channel 16 open at its two ends, and by a lower container 17 closed at its two ends and disposed under the guide channel. The channel 16 and the container 17 communicate over their entire length.

The guide channel is associated with means 18 for supplying said particles, these supply means comprising for example a conveyor belt 19 arranged to transport particles of the granular product to be separated from a source of particles (not shown) to a first end 20, called the downstream end, of the guide channel 16.

The lower container 17 is formed by two parallel planar walls 21 spaced apart by a distance less than the maximum width of the guide channel 16 and greater than the largest dimension of the particles to be sorted. This container 17 has an open bottom 22 and disposed above the recovery means 13. The latter comprise an endless conveyor 23, placed over the entire length of the tank 11.

The separation member 12 comprises a movement generator 24 disposed at the downstream end 20 of the guide channel 16 and placed in such a way that it generates a substantially homogeneous and longitudinal flow of fluid in this channel. The movement generator 24 may for example be a pump, a blower or a source of water and its nature depends on the product to be separated. It must be able to transmit part of the energy of the fluid flow to the particles, without exhibiting any chemical interaction with these particles.

The weighing means 14 are placed below one end of the conveyor belt 23 so that by moving this ribbon, part of the particles which it carries falls on these weighing means.

The data processing device 15 is connected to the weighing means 14 and is arranged to record the masses measured by these weighing means as well as the movements of the endless conveyor 23.

The separation device 10 described above is essentially used for three different operations, namely the production of a reference curve, the qualification of a product and the sorting of the particles which constitute a granular product.

To make a reference curve, we proceed as follows:

- Is introduced into the separation tank 11, a granular reference product whose characteristics are known;

- A substantially homogeneous and longitudinal flow of fluid, of constant amplitude, is simultaneously generated in the guide channel 16. This flow is for example an air flow;

- the endless conveyor belt 23 being stationary, all the particles are passed through the device.

The fluid flow transmits part of its kinetic energy to the particles. Each particle receives an amount of kinetic energy which depends on different parameters such as its transverse surface which can vary at all instant, and the coefficient of friction between the particles and the fluid. These particles therefore have a speed having a horizontal component due to the flow of fluid and a vertical component due to the terrestrial attraction. The particles follow a parabolic trajectory and fall on the recovery means 13 in places depending on the different parameters mentioned above. The fluid flow undergoes a pressure drop in the guide channel 16, this pressure drop being used to improve the separation of the particles. The fluid therefore does not supply the particles with constant energy regardless of the location of the guide channel where its particles are located, but it does have an energy gradient.

- The conveyor belt 23 is advanced by a distance corresponding to the desired measurement resolution;

- Weigh the particles fallen on the weighing means 14; - this mass and a positioning reference are recorded in the data processing device 15;

- The particles are removed from the weighing means 14, the conveyor belt is again advanced and the particles which have fallen on the weighing means are weighed. This operation is repeated until no more particles remain on the conveyor belt.

It is thus possible to establish a reference curve as illustrated in FIG. 3, which is representative of the distribution of the particles of a given reference product for given measurement conditions.

When it is desired to qualify a granular product, the procedure is the same as above, in order to obtain a distribution curve of the particles of this product. This distribution curve is then compared to the reference curve, which makes it possible to observe the possible displacement of the peaks of the distribution curve relative to the reference curve. The displacement of the peaks can for example be a sign of product aging, crumbling or agglomeration of the particles. It can also reflect dehydration or absorption of water.

Finally, the third operation which can be carried out by means of the separation device of FIGS. 1 and 2, namely the sorting of the particles forming a product, consists of separating these particles into different classes depending on their position on the conveyor belt and using only the class or classes of interest.

The separation device 30 as illustrated in FIG. 4 differs from that of FIGS. 1 and 2 essentially by the recovery means 31. These comprise a separation element 32 produced in the form of a container 33 placed under the bottom of the tank between two positioning stops 34. This device is essentially used to separate particles from a product of which only a fraction is of interest. The container is placed in a position such that the interesting fraction of the granular product falls into the latter when all of the particles pass through the separation tank. Thus, the container makes it possible to harvest a product whose particle content of interest is particularly high, while the product falling on the recovery means outside of the container 33 has a low, even zero, content of interesting particles.

The separation device 40 illustrated in FIG. 5 comprises three vibration generators 41 arranged along the guide channel 42 in the upper part of the latter. These three vibration generators generate a transverse acoustic wave in this channel, these waves each having a different natural frequency and / or amplitude. Their purpose is to modify the trajectory of the particles passing in their immediate vicinity. The light particles moving in front of one of these generators 41 will have their trajectory strongly deviated while the heavy particles will only be weakly influenced by these acoustic waves. Thus, the distribution of the particles on the recovery means can be modified by the addition of these vibration generators. A container 43 is also placed under each of these generators 41 slightly offset towards the front, in order to recover the particles in three separate batches. It is possible to modify the amplitude and the frequency of the vibrations, as well as the speed of the fluid flow so as to obtain an optimal separation.

In the separation device 50 illustrated in FIG. 6, three sources 51 of fluid are arranged above the guide channel 52 so as to generate in this channel, a downward vertical fluid flow. These sources 51 of fluid have the same function as the vibration generators 41 illustrated in the figure. 5. The recovery means 53 comprise two containers 54, 55 one of which

54 is open and connected to evacuation means (not shown) and the other of which

55 is closed. This device is particularly suitable for separating the usable particles from a mixture of particles. As in the embodiment illustrated in FIG. 5, it is possible to vary the speeds of the different flows, so as to obtain the best possible separation. These flow rates are determined experimentally depending on the type of product to be sorted and the desired result.

The device according to the present invention can be used in numerous fields for the separation, sorting, qualification and control of granular products. For each type of use and for each desired form of result, the various components of the device and in particular the movement generator and the recovery means must be adapted. Among the many possible applications, there are a few examples.

In a production line in which a granular product such as a food powder intervenes, it is desired to control the stability of various parameters of the product, these parameters possibly being its composition, the size of the particles which form it, their water content. , etc. For this, it suffices to make a curve representing the mass of particles in transverse sections on the conveyor belt and to compare this curve with a reference curve. This type of measurement allows continuous control of the quality of a product. It is thus possible to react almost immediately when this product no longer meets the imposed criteria, which results in an offset or a deformation of the distribution curve of the product compared to the reference curve.

When it is desired to separate a usable fraction from a mixture of particles containing an unusable fraction, such as seeds being germinated in a batch of seeds at different stages of maturity, a separation element is placed on the recovery means. This separating element may consist of a transverse wall or of a recovery tank into which the interesting fraction of the mixture falls. The determination of the position of the wall or of the tank makes it possible to choose the fraction used of the mixture. The device according to the present invention can, for example, also be used to separate a gold powder from the rock which contains it. To this end, the rock is ground into fine particles, then introduced into the device. In this embodiment, the fluid flowing in the guide channel is water. Three vertical water jets are arranged at the top of the tank. The particles are entrained by the longitudinal water flow. When they pass through the first vertical water jet, the heavy particles have a high kinetic energy and their trajectory is practically not affected by the water jet. On the other hand, sparse particles are entrained at the bottom of the tank by this first jet of water. When the particles arrive at the second water jet, they have lost part of their kinetic energy by pressure drop. The second jet of water can thus capture the least dense particles. Finally, the third jet captures the densest particles which can be collected in an independent container. As the gold particles are the densest, the first container will contain a high percentage of gold.

It should be noted that the separation method of the present invention is fully compatible with the current methods of the prior art. Thus, it is possible to reuse reference curves of given products, established according to other methods. This process also allows a particularly fine and precise analysis of granular products. It is therefore possible to refine the reference curves of the prior art.

The separation process according to the present invention further allows the study of the friability of a product. This study can be carried out by passing a batch of product through the device, then subjecting this product to a stress and passing this same batch through the device. The comparison of the two particle distribution curves makes it possible to characterize the friability of the product.

In order to be able to use such a device correctly, it is essential that the flow of fluid circulating in the guide channel is as turbulent as possible. This is very easily obtained in the device according to the present invention, due to the geometric shape of this device. The fluid flow essentially flows in the guide channel. This flow is little affected by the presence of particles since they only cross this channel for a lapse of time. very short time. The flow can be relatively turbulent, even at high speeds, which makes it possible to sort large particles.

The products used can for example be food powders, vegetable seeds, mechanical parts such as timepieces, mineral mixtures or pharmaceutical granules. The fluid used to generate a flow can for example be a gas such as air or a neutral gas, or a liquid such as water or mercury.

The guide channel can have an annular shape so that the fluid circulates in a closed circuit in the device. In this way, only a small amount of fluid is necessary and it is not wasted which can be advantageous in the case of an expensive or polluting fluid for example.

The width of the lower container could be adjustable so as to be adapted to the dimensions of the particles to be sorted.

The recovery means could be formed by a conveyor placed perpendicular to the guide channel. This embodiment is similar to the cases illustrated in Figures 4 and 5 in which the recovery means comprise a container. These recovery means can also include a container disposed between the parallel walls of the tank.

The process according to the present invention can be used either only for separating the particles forming the granular product, or for separating and qualifying them.

It is also possible to electrically charge the guide channel so as to separate particles also having an electric charge, such as for example particles of charged polyethylene or polyvinyl chloride.

Claims

1. Device for separating and qualifying particles forming a granular product, this device comprising a particle separation tank, means for bringing the particles into the tank, a member for separating these particles formed from at least one generator movements arranged to generate in said separation tank, a longitudinal flow of a fluid carrying said particles, and means for recovering said particles, characterized in that the separation tank (11) comprises a guide channel (16, 42 , 52) in which said fluid flow circulates, and a lower container (17) in which the fluid flow does not circulate, this channel and this container being in communication over their entire length.

2. Device according to claim 1, characterized in that the guide channel (16, 42, 52) is substantially cylindrical and open at its two ends.

3. Device according to claim 1, characterized in that the lower container (17) has two parallel flat walls (21) and a bottom (22) having at least one opening, the distance between these two flat walls (21) being less at the maximum width of the guide channel (16, 42, 52).

4. Device according to claim 1, characterized in that the movement generator (24) comprises a pump arranged upstream of the guide channel (16) and arranged to propel the fluid through this channel.

5. Device according to claim 1, characterized in that it comprises at least one source of fluid (51) arranged to generate a downward flow of fluid, perpendicular to the longitudinal flow of fluid generated by the movement generator (24).

6. Device according to claim 1, characterized in that it comprises at least one vibration generator (41) arranged to generate a vibration of the fluid in the guide channel (42), in a transverse direction relative to the longitudinal flow generated by the motion generator.

7. Device according to claim 1, characterized in that it comprises weighing means (14) arranged to measure the mass of the particles as a function of their position on said recovery means, and a device (15) for data processing arranged to record these masses and these positions.

8. A method of separating and qualifying particles forming a granular product, in which said particles are gradually introduced into a separation device according to claim 1, and the particles are collected on recovery means placed under said tank, taking into account their longitudinal position on these recovery means, this method being characterized in that a longitudinal flow of a fluid is generated in the guide channel (16, 42, 52), without generating a flow of fluid in the lower container (17).

9. Method according to claim 8, characterized in that each transverse portion of particles is weighed on the recovery means and in that a mass curve of each portion is established as a function of its position on the means recovery (13).

10. Method according to claim 9, characterized in that the curve of the mass of each portion is compared as a function of its position on the recovery means (13) to a similar curve produced using a granular reference product of which the characteristics are known.

11. Method according to claim 8, characterized in that a downward flow of fluid is generated, in a direction substantially perpendicular to the direction of the longitudinal flow of fluid generated by said motion generator (24).

12. Method according to claim 8, characterized in that transverse horizontal vibrations are generated in the separation device (50).