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EP0595378A1 - Réacteur pour sécher des solides aqueux dans un lit fluidisé chauffé et procédé d'opération pour le réacteur - Google Patents

Réacteur pour sécher des solides aqueux dans un lit fluidisé chauffé et procédé d'opération pour le réacteur Download PDF

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Publication number
EP0595378A1
EP0595378A1 EP93202451A EP93202451A EP0595378A1 EP 0595378 A1 EP0595378 A1 EP 0595378A1 EP 93202451 A EP93202451 A EP 93202451A EP 93202451 A EP93202451 A EP 93202451A EP 0595378 A1 EP0595378 A1 EP 0595378A1
Authority
EP
European Patent Office
Prior art keywords
reactor
fluidized bed
distributor surface
vapor
distributor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP93202451A
Other languages
German (de)
English (en)
Other versions
EP0595378B1 (fr
Inventor
Hans-Jürgen Dr. Weiss
Wolfgang Frank
Wladislaw Lewandowski
Wolfgang Scheler
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GEA Group AG
Original Assignee
Metallgesellschaft AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Metallgesellschaft AG filed Critical Metallgesellschaft AG
Publication of EP0595378A1 publication Critical patent/EP0595378A1/fr
Application granted granted Critical
Publication of EP0595378B1 publication Critical patent/EP0595378B1/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00Drying solid materials or objects by processes involving the application of heat
    • F26B3/02Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air
    • F26B3/06Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried
    • F26B3/08Drying solid materials or objects by processes involving the application of heat by convection, i.e. heat being conveyed from a heat source to the materials or objects to be dried by a gas or vapour, e.g. air the gas or vapour flowing through the materials or objects to be dried so as to loosen them, e.g. to form a fluidised bed
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/001Handling, e.g. loading or unloading arrangements
    • F26B25/002Handling, e.g. loading or unloading arrangements for bulk goods

Definitions

  • the invention relates to a reactor for drying a water-containing solid in a heated fluidized bed, a vapor collecting space with a vapor outlet being located above the fluidized bed and a feed device for the water-containing solid being arranged above the vapor collecting space, and a method for operating the reactor.
  • Reactors of this type are known, e.g. described in German patent 29 01 723 and in the corresponding US patent 4,295,281 as well as in German patent 36 44 806 and in DE-A-39 43 366. These publications do not deal with how to apply the water-containing solids, which preferably form lumps on delivery, to the fluidized bed as finely and uniformly as possible.
  • a rotating, plate-like disk is known from US Pat. No. 2,412,057 in order to eject material to be dried to the side from an inlet channel.
  • the invention has for its object to separate the water-containing solids in the vapor collection space in a simple and effective manner in the reactor mentioned at the outset in such a way that larger lumps are destroyed.
  • the solids should be distributed as evenly as possible over the top of the fluidized bed. According to the invention, this is achieved in that an approximately conical distributor surface which can be rotated about a vertical axis is arranged in the vapor collecting space below the feed device and has a slope corresponding to an angle of 25 to 70 ° measured against the horizontal and at least one recess which is 30 to 90%. the theoretical total area of the distributor area.
  • the approximately conical distributor surface is not closed, but has one or more recesses through which a part of the solids comes from the distributor surface. These solids falling through the recess or recesses are moved less far radially outwards by the rotating distributor surface, so that the central region of the fluidized bed lying below the distributor surface can also be acted upon fairly uniformly with solids in the same way as the outer regions. Nevertheless, the distributor surface also acts as a baffle here, which breaks up larger agglomerates of the solids falling from above.
  • the vapor collection space is usually at least 80% and often about 100% saturated with water vapor.
  • This water vapor comes into contact with the water-containing, cold solids above the distributor surface and condenses on its surface. This favors the formation of agglomerates, which is counteracted by the rotating distributor surface.
  • the speed of rotation is usually in the range of 20 to 250 revolutions per minute.
  • the granular solids to be dried may e.g. to deal with coal, lignite, sand, ores or sludges of all kinds.
  • the distributor surface preferably has a largest diameter of 0.1 to 0.4 times the diameter of the top of the fluidized bed.
  • protrusions can be, for example, cams, teeth or ribs.
  • water-containing, granular solids are dried in a fluidized bed (2) which is indirectly heated by a heat exchanger device (3).
  • Superheated steam is preferably used as the fluidizing medium, which is brought in through the line (4) and passed into the fluidized bed (2) via a nozzle grate (5), which can be formed, for example, by horizontal pipes.
  • the water vapor formed by the drying collects together with the fluidizing medium in the vapor collecting space (8) above the fluidized bed (2), the vapor-rich atmosphere being drawn off through the vapor outlet (9). Solids that have largely dried are removed at the lower end of the reactor (1) through a metering lock (10).
  • the solids to be dried are passed through an inlet lock (11) into a storage chamber (12), the bottom (13) of which has an outlet opening (14), cf. also Fig. 2.
  • a sickle pusher (16) which is moved above the bottom (13) in the direction of arrow (15), pushes the solids to the outlet (14).
  • the vertical shaft (18) is also guided through the outlet (14), at the lower end of which an approximately conical distributor surface (19) is attached.
  • the distributor surface (19) can be driven in a manner known per se, not shown, by means of a drive about a vertical axis with adjustable speed via the shaft (18) guided to the outside.
  • the rotary movement of the distributor surface (19) takes place independently of the movement of the sickle slide (16), to which a separate drive (not shown) belongs.
  • FIG. 3 and 4 show one possibility of the shape of the distributor surface (19), with FIG. 3 being a perspective 4 and a plan view seen in the direction of arrow (B) in FIG. 3.
  • the conical distributor surface (19) has two recesses (20a) and (20b), so that the surface (19) is partially perforated.
  • the shape of these recesses can vary within a wide range, and a distributor surface can also have only one or more recesses. Without these recesses, the largest diameter of the distributor surface (19) would describe a circle, cf. Fig. 4, where this circle is indicated by dashed lines in the region of the recesses (20a) and (20b).
  • the closed circle thus formed limits the total theoretical area of the distributor area (19); the recesses are not taken into account for this theoretical total area.
  • the recesses themselves comprise an area which corresponds to 30 to 90% of the theoretical total area of the distributor area (19).
  • the size and shape of the recesses (20a) and (20b) can be selected differently, so that the design of the distributor surface can be adapted to different tasks.
  • the distributor surface (19) usually has a largest diameter (D), cf. Fig. 4, from 0.1 to 0.4 times the diameter of the top of the fluidized bed (2).
  • Fig. 5 shows a slightly different shaped distributor surface (19a), which is preferably rotated in the direction of arrow (22) around the vertical shaft (18).
  • the recesses (23a) and (23b) are delimited on the outside by the dashed circular line which marks the largest diameter.
  • This distributor surface (19a) also shows how the top of the distributor surface e.g. can be equipped with cams (23) or ribs (24), on the one hand to reinforce the breaking up of lumps of solid when rotating the surface (19a) and on the other hand to influence the solids flow. Projections of this type can improve the uniform distribution of the solids on the fluidized bed (2).

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Drying Of Solid Materials (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
EP93202451A 1992-09-25 1993-08-19 Réacteur pour sécher des solides aqueux dans un lit fluidisé chauffé et procédé d'opération pour le réacteur Expired - Lifetime EP0595378B1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE4232110A DE4232110A1 (de) 1992-09-25 1992-09-25 Reaktor zum Trocknen wasserhaltiger Feststoffe in einem beheizten Wirbelbett und Verfahren zum Betreiben des Reaktors
DE4232110 1992-09-25

Publications (2)

Publication Number Publication Date
EP0595378A1 true EP0595378A1 (fr) 1994-05-04
EP0595378B1 EP0595378B1 (fr) 1996-11-20

Family

ID=6468799

Family Applications (1)

Application Number Title Priority Date Filing Date
EP93202451A Expired - Lifetime EP0595378B1 (fr) 1992-09-25 1993-08-19 Réacteur pour sécher des solides aqueux dans un lit fluidisé chauffé et procédé d'opération pour le réacteur

Country Status (7)

Country Link
US (1) US5325607A (fr)
EP (1) EP0595378B1 (fr)
AU (1) AU661197B2 (fr)
CA (1) CA2101368A1 (fr)
DE (2) DE4232110A1 (fr)
ES (1) ES2094467T3 (fr)
GR (1) GR3021754T3 (fr)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001069150A1 (fr) * 2000-03-13 2001-09-20 Energy Engineering International (Pty) Ltd. Procede de production de produits particulaires

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU747195B2 (en) * 1997-03-26 2002-05-09 Evergreen Energy Inc. Liquid/gas/solid separation
AUPO589097A0 (en) * 1997-03-26 1997-04-24 Technological Resources Pty Limited Liquid/gas/solid separation
US6601315B2 (en) 2000-12-14 2003-08-05 Bausch & Lomb Incorporated Combined fluidized bed dryer and absorption bed

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE156981C (fr) *
US2412057A (en) * 1944-03-06 1946-12-03 Charles W Nichols Jr Furnace construction
US2668041A (en) * 1949-04-12 1954-02-02 Knibbs Norman Victor Syndney Heat treatment of finely divided solids
DE2217578A1 (de) * 1971-04-16 1972-11-02 Aktieselskabet Niro Atomizer, Soeborg (Dänemark) Vorrichtung zum Trocknen feuchter Pulver und Verfahren zum Betreiben einer derartigen Vorrichtung
US4492040A (en) * 1980-11-20 1985-01-08 A/S Niro Atomizer Method and apparatus for drying a pulverulent or particulate product

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU4296978A (en) * 1978-02-10 1979-08-16 Monash University Drying particulate materials
US4423558A (en) * 1978-09-21 1984-01-03 St. Gobain Vitrage Device for heat exchange between solid particles and a gas current
LU86335A1 (fr) * 1986-03-04 1987-11-11 Wurth Paul Sa Installation de chargement d'un four a cuve
DK222686D0 (da) * 1986-05-14 1986-05-14 Rockwool Int Mineraluldsfremstilling
DD282509A5 (de) * 1989-04-18 1990-09-12 Orgreb Inst Kraftwerke Verfahren und vorrichtung zum trocknen von feststoffmaterialien in einem indirekt beheizten wirbelschichtbett
US5243767A (en) * 1992-07-30 1993-09-14 Peter Stein Method and apparatus for processing particulate material

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE156981C (fr) *
US2412057A (en) * 1944-03-06 1946-12-03 Charles W Nichols Jr Furnace construction
US2668041A (en) * 1949-04-12 1954-02-02 Knibbs Norman Victor Syndney Heat treatment of finely divided solids
DE2217578A1 (de) * 1971-04-16 1972-11-02 Aktieselskabet Niro Atomizer, Soeborg (Dänemark) Vorrichtung zum Trocknen feuchter Pulver und Verfahren zum Betreiben einer derartigen Vorrichtung
US4492040A (en) * 1980-11-20 1985-01-08 A/S Niro Atomizer Method and apparatus for drying a pulverulent or particulate product

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001069150A1 (fr) * 2000-03-13 2001-09-20 Energy Engineering International (Pty) Ltd. Procede de production de produits particulaires

Also Published As

Publication number Publication date
ES2094467T3 (es) 1997-01-16
CA2101368A1 (fr) 1994-03-26
AU4754693A (en) 1994-03-31
GR3021754T3 (en) 1997-02-28
EP0595378B1 (fr) 1996-11-20
DE59304537D1 (de) 1997-01-02
US5325607A (en) 1994-07-05
AU661197B2 (en) 1995-07-13
DE4232110A1 (de) 1994-03-31

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